Crystallography Open Database

Information card for entry 4088424

Preview

Coordinates	4088424.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H66 O Ru2
Calculated formula	C38 H42 O Ru2
Title of publication	Photoinduced Reactions of Diruthenium Tetrahydride Complexes: Carbon‒Hydrogen Bond Cleavage of Tetrahydrofuran Leading to Bridging Cyclic Fischer-Type Carbene Complexes
Authors of publication	Shimogawa, Ryuichi; Konishi, Gen-ichi; Takao, Toshiro; Suzuki, Hiroharu
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	10
Pages of publication	1446
a	10.2806 ± 0.0006 Å
b	11.8219 ± 0.0007 Å
c	15.4868 ± 0.001 Å
α	90°
β	103.059 ± 0.002°
γ	90°
Cell volume	1833.53 ± 0.19 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	4
Space group number	7
Hermann-Mauguin space group symbol	P 1 n 1
Hall space group symbol	P -2yac
Residual factor for all reflections	0.0283
Residual factor for significantly intense reflections	0.0275
Weighted residual factors for significantly intense reflections	0.0703
Weighted residual factors for all reflections included in the refinement	0.0711
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
237556 (current)	2019-11-24	cif/ Adding structures of 4088422, 4088423, 4088424, 4088425, 4088426, 4088427, 4088428 via cif-deposit CGI script.	4088424.cif