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Information card for entry 4088695
Preview
| Coordinates | 4088695.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C79 H75 Cl2 N P2 Rh |
|---|---|
| Calculated formula | C79 H75 Cl2 N P2 Rh |
| Title of publication | C‒H Activation Induced by Oxidative Addition of N‒O Bonds in Oxime Esters: Formation of Rhodacycles and Cycloaddition with Alkynes |
| Authors of publication | Shimbayashi, Takuya; Okamoto, Kazuhiro; Ohe, Kouichi |
| Journal of publication | Organometallics |
| Year of publication | 2016 |
| Journal volume | 35 |
| Journal issue | 11 |
| Pages of publication | 2026 |
| a | 13.788 ± 0.006 Å |
| b | 14.476 ± 0.006 Å |
| c | 18.584 ± 0.007 Å |
| α | 106.5 ± 0.004° |
| β | 94.464 ± 0.003° |
| γ | 109.53 ± 0.006° |
| Cell volume | 3290 ± 2 Å3 |
| Cell temperature | 143 K |
| Ambient diffraction temperature | 143 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1062 |
| Residual factor for significantly intense reflections | 0.0653 |
| Weighted residual factors for significantly intense reflections | 0.1298 |
| Weighted residual factors for all reflections included in the refinement | 0.1528 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.065 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 237772 (current) | 2019-11-24 | cif/ Adding structures of 4088693, 4088694, 4088695, 4088696 via cif-deposit CGI script. |
4088695.cif |
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Users of the data should acknowledge the original authors of the
structural data.