Crystallography Open Database

Information card for entry 4089696

Preview

Coordinates	4089696.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C288 H648 La8 O96 Si24
Calculated formula	C288 H648 La8 O96 Si24
Title of publication	Synthesis and Characterization of Rare Earth Siloxide Complexes, M[OSi(OtBu)3]3(L)x where L is HOSi(OtBu)3 and x = 0 or 1
Authors of publication	Lapadula, Giuseppe; Conley, Matthew P.; Copéret, Christophe; Andersen, Richard A.
Journal of publication	Organometallics
Year of publication	2014
Journal volume	34
Journal issue	11
Pages of publication	2271
a	25.912 ± 0.004 Å
b	14.118 ± 0.002 Å
c	27.368 ± 0.005 Å
α	90°
β	97.791 ± 0.003°
γ	90°
Cell volume	9919 ± 3 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1123
Residual factor for significantly intense reflections	0.0727
Weighted residual factors for significantly intense reflections	0.1602
Weighted residual factors for all reflections included in the refinement	0.1729
Goodness-of-fit parameter for all reflections included in the refinement	1.164
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
243723 (current)	2019-11-26	cif/ Adding structures of 4089694, 4089695, 4089696, 4089697, 4089698, 4089699, 4089700, 4089701, 4089702, 4089703 via cif-deposit CGI script.	4089696.cif