Crystallography Open Database

Information card for entry 4104930

Preview

Coordinates	4104930.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H38 N O2 P Pd
Calculated formula	C28 H38 N O2 P Pd
Title of publication	Influence of Biaryl Phosphine Structure on C-N and C-C Bond Formation
Authors of publication	Ramendra Pratap; Damon Parrish; Padmaja Gunda; D. Venkataraman; Mahesh K. Lakshman
Journal of publication	Journal of the American Chemical Society
Year of publication	2009
Journal volume	131
Pages of publication	12240 - 12249
a	14.4432 ± 0.0004 Å
b	17.5999 ± 0.0005 Å
c	21.5142 ± 0.0006 Å
α	90°
β	106.756 ± 0.001°
γ	90°
Cell volume	5236.7 ± 0.3 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0248
Residual factor for significantly intense reflections	0.0238
Weighted residual factors for significantly intense reflections	0.0651
Weighted residual factors for all reflections included in the refinement	0.0659
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178795 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/49.	4104930.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4104930.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4104930.cif
30047	2011-11-09	../uploads/cif-deposit/cod/cif Adding structures of 4104930 via cif-deposit CGI script.	4104930.cif