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Information card for entry 4089332
Preview
| Coordinates | 4089332.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C39 H43 I O3 P2 Pd |
|---|---|
| Calculated formula | C39 H43 I O3 P2 Pd |
| Title of publication | Palladacycles with a Metal-Bonded sp3-Hybridized Carbon as Intermediates in the Synthesis of 2,2,3,4-Tetrasubstituted 2H-1-Benzopyrans and 1,2-Dihydroquinolines. Effects of Auxiliary Ligands and Substitution at a Palladium-Bonded Tertiary Carbon |
| Authors of publication | Lu, Genliang; Portscheller, Janelle L.; Malinakova, Helena C. |
| Journal of publication | Organometallics |
| Year of publication | 2005 |
| Journal volume | 24 |
| Journal issue | 5 |
| Pages of publication | 945 |
| a | 10.138 ± 0.004 Å |
| b | 13.78 ± 0.005 Å |
| c | 27.372 ± 0.01 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 3824 ± 2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0339 |
| Residual factor for significantly intense reflections | 0.0333 |
| Weighted residual factors for significantly intense reflections | 0.088 |
| Weighted residual factors for all reflections included in the refinement | 0.0884 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.016 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 243612 (current) | 2019-11-26 | cif/ Adding structures of 4089329, 4089330, 4089331, 4089332, 4089333, 4089334 via cif-deposit CGI script. |
4089332.cif |
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Users of the data should acknowledge the original authors of the
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