Crystallography Open Database

Information card for entry 4102512

Preview

Coordinates	4102512.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H43 B N4 O3 Si2 Zn
Calculated formula	C25 H43 B N4 O3 Si2 Zn
Title of publication	Conversion of a Zinc Disilazide to a Zinc Hydride Mediated by LiCl
Authors of publication	Debabrata Mukherjee; Arkady Ellern; Aaron D. Sadow
Journal of publication	Journal of the American Chemical Society
Year of publication	2010
Journal volume	132
Pages of publication	7582 - 7583
a	9.8932 ± 0.0018 Å
b	10.985 ± 0.002 Å
c	15.147 ± 0.003 Å
α	76.651 ± 0.003°
β	75.037 ± 0.003°
γ	81.611 ± 0.003°
Cell volume	1540.8 ± 0.5 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0928
Residual factor for significantly intense reflections	0.0638
Weighted residual factors for significantly intense reflections	0.1439
Weighted residual factors for all reflections included in the refinement	0.1565
Goodness-of-fit parameter for all reflections included in the refinement	1.065
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178771 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/25.	4102512.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4102512.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4102512.cif
25393	2011-09-11	../uploads/cif-deposit/cod/cif Adding structures of 4102512 via cif-deposit CGI script.	4102512.cif