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Information card for entry 4089657
Preview
| Coordinates | 4089657.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C33 H49 Cl N4 O4 Rh |
|---|---|
| Calculated formula | C33 H49 Cl N4 O4 Rh |
| Title of publication | Rhodium(I) Complexes of the Conformationally Rigid IBioxMe4 Ligand: Preparation of Mono-, Bis-, and Tris-ligated NHC Complexes |
| Authors of publication | Chaplin, Adrian B. |
| Journal of publication | Organometallics |
| Year of publication | 2014 |
| Journal volume | 33 |
| Journal issue | 12 |
| Pages of publication | 3069 |
| a | 10.60751 ± 0.00016 Å |
| b | 16.42 ± 0.0003 Å |
| c | 20.2981 ± 0.0004 Å |
| α | 70.9975 ± 0.0015° |
| β | 79.908 ± 0.0014° |
| γ | 84.7055 ± 0.0013° |
| Cell volume | 3288.69 ± 0.11 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0419 |
| Residual factor for significantly intense reflections | 0.0335 |
| Weighted residual factors for significantly intense reflections | 0.0781 |
| Weighted residual factors for all reflections included in the refinement | 0.0826 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.037 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 243716 (current) | 2019-11-26 | cif/ Adding structures of 4089657, 4089658, 4089659, 4089660, 4089661, 4089662, 4089663, 4089664, 4089665, 4089666 via cif-deposit CGI script. |
4089657.cif |
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Users of the data should acknowledge the original authors of the
structural data.