Crystallography Open Database

Information card for entry 4102775

Preview

Coordinates	4102775.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H33 O2 Si2
Calculated formula	C40 H33 O2 Si2
Title of publication	Palladium-Catalyzed Dimerization of Vinyl Ethers to Acetals
Authors of publication	Changle Chen; Richard F. Jordan
Journal of publication	Journal of the American Chemical Society
Year of publication	2010
Journal volume	132
Pages of publication	10254 - 10255
a	9.306 ± 0.004 Å
b	18.733 ± 0.008 Å
c	19.586 ± 0.008 Å
α	90°
β	98.302 ± 0.007°
γ	90°
Cell volume	3379 ± 2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.06
Residual factor for significantly intense reflections	0.051
Weighted residual factors for significantly intense reflections	0.1381
Weighted residual factors for all reflections included in the refinement	0.1442
Goodness-of-fit parameter for all reflections included in the refinement	1.065
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178773 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/27.	4102775.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4102775.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4102775.cif
25692	2011-09-13	../uploads/cif-deposit/cod/cif Adding structures of 4102775 via cif-deposit CGI script.	4102775.cif