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Information card for entry 4088989
Preview
| Coordinates | 4088989.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C37 H39 Cl2 F12 Fe3 N3 S Sb2 |
|---|---|
| Calculated formula | C37 H39 Cl2 F12 Fe3 N3 S Sb2 |
| Title of publication | Generation and Oligomerization ofN-Ferrocenyl Ketenimines via Open-Shell Intermediates |
| Authors of publication | Kienz, Torben; Förster, Christoph; Heinze, Katja |
| Journal of publication | Organometallics |
| Year of publication | 2016 |
| Journal volume | 35 |
| Journal issue | 21 |
| Pages of publication | 3681 |
| a | 9.6219 ± 0.0008 Å |
| b | 13.1 ± 0.0011 Å |
| c | 17.2736 ± 0.0015 Å |
| α | 104.403 ± 0.002° |
| β | 92.447 ± 0.002° |
| γ | 96.711 ± 0.002° |
| Cell volume | 2088.6 ± 0.3 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1114 |
| Residual factor for significantly intense reflections | 0.0556 |
| Weighted residual factors for significantly intense reflections | 0.1172 |
| Weighted residual factors for all reflections included in the refinement | 0.1329 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.883 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 237915 (current) | 2019-11-24 | cif/ Adding structures of 4088989 via cif-deposit CGI script. |
4088989.cif |
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Users of the data should acknowledge the original authors of the
structural data.