Crystallography Open Database

Information card for entry 4089163

Preview

Coordinates	4089163.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41.5 H49 Br Cl7 N4 O Os P
Calculated formula	C41.5 H49 Br Cl7 N4 O Os P
Title of publication	Osmium(II) Complexes Containing a Dianionic CCCC-Donor Tetradentate Ligand
Authors of publication	Alabau, Roberto G.; Esteruelas, Miguel A.; Oliván, Montserrat; Oñate, Enrique; Palacios, Adrián U.; Tsai, Jui-Yi; Xia, Chuanjun
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	23
Pages of publication	3981
a	11.8972 ± 0.0008 Å
b	13.1287 ± 0.0008 Å
c	16.597 ± 0.0016 Å
α	102.145 ± 0.001°
β	94.266 ± 0.001°
γ	114.786 ± 0.001°
Cell volume	2261.9 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0416
Residual factor for significantly intense reflections	0.0337
Weighted residual factors for significantly intense reflections	0.0839
Weighted residual factors for all reflections included in the refinement	0.0882
Goodness-of-fit parameter for all reflections included in the refinement	0.88
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
238011 (current)	2019-11-24	cif/ Adding structures of 4089163, 4089164, 4089165, 4089166, 4089167, 4089168 via cif-deposit CGI script.	4089163.cif