Crystallography Open Database

Information card for entry 4088856

Preview

Coordinates	4088856.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C9 H18 Cl3 Ga O3 Os P2
Calculated formula	C9 H18 Cl3 Ga O3 Os P2
SMILES	[Os]([Ga](Cl)(Cl)Cl)(C#[O])([P](C)(C)C)(C#[O])([P](C)(C)C)C#[O]
Title of publication	Metal-Only Lewis Pairs Based on Zerovalent Osmium
Authors of publication	Bissert, Robin; Braunschweig, Holger; Dewhurst, Rian D.; Schneider, Christoph
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	15
Pages of publication	2567
a	8.983 ± 0.0012 Å
b	12.9064 ± 0.0019 Å
c	19.16 ± 0.003 Å
α	90°
β	97.911 ± 0.004°
γ	90°
Cell volume	2200.2 ± 0.6 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0188
Residual factor for significantly intense reflections	0.0171
Weighted residual factors for significantly intense reflections	0.0445
Weighted residual factors for all reflections included in the refinement	0.046
Goodness-of-fit parameter for all reflections included in the refinement	1.043
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
237858 (current)	2019-11-24	cif/ Adding structures of 4088852, 4088853, 4088854, 4088855, 4088856, 4088857, 4088858 via cif-deposit CGI script.	4088856.cif