Crystallography Open Database

Information card for entry 4106441

Preview

Coordinates	4106441.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H32 As8 Cl5 O62 V16
Calculated formula	C48 H32 As8 Cl5 O62 V16
Title of publication	From Platonic Templates to Archimedean Solids: Successive Construction of Nanoscopic {V16As8}, {V16As10}, {V20As8}, and {V24As8} Polyoxovanadate Cages
Authors of publication	Lei Zhang; Wolfgang Schmitt
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	11240 - 11248
a	22.342 ± 0.003 Å
b	22.342 ± 0.003 Å
c	14.023 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	7000 ± 2 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	6
Space group number	87
Hermann-Mauguin space group symbol	I 4/m
Hall space group symbol	-I 4
Residual factor for all reflections	0.1052
Residual factor for significantly intense reflections	0.0818
Weighted residual factors for significantly intense reflections	0.2178
Weighted residual factors for all reflections included in the refinement	0.2353
Goodness-of-fit parameter for all reflections included in the refinement	0.985
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178810 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/64.	4106441.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4106441.cif
53241	2012-04-18	cif/ Adding structures of 4106441 via cif-deposit CGI script.	4106441.cif