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Information card for entry 4089654
Preview
| Coordinates | 4089654.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C66 H59 B F24 N6 O7 Rh |
|---|---|
| Calculated formula | C66 H59 B F24 N6 O7 Rh |
| Title of publication | Rhodium(I) Complexes of the Conformationally Rigid IBioxMe4 Ligand: Isolation of a Stable Low-Coordinate T-Shaped Complex |
| Authors of publication | Chaplin, Adrian B. |
| Journal of publication | Organometallics |
| Year of publication | 2014 |
| Journal volume | 33 |
| Journal issue | 3 |
| Pages of publication | 624 |
| a | 13.1514 ± 0.0004 Å |
| b | 13.475 ± 0.0004 Å |
| c | 21.9169 ± 0.0007 Å |
| α | 105.287 ± 0.003° |
| β | 101.319 ± 0.003° |
| γ | 93.354 ± 0.002° |
| Cell volume | 3648.7 ± 0.2 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0854 |
| Residual factor for significantly intense reflections | 0.0639 |
| Weighted residual factors for significantly intense reflections | 0.143 |
| Weighted residual factors for all reflections included in the refinement | 0.1537 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.058 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 243714 (current) | 2019-11-26 | cif/ Adding structures of 4089653, 4089654 via cif-deposit CGI script. |
4089654.cif |
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Users of the data should acknowledge the original authors of the
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