Crystallography Open Database

Information card for entry 4105539

Preview

Coordinates	4105539.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	catena-(di(hexafluoroacetylacetonate)-iron(II)- di(hexafluoroacetylacetonate)-lead(II))
Formula	C20 H4 F24 Fe O8 Pb
Calculated formula	C20 H4 F24 Fe O8 Pb
Title of publication	Fluorinated Heterometallic β-Diketonates as Volatile Single-Source Precursors for the Synthesis of Low-Valent Mixed-Metal Fluorides
Authors of publication	Anantharamulu Navulla; Alexander A. Tsirlin; Artem M. Abakumov; Roman V. Shpanchenko; Haitao Zhang; Evgeny V. Dikarev
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	692 - 694
a	11.4406 ± 0.0006 Å
b	12.3702 ± 0.0007 Å
c	13.582 ± 0.0008 Å
α	65.896 ± 0.001°
β	66.64 ± 0.001°
γ	64.316 ± 0.001°
Cell volume	1523.87 ± 0.15 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0418
Residual factor for significantly intense reflections	0.0384
Weighted residual factors for significantly intense reflections	0.0964
Weighted residual factors for all reflections included in the refinement	0.0991
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178801 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/55.	4105539.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4105539.cif
52298	2012-04-10	../uploads/cif-deposit/cod/cif Adding structures of 4105539 via cif-deposit CGI script.	4105539.cif