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Information card for entry 4088636
Preview
| Coordinates | 4088636.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C27 H51 N Os P2 |
|---|---|
| Calculated formula | C27 H51 N Os P2 |
| Title of publication | Osmium-Mediated Direct C‒H Bond Activation at the 8-Position of Quinolines |
| Authors of publication | Esteruelas, Miguel A.; Larramona, Carmen; Oñate, Enrique |
| Journal of publication | Organometallics |
| Year of publication | 2016 |
| Journal volume | 35 |
| Journal issue | 11 |
| Pages of publication | 1597 |
| a | 9.0424 ± 0.0004 Å |
| b | 16.1531 ± 0.0007 Å |
| c | 19.6745 ± 0.0009 Å |
| α | 90° |
| β | 101.304 ± 0.001° |
| γ | 90° |
| Cell volume | 2818 ± 0.2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0315 |
| Residual factor for significantly intense reflections | 0.0256 |
| Weighted residual factors for significantly intense reflections | 0.0572 |
| Weighted residual factors for all reflections included in the refinement | 0.0608 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.977 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 237739 (current) | 2019-11-24 | cif/ Adding structures of 4088636, 4088637 via cif-deposit CGI script. |
4088636.cif |
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Users of the data should acknowledge the original authors of the
structural data.