Crystallography Open Database

Information card for entry 4088865

Preview

Coordinates	4088865.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H33 F2 N Sn2
Calculated formula	C26 H33 F2 N Sn2
SMILES	[Sn]12([F][Sn](F)(CCC1)(c1ccccc1)c1ccccc1)([N](CCC2)(C)C)c1ccccc1
Title of publication	Unsymmetrical Bicentric Organotin Lewis Acids {Me2N(CH2)3}Ph(X)Sn(CH2)nSnPh2X (X = F, I; n = 1, 3): Syntheses and Structures
Authors of publication	Alashkar, Nour; Dietz, Christina; Baba Haj, Samer; Hiller, Wolf; Jurkschat, Klaus
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	16
Pages of publication	2738
a	16.8757 ± 0.0009 Å
b	7.9337 ± 0.0004 Å
c	18.9274 ± 0.0013 Å
α	90°
β	95.777 ± 0.006°
γ	90°
Cell volume	2521.3 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0678
Residual factor for significantly intense reflections	0.0318
Weighted residual factors for significantly intense reflections	0.0374
Weighted residual factors for all reflections included in the refinement	0.039
Goodness-of-fit parameter for all reflections included in the refinement	0.803
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
237862 (current)	2019-11-24	cif/ Adding structures of 4088862, 4088863, 4088864, 4088865 via cif-deposit CGI script.	4088865.cif