Crystallography Open Database

Information card for entry 4088544

Preview

Coordinates	4088544.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H37 Br Ge Mn N3 O3
Calculated formula	C25 H37 Br Ge Mn N3 O3
Title of publication	[MnBrL(CO)4] (L = Amidinatogermylene): Reductive Dimerization, Carbonyl Substitution, and Hydrolysis Reactions
Authors of publication	Cabeza, Javier A.; García-Álvarez, Pablo; Gobetto, Roberto; González-Álvarez, Laura; Nervi, Carlo; Pérez-Carreño, Enrique; Polo, Diego
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	11
Pages of publication	1761
a	9.456 ± 0.002 Å
b	16.545 ± 0.004 Å
c	18.54 ± 0.004 Å
α	90°
β	92.705 ± 0.003°
γ	90°
Cell volume	2897.3 ± 1.1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.036
Residual factor for significantly intense reflections	0.0312
Weighted residual factors for significantly intense reflections	0.068
Weighted residual factors for all reflections included in the refinement	0.0698
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
237656 (current)	2019-11-24	cif/ Adding structures of 4088541, 4088542, 4088543, 4088544, 4088545 via cif-deposit CGI script.	4088544.cif