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Information card for entry 4088859
Preview
| Coordinates | 4088859.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C14 H22 B N5 O4 |
|---|---|
| Calculated formula | C14 H22 B N5 O4 |
| Title of publication | Radical and Thermal Reactions of N-Heterocyclic Carbene Boranes with Diazo Compounds |
| Authors of publication | Allen, Thomas H.; Geib, Steven J.; Curran, Dennis P. |
| Journal of publication | Organometallics |
| Year of publication | 2016 |
| Journal volume | 35 |
| Journal issue | 17 |
| Pages of publication | 2975 |
| a | 12.044 ± 0.0005 Å |
| b | 9.0062 ± 0.0004 Å |
| c | 16.9281 ± 0.0007 Å |
| α | 90° |
| β | 102.976 ± 0.0017° |
| γ | 90° |
| Cell volume | 1789.31 ± 0.13 Å3 |
| Cell temperature | 230 ± 2 K |
| Ambient diffraction temperature | 230 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0485 |
| Residual factor for significantly intense reflections | 0.0467 |
| Weighted residual factors for significantly intense reflections | 0.1721 |
| Weighted residual factors for all reflections included in the refinement | 0.1762 |
| Goodness-of-fit parameter for all reflections included in the refinement | 2.305 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 237860 (current) | 2019-11-24 | cif/ Adding structures of 4088859, 4088860, 4088861 via cif-deposit CGI script. |
4088859.cif |
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Users of the data should acknowledge the original authors of the
structural data.