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Information card for entry 4105132
Preview
| Coordinates | 4105132.cif |
|---|---|
| Original paper (by DOI) | HTML |
| External links | PubChem |
| Formula | C78 H84 O6 Si3 |
|---|---|
| Calculated formula | C78 H84 O6 Si3 |
| Title of publication | Development of a Sila-Friedel-Crafts Reaction and Its Application to the Synthesis of Dibenzosilole Derivatives |
| Authors of publication | Shunsuke Furukawa; Junji Kobayashi; Takayuki Kawashima |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2009 |
| Journal volume | 131 |
| Pages of publication | 14192 - 14193 |
| a | 27.695 ± 0.008 Å |
| b | 15.054 ± 0.005 Å |
| c | 32.739 ± 0.011 Å |
| α | 90 ± 0.0014° |
| β | 102.696 ± 0.0016° |
| γ | 90 ± 0.0014° |
| Cell volume | 13316 ± 7 Å3 |
| Cell temperature | 120 ± 2 K |
| Ambient diffraction temperature | 120 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/a 1 |
| Hall space group symbol | -P 2yab |
| Residual factor for all reflections | 0.1961 |
| Residual factor for significantly intense reflections | 0.1489 |
| Weighted residual factors for significantly intense reflections | 0.3862 |
| Weighted residual factors for all reflections included in the refinement | 0.4551 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.58 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301832 (current) | 2025-08-20 | Add cross-references to PubChem compounds in COD range 4/10/ Each referenced PubChem compound corresponds to the full crystal structure. |
4105132.cif |
| 178797 | 2016-03-21 | cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/51. |
4105132.cif |
| 120076 | 2014-07-11 | Adding DOIs to range 4/10 structures. | 4105132.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4105132.cif |
| 30324 | 2011-11-11 | ../uploads/cif-deposit/cod/cif Adding structures of 4105132 via cif-deposit CGI script. |
4105132.cif |
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Users of the data should acknowledge the original authors of the
structural data.