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Information card for entry 4088529
Preview
| Coordinates | 4088529.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C90 H138 F9 O9 P6 Rh3 S3 |
|---|---|
| Calculated formula | C90 H138 F9 O9 P6 Rh3 S3 |
| Title of publication | Ligand Attachment Chemistry in the Preparation of PCsp3P and PCsp2P Complexes of Rhodium |
| Authors of publication | Logan, Jessamyn R.; Piers, Warren E.; Borau-Garcia, Javier; Spasyuk, Denis M. |
| Journal of publication | Organometallics |
| Year of publication | 2016 |
| Journal volume | 35 |
| Journal issue | 9 |
| Pages of publication | 1279 |
| a | 31.7741 ± 0.0016 Å |
| b | 20.8238 ± 0.0009 Å |
| c | 34.6631 ± 0.0017 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 22935.1 ± 1.9 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 61 |
| Hermann-Mauguin space group symbol | P b c a |
| Hall space group symbol | -P 2ac 2ab |
| Residual factor for all reflections | 0.133 |
| Residual factor for significantly intense reflections | 0.074 |
| Weighted residual factors for significantly intense reflections | 0.172 |
| Weighted residual factors for all reflections included in the refinement | 0.1973 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.888 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 237642 (current) | 2019-11-24 | cif/ Adding structures of 4088526, 4088527, 4088528, 4088529, 4088530 via cif-deposit CGI script. |
4088529.cif |
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Users of the data should acknowledge the original authors of the
structural data.