Crystallography Open Database

Information card for entry 4089090

Preview

Coordinates	4089090.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H53 Ag3 Cl8 P4
Calculated formula	C65 H53 Ag3 Cl8 P4
Title of publication	Low-Nuclearity Alkynyl d10Clusters Supported by Chelating Multidentate Phosphines
Authors of publication	Belyaev, Andrey; Dau, Thuy Minh; Jänis, Janne; Grachova, Elena V.; Tunik, Sergey P.; Koshevoy, Igor O.
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	21
Pages of publication	3763
a	13.2568 ± 0.0012 Å
b	18.0465 ± 0.0016 Å
c	15.1861 ± 0.0013 Å
α	90°
β	115.132 ± 0.002°
γ	90°
Cell volume	3289.2 ± 0.5 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0613
Residual factor for significantly intense reflections	0.0586
Weighted residual factors for significantly intense reflections	0.1537
Weighted residual factors for all reflections included in the refinement	0.1556
Goodness-of-fit parameter for all reflections included in the refinement	1.101
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
237980 (current)	2019-11-24	cif/ Adding structures of 4089088, 4089089, 4089090, 4089091, 4089092, 4089093, 4089094, 4089095, 4089096, 4089097, 4089098, 4089099, 4089100, 4089101 via cif-deposit CGI script.	4089090.cif