Crystallography Open Database

Information card for entry 4103193

Preview

Coordinates	4103193.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	tr040
Chemical name	(Acetato){10-benzo[<i>h</i>]quinolinato)chloropalladium(III) Dimer . Iodobenzene . Dichloromethane Solvate
Formula	C37 H29 Cl4 I N2 O4 Pd2
Calculated formula	C36 H27 Cl2 I N2 O4 Pd2
Title of publication	Bimetallic Reductive Elimination from Dinuclear Pd(III) Complexes
Authors of publication	David C. Powers; Diego Benitez; Ekaterina Tkatchouk; William A. Goddard; Tobias Ritter
Journal of publication	Journal of the American Chemical Society
Year of publication	2010
Journal volume	132
Pages of publication	14092 - 14103
a	16.7605 ± 0.0005 Å
b	17.7508 ± 0.0005 Å
c	14.1762 ± 0.0004 Å
α	90°
β	117.053 ± 0.002°
γ	90°
Cell volume	3756.1 ± 0.2 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0491
Residual factor for significantly intense reflections	0.0336
Weighted residual factors for significantly intense reflections	0.0761
Weighted residual factors for all reflections included in the refinement	0.0804
Goodness-of-fit parameter for all reflections included in the refinement	1.075
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178777 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/31.	4103193.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4103193.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4103193.cif
26151	2011-09-19	../uploads/cif-deposit/cod/cif Adding structures of 4103193 via cif-deposit CGI script.	4103193.cif