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Information card for entry 4088862
Preview
| Coordinates | 4088862.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C29.4 H33.5 I1.1 N Sn2 |
|---|---|
| Calculated formula | C29.4 H33.5 I1.1 N Sn2 |
| Title of publication | Unsymmetrical Bicentric Organotin Lewis Acids {Me2N(CH2)3}Ph(X)Sn(CH2)nSnPh2X (X = F, I; n = 1, 3): Syntheses and Structures |
| Authors of publication | Alashkar, Nour; Dietz, Christina; Baba Haj, Samer; Hiller, Wolf; Jurkschat, Klaus |
| Journal of publication | Organometallics |
| Year of publication | 2016 |
| Journal volume | 35 |
| Journal issue | 16 |
| Pages of publication | 2738 |
| a | 10.3926 ± 0.0004 Å |
| b | 11.7904 ± 0.0004 Å |
| c | 23.7767 ± 0.0008 Å |
| α | 90° |
| β | 99.43 ± 0.004° |
| γ | 90° |
| Cell volume | 2874.06 ± 0.18 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0478 |
| Residual factor for significantly intense reflections | 0.0291 |
| Weighted residual factors for significantly intense reflections | 0.0586 |
| Weighted residual factors for all reflections included in the refinement | 0.0614 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.833 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 237862 (current) | 2019-11-24 | cif/ Adding structures of 4088862, 4088863, 4088864, 4088865 via cif-deposit CGI script. |
4088862.cif |
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Users of the data should acknowledge the original authors of the
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