Crystallography Open Database

Information card for entry 4102229

Preview

Coordinates	4102229.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H32 N3 Pt
Calculated formula	C25 H32 N3 Pt
Title of publication	Net Hydrogenation of Pt-NHPh Bond Is Catalyzed by Elemental Pt
Authors of publication	Joanna R. Webb; Aaron W. Pierpont; Colleen Munro-Leighton; T. Brent Gunnoe; Thomas R. Cundari; Paul D. Boyle
Journal of publication	Journal of the American Chemical Society
Year of publication	2010
Journal volume	132
Pages of publication	4520 - 4521
a	9.323 ± 0.0004 Å
b	11.6735 ± 0.0005 Å
c	11.7514 ± 0.0005 Å
α	87.448 ± 0.002°
β	73.626 ± 0.002°
γ	67.519 ± 0.002°
Cell volume	1130.92 ± 0.09 Å³
Cell temperature	110 K
Ambient diffraction temperature	110 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.043
Residual factor for significantly intense reflections	0.0316
Weighted residual factors for significantly intense reflections	0.0605
Weighted residual factors for all reflections included in the refinement	0.0647
Goodness-of-fit parameter for all reflections included in the refinement	1.001
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178768 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/22.	4102229.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4102229.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4102229.cif
25086	2011-09-09	../uploads/cif-deposit/cod/cif Adding structures of 4102229 via cif-deposit CGI script.	4102229.cif