Crystallography Open Database

Information card for entry 4088278

Preview

Coordinates	4088278.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H24 F6 N2 Zn
Calculated formula	C23 H24 F6 N2 Zn
Title of publication	Electron-Deficient β-Diiminato-Zinc-Ethyl Complexes: Synthesis, Structure, and Reactivity in Ring-Opening Polymerization of Lactones
Authors of publication	Kronast, Alexander; Reiter, Marina; Altenbuchner, Peter T.; Jandl, Christian; Pöthig, Alexander; Rieger, Bernhard
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	5
Pages of publication	681
a	12.3089 ± 0.0003 Å
b	9.6492 ± 0.0003 Å
c	19.8991 ± 0.0005 Å
α	90°
β	96.953 ± 0.001°
γ	90°
Cell volume	2346.06 ± 0.11 Å³
Cell temperature	200 K
Ambient diffraction temperature	200 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0546
Residual factor for significantly intense reflections	0.0461
Weighted residual factors for significantly intense reflections	0.1156
Weighted residual factors for all reflections included in the refinement	0.1249
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
237433 (current)	2019-11-24	cif/ Adding structures of 4088276, 4088277, 4088278 via cif-deposit CGI script.	4088278.cif