Crystallography Open Database

Information card for entry 4105261

Preview

Coordinates	4105261.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C72 H132 Cl Ge12 N6 O91 Pr11
Calculated formula	C72 Cl0.99 Ge12 N6 O74 Pr11
Title of publication	Lanthanide Germanate Cluster Organic Frameworks Constructed from {Ln8Ge12} or {Ln11Ge12} Cage Cluster Building Blocks
Authors of publication	Huan He; Gao-Juan Cao; Shou-Tian Zheng; Guo-Yu Yang
Journal of publication	Journal of the American Chemical Society
Year of publication	2009
Journal volume	131
Pages of publication	15588 - 15589
a	32.2786 ± 0.0011 Å
b	32.2786 ± 0.0011 Å
c	32.2786 ± 0.0011 Å
α	90°
β	90°
γ	90°
Cell volume	33631 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	217
Hermann-Mauguin space group symbol	I -4 3 m
Hall space group symbol	I -4 2 3
Residual factor for all reflections	0.0568
Residual factor for significantly intense reflections	0.056
Weighted residual factors for significantly intense reflections	0.1504
Weighted residual factors for all reflections included in the refinement	0.1509
Goodness-of-fit parameter for all reflections included in the refinement	1.096
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178798 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/52.	4105261.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4105261.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4105261.cif
30455	2011-11-12	../uploads/cif-deposit/cod/cif Adding structures of 4105261 via cif-deposit CGI script.	4105261.cif