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Information card for entry 4089175
Preview
| Coordinates | 4089175.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C42 H44 Cl5 O P3 Ru Si |
|---|---|
| Calculated formula | C42 H44 Cl5 O P3 Ru Si |
| Title of publication | Hydrochlorination of Ruthenaphosphaalkenyls: Unexpectedly Facile Access to Alkylchlorohydrophosphane Complexes |
| Authors of publication | Greenacre, Victoria K.; Day, Iain J.; Crossley, Ian R. |
| Journal of publication | Organometallics |
| Year of publication | 2017 |
| Journal volume | 36 |
| Journal issue | 2 |
| Pages of publication | 435 |
| a | 12.5318 ± 0.0008 Å |
| b | 13.0932 ± 0.0011 Å |
| c | 15.9653 ± 0.001 Å |
| α | 99.39 ± 0.006° |
| β | 101.138 ± 0.005° |
| γ | 116.048 ± 0.007° |
| Cell volume | 2215.9 ± 0.3 Å3 |
| Cell temperature | 173 K |
| Ambient diffraction temperature | 173 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1022 |
| Residual factor for significantly intense reflections | 0.0754 |
| Weighted residual factors for significantly intense reflections | 0.1955 |
| Weighted residual factors for all reflections included in the refinement | 0.2295 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.034 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 238018 (current) | 2019-11-24 | cif/ Adding structures of 4089175 via cif-deposit CGI script. |
4089175.cif |
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Users of the data should acknowledge the original authors of the
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