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Information card for entry 4089694
Preview
| Coordinates | 4089694.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C49 H111 Ce Cl2 O16 Si4 |
|---|---|
| Calculated formula | C49 H111 Ce Cl2 O16 Si4 |
| Title of publication | Synthesis and Characterization of Rare Earth Siloxide Complexes, M[OSi(OtBu)3]3(L)x where L is HOSi(OtBu)3 and x = 0 or 1 |
| Authors of publication | Lapadula, Giuseppe; Conley, Matthew P.; Copéret, Christophe; Andersen, Richard A. |
| Journal of publication | Organometallics |
| Year of publication | 2014 |
| Journal volume | 34 |
| Journal issue | 11 |
| Pages of publication | 2271 |
| a | 13.684 ± 0.002 Å |
| b | 13.866 ± 0.002 Å |
| c | 21.622 ± 0.003 Å |
| α | 75.471 ± 0.002° |
| β | 81.717 ± 0.002° |
| γ | 60.894 ± 0.002° |
| Cell volume | 3468.7 ± 0.9 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0837 |
| Residual factor for significantly intense reflections | 0.0737 |
| Weighted residual factors for significantly intense reflections | 0.1871 |
| Weighted residual factors for all reflections included in the refinement | 0.1916 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.203 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 243723 (current) | 2019-11-26 | cif/ Adding structures of 4089694, 4089695, 4089696, 4089697, 4089698, 4089699, 4089700, 4089701, 4089702, 4089703 via cif-deposit CGI script. |
4089694.cif |
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Users of the data should acknowledge the original authors of the
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