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Information card for entry 4089298
Preview
| Coordinates | 4089298.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C34 H61 N3 O2 Os P2 |
|---|---|
| Calculated formula | C34 H61 N3 O2 Os P2 |
| Title of publication | Preparation of Phosphorescent Osmium(IV) Complexes with N,N′,C- and C,N,C′-Pincer Ligands |
| Authors of publication | Alabau, Roberto G.; Esteruelas, Miguel A.; Oliván, Montserrat; Oñate, Enrique |
| Journal of publication | Organometallics |
| Year of publication | 2017 |
| Journal volume | 36 |
| Journal issue | 9 |
| Pages of publication | 1848 |
| a | 16.9732 ± 0.0008 Å |
| b | 13.4054 ± 0.0006 Å |
| c | 16.3797 ± 0.0008 Å |
| α | 90° |
| β | 98.278 ± 0.001° |
| γ | 90° |
| Cell volume | 3688.1 ± 0.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0367 |
| Residual factor for significantly intense reflections | 0.0271 |
| Weighted residual factors for significantly intense reflections | 0.0498 |
| Weighted residual factors for all reflections included in the refinement | 0.0539 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.092 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 238097 (current) | 2019-11-24 | cif/ Adding structures of 4089298, 4089299, 4089300 via cif-deposit CGI script. |
4089298.cif |
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Users of the data should acknowledge the original authors of the
structural data.