#------------------------------------------------------------------------------ #$Date: 2013-12-29 13:49:26 +0200 (Sun, 29 Dec 2013) $ #$Revision: 91935 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/10/71/4107188.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4107188 loop_ _publ_author_name 'Saskia Stegmaier' 'Thomas F. F\"assler' _publ_contact_author_address ;Department Chemie Technische Universit\"at M\"unchen Lichtenbergstr. 4 85747 Garching Germany ; _publ_contact_author_email thomas.faessler@lrz.tu-muenchen.de _publ_contact_author_fax '+49 89 28913186' _publ_contact_author_name 'Prof. Dr. Thomas F. F\"assler' _publ_contact_author_phone '+49 89 28913134' _publ_section_title ; A Bronze Matryoshka: The Discrete Intermetalloid Cluster [Sn@Cu12@Sn20]^12-^ in the Ternary Phases A~12~Cu~12~Sn~21~ (A = Na, K) ; _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 19758 _journal_page_last 19768 _journal_volume 133 _journal_year 2011 _chemical_formula_sum 'Cu12 Na12 Sn21' _chemical_formula_weight 3530.85 _space_group_IT_number 224 _symmetry_cell_setting cubic _symmetry_Int_Tables_number 224 _symmetry_space_group_name_Hall '-P 4bc 2bc 3' _symmetry_space_group_name_H-M 'P n -3 m :2' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method 'manual editing of SHELXL-97 cif-file' _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_formula_units_Z 4 _cell_length_a 16.6253(3) _cell_length_b 16.6253(3) _cell_length_c 16.6253(3) _cell_measurement_reflns_used 102593 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 27.2 _cell_measurement_theta_min 3.7 _cell_volume 4595.24(14) _computing_cell_refinement 'STOE X-AREA (STOE, 2004)' _computing_data_collection 'STOE X-AREA (STOE, 2004)' _computing_data_reduction 'STOE X-AREA, STOE X-RED (STOE, 2004)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.987 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measurement_device_type 'STOE IPDS 2T imaging plate diffractomter' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0411 _diffrn_reflns_av_sigmaI/netI 0.0097 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 34966 _diffrn_reflns_theta_full 26.83 _diffrn_reflns_theta_max 26.83 _diffrn_reflns_theta_min 3.68 _diffrn_source 'rotating anode' _diffrn_source_type 'BRUKER NONIUS FR591' _exptl_absorpt_coefficient_mu 16.701 _exptl_absorpt_correction_T_max 0.1872 _exptl_absorpt_correction_T_min 0.0768 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details 'STOE X-RED (crystal shape optimized with STOE X-SHAPE)' _exptl_crystal_colour 'lustrous black/silver' _exptl_crystal_density_diffrn 5.104 _exptl_crystal_description 'block shaped' _exptl_crystal_F_000 6120 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.10 _exptl_crystal_size_min 0.10 _refine_diff_density_max 1.015 _refine_diff_density_min -1.877 _refine_diff_density_rms 0.218 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.643 _refine_ls_matrix_type full _refine_ls_number_parameters 50 _refine_ls_number_reflns 945 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.643 _refine_ls_R_factor_all 0.0356 _refine_ls_R_factor_gt 0.0354 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0053P)^2^+89.1539P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0716 _refine_ls_wR_factor_ref 0.0716 _reflns_number_gt 943 _reflns_number_total 945 _reflns_threshold_expression >2sigma(I) _[local]_cod_data_source_file ja205934p_si_003.cif _[local]_cod_data_source_block Na12Cu12Sn21 _[local]_cod_cif_authors_sg_H-M 'P n -3 m' _cod_database_code 4107188 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-x+1/2, y, -z+1/2' 'x, -y+1/2, -z+1/2' 'z, x, y' 'z, -x+1/2, -y+1/2' '-z+1/2, -x+1/2, y' '-z+1/2, x, -y+1/2' 'y, z, x' '-y+1/2, z, -x+1/2' 'y, -z+1/2, -x+1/2' '-y+1/2, -z+1/2, x' 'y+1/2, x+1/2, -z' '-y, -x, -z' 'y+1/2, -x, z+1/2' '-y, x+1/2, z+1/2' 'x+1/2, z+1/2, -y' '-x, z+1/2, y+1/2' '-x, -z, -y' 'x+1/2, -z, y+1/2' 'z+1/2, y+1/2, -x' 'z+1/2, -y, x+1/2' '-z, y+1/2, x+1/2' '-z, -y, -x' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'x-1/2, -y, z-1/2' '-x, y-1/2, z-1/2' '-z, -x, -y' '-z, x-1/2, y-1/2' 'z-1/2, x-1/2, -y' 'z-1/2, -x, y-1/2' '-y, -z, -x' 'y-1/2, -z, x-1/2' '-y, z-1/2, x-1/2' 'y-1/2, z-1/2, -x' '-y-1/2, -x-1/2, z' 'y, x, z' '-y-1/2, x, -z-1/2' 'y, -x-1/2, -z-1/2' '-x-1/2, -z-1/2, y' 'x, -z-1/2, -y-1/2' 'x, z, y' '-x-1/2, z, -y-1/2' '-z-1/2, -y-1/2, x' '-z-1/2, y, -x-1/2' 'z, -y-1/2, -x-1/2' 'z, y, x' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags Sn1 Sn 0.07718(4) 0.28989(4) 0.63648(4) 0.01912(17) Uani 1 1 d . Sn2 Sn 0.03901(4) 0.03901(4) 0.25625(5) 0.0197(2) Uani 1 2 d S Sn3 Sn 0.14818(5) 0.14818(5) 0.14818(5) 0.0177(3) Uani 1 6 d S Sn4 Sn 0.0000 0.0000 0.0000 0.0126(4) Uani 1 12 d S Cu1 Cu 0.54668(6) 0.54668(6) 0.14384(9) 0.0166(3) Uani 1 2 d S Cu2 Cu 0.61177(6) 0.61177(6) 0.00697(9) 0.0160(3) Uani 1 2 d S Na1 Na 0.1023(3) 0.1023(3) 0.6807(4) 0.0425(16) Uani 1 2 d S Na2 Na 0.5200(6) 0.2500 0.2500 0.042(2) Uani 1 4 d S Na3 Na 0.3419(4) 0.3419(4) 0.3419(4) 0.029(4) Uani 0.91(4) 6 d SP Na4 Na 0.2500 0.7500 0.7500 0.037(4) Uani 0.96(4) 8 d SP loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sn1 0.0214(3) 0.0158(3) 0.0202(3) 0.0037(2) -0.0007(2) 0.0040(2) Sn2 0.0224(3) 0.0224(3) 0.0143(4) -0.0019(2) -0.0019(2) -0.0032(3) Sn3 0.0177(3) 0.0177(3) 0.0177(3) -0.0036(3) -0.0036(3) -0.0036(3) Sn4 0.0126(4) 0.0126(4) 0.0126(4) -0.0009(4) -0.0009(4) -0.0009(4) Cu1 0.0172(4) 0.0172(4) 0.0155(7) 0.0007(4) 0.0007(4) -0.0019(6) Cu2 0.0159(4) 0.0159(4) 0.0162(7) 0.0003(4) 0.0003(4) -0.0012(5) Na1 0.037(2) 0.037(2) 0.053(4) 0.011(2) 0.011(2) 0.004(3) Na2 0.044(6) 0.041(3) 0.041(3) 0.020(4) 0.000 0.000 Na3 0.029(4) 0.029(4) 0.029(4) 0.012(3) 0.012(3) 0.012(3) Na4 0.033(8) 0.039(6) 0.039(6) 0.000 0.000 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 Cu2 Sn1 Cu1 59.45(4) 27_566 27_566 Cu2 Sn1 Cu1 59.99(4) 27_566 12 Cu1 Sn1 Cu1 59.82(5) 27_566 12 Cu2 Sn1 Sn2 56.83(3) 27_566 11 Cu1 Sn1 Sn2 104.39(4) 27_566 11 Cu1 Sn1 Sn2 55.68(3) 12 11 Cu2 Sn1 Sn1 104.28(3) 27_566 19_566 Cu1 Sn1 Sn1 56.09(2) 27_566 19_566 Cu1 Sn1 Sn1 55.94(3) 12 19_566 Sn2 Sn1 Sn1 107.58(3) 11 19_566 Cu2 Sn1 Sn1 55.57(2) 27_566 37_665 Cu1 Sn1 Sn1 55.61(2) 27_566 37_665 Cu1 Sn1 Sn1 104.14(3) 12 37_665 Sn2 Sn1 Sn1 108.76(2) 11 37_665 Sn1 Sn1 Sn1 107.852(19) 19_566 37_665 Cu2 Sn1 Na1 136.16(12) 27_566 . Cu1 Sn1 Na1 164.03(13) 27_566 . Cu1 Sn1 Na1 127.03(13) 12 . Sn2 Sn1 Na1 90.11(14) 11 . Sn1 Sn1 Na1 113.51(9) 19_566 . Sn1 Sn1 Na1 126.23(10) 37_665 . Cu2 Sn1 Na4 111.18(3) 27_566 33_666 Cu1 Sn1 Na4 108.21(3) 27_566 33_666 Cu1 Sn1 Na4 167.25(4) 12 33_666 Sn2 Sn1 Na4 129.20(2) 11 33_666 Sn1 Sn1 Na4 122.82(2) 19_566 33_666 Sn1 Sn1 Na4 63.490(10) 37_665 33_666 Na1 Sn1 Na4 65.69(12) . 33_666 Cu2 Sn1 Na2 60.93(10) 27_566 9 Cu1 Sn1 Na2 110.99(4) 27_566 9 Cu1 Sn1 Na2 112.59(13) 12 9 Sn2 Sn1 Na2 66.51(12) 11 9 Sn1 Sn1 Na2 165.15(8) 19_566 9 Sn1 Sn1 Na2 63.70(4) 37_665 9 Na1 Sn1 Na2 80.69(11) . 9 Na4 Sn1 Na2 65.91(13) 33_666 9 Cu2 Sn1 Na1 110.72(8) 27_566 35_556 Cu1 Sn1 Na1 110.87(12) 27_566 35_556 Cu1 Sn1 Na1 59.40(9) 12 35_556 Sn2 Sn1 Na1 63.05(9) 11 35_556 Sn1 Sn1 Na1 64.36(12) 19_566 35_556 Sn1 Sn1 Na1 163.53(9) 37_665 35_556 Na1 Sn1 Na1 69.55(18) . 35_556 Na4 Sn1 Na1 132.96(9) 33_666 35_556 Na2 Sn1 Na1 120.15(14) 9 35_556 Cu2 Sn1 Na1 110.09(7) 27_566 4_556 Cu1 Sn1 Na1 59.22(10) 27_566 4_556 Cu1 Sn1 Na1 110.34(11) 12 4_556 Sn2 Sn1 Na1 163.60(10) 11 4_556 Sn1 Sn1 Na1 63.88(9) 19_566 4_556 Sn1 Sn1 Na1 63.91(5) 37_665 4_556 Na1 Sn1 Na1 106.08(14) . 4_556 Na4 Sn1 Na1 62.48(10) 33_666 4_556 Na2 Sn1 Na1 117.94(13) 9 4_556 Na1 Sn1 Na1 119.68(5) 35_556 4_556 Cu2 Sn1 Sn1 158.59(3) 27_566 4_556 Cu1 Sn1 Sn1 106.49(4) 27_566 4_556 Cu1 Sn1 Sn1 129.79(3) 12 4_556 Sn2 Sn1 Sn1 144.13(3) 11 4_556 Sn1 Sn1 Sn1 75.995(16) 19_566 4_556 Sn1 Sn1 Sn1 103.557(12) 37_665 4_556 Na1 Sn1 Sn1 57.68(13) . 4_556 Na4 Sn1 Sn1 55.152(10) 33_666 4_556 Na2 Sn1 Sn1 117.10(12) 9 4_556 Na1 Sn1 Sn1 88.94(8) 35_556 4_556 Na1 Sn1 Sn1 50.22(8) 4_556 4_556 Cu2 Sn1 Sn4 35.08(3) 27_566 4 Cu1 Sn1 Sn4 35.12(3) 27_566 4 Cu1 Sn1 Sn4 35.15(3) 12 4 Sn2 Sn1 Sn4 69.278(19) 11 4 Sn1 Sn1 Sn4 69.199(8) 19_566 4 Sn1 Sn1 Sn4 68.989(8) 37_665 4 Na1 Sn1 Sn4 158.45(13) . 4 Na4 Sn1 Sn4 132.381(16) 33_666 4 Na2 Sn1 Sn4 96.01(9) 9 4 Na1 Sn1 Sn4 94.54(9) 35_556 4 Na1 Sn1 Sn4 94.34(9) 4_556 4 Sn1 Sn1 Sn4 139.19(2) 4_556 4 Cu2 Sn1 Sn1 155.54(3) 27_566 18_545 Cu1 Sn1 Sn1 115.73(3) 27_566 18_545 Cu1 Sn1 Sn1 96.24(4) 12 18_545 Sn2 Sn1 Sn1 106.41(2) 11 18_545 Sn1 Sn1 Sn1 61.277(18) 19_566 18_545 Sn1 Sn1 Sn1 144.820(8) 37_665 18_545 Na1 Sn1 Sn1 52.25(9) . 18_545 Na4 Sn1 Sn1 93.211(18) 33_666 18_545 Na2 Sn1 Sn1 132.85(5) 9 18_545 Na1 Sn1 Sn1 46.22(8) 35_556 18_545 Na1 Sn1 Sn1 82.30(6) 4_556 18_545 Sn1 Sn1 Sn1 42.729(16) 4_556 18_545 Sn4 Sn1 Sn1 126.23(2) 4 18_545 Cu2 Sn1 Cu2 68.94(5) 27_566 12 Cu1 Sn1 Cu2 33.21(2) 27_566 12 Cu1 Sn1 Cu2 32.69(3) 12 12 Sn2 Sn1 Cu2 87.59(2) 11 12 Sn1 Sn1 Cu2 35.341(19) 19_566 12 Sn1 Sn1 Cu2 87.936(17) 37_665 12 Na1 Sn1 Cu2 144.27(9) . 12 Na4 Sn1 Cu2 137.963(19) 33_666 12 Na2 Sn1 Cu2 129.86(9) 9 12 Na1 Sn1 Cu2 77.74(11) 35_556 12 Na1 Sn1 Cu2 77.75(11) 4_556 12 Sn1 Sn1 Cu2 108.99(2) 4_556 12 Sn4 Sn1 Cu2 33.859(18) 4 12 Sn1 Sn1 Cu2 94.48(2) 18_545 12 Cu2 Sn1 Cu2 33.28(4) 27_566 29_566 Cu1 Sn1 Cu2 68.85(4) 27_566 29_566 Cu1 Sn1 Cu2 32.80(4) 12 29_566 Sn2 Sn1 Cu2 35.55(2) 11 29_566 Sn1 Sn1 Cu2 87.86(2) 19_566 29_566 Sn1 Sn1 Cu2 87.946(18) 37_665 29_566 Na1 Sn1 Cu2 125.43(14) . 29_566 Na4 Sn1 Cu2 142.30(2) 33_666 29_566 Na2 Sn1 Cu2 79.87(13) 9 29_566 Na1 Sn1 Cu2 77.55(8) 35_556 29_566 Na1 Sn1 Cu2 128.07(10) 4_556 29_566 Sn1 Sn1 Cu2 162.37(2) 4_556 29_566 Sn4 Sn1 Cu2 33.735(17) 4 29_566 Sn1 Sn1 Cu2 122.62(3) 18_545 29_566 Cu2 Sn1 Cu2 57.40(3) 12 29_566 Cu2 Sn1 Cu1 32.69(3) 27_566 5 Cu1 Sn1 Cu1 32.59(4) 27_566 5 Cu1 Sn1 Cu1 68.88(5) 12 5 Sn2 Sn1 Cu1 88.49(3) 11 5 Sn1 Sn1 Cu1 87.80(2) 19_566 5 Sn1 Sn1 Cu1 35.255(18) 37_665 5 Na1 Sn1 Cu1 157.98(9) . 5 Na4 Sn1 Cu1 98.69(2) 33_666 5 Na2 Sn1 Cu1 78.61(4) 9 5 Na1 Sn1 Cu1 128.28(9) 35_556 5 Na1 Sn1 Cu1 77.51(7) 4_556 5 Sn1 Sn1 Cu1 127.33(3) 4_556 5 Sn4 Sn1 Cu1 33.734(17) 4 5 Sn1 Sn1 Cu1 148.32(2) 18_545 5 Cu2 Sn1 Cu1 57.61(3) 12 5 Cu2 Sn1 Cu1 57.67(2) 29_566 5 Cu2 Sn1 Sn3 24.36(3) 27_566 4 Cu1 Sn1 Sn3 83.26(3) 27_566 4 Cu1 Sn1 Sn3 65.32(3) 12 4 Sn2 Sn1 Sn3 37.029(18) 11 4 Sn1 Sn1 Sn3 119.344(17) 19_566 4 Sn1 Sn1 Sn3 71.730(8) 37_665 4 Na1 Sn1 Sn3 112.63(12) . 4 Na4 Sn1 Sn3 110.890(17) 33_666 4 Na2 Sn1 Sn3 47.54(12) 9 4 Na1 Sn1 Sn3 98.81(8) 35_556 4 Na1 Sn1 Sn3 132.85(6) 4_556 4 Sn1 Sn1 Sn3 164.610(17) 4_556 4 Sn4 Sn1 Sn3 53.840(15) 4 4 Sn1 Sn1 Sn3 143.442(12) 18_545 4 Cu2 Sn1 Sn3 85.74(2) 12 4 Cu2 Sn1 Sn3 32.52(2) 29_566 4 Cu1 Sn1 Sn3 56.63(2) 5 4 Cu2 Sn1 Sn2 84.28(3) 27_566 28_566 Cu1 Sn1 Sn2 25.23(3) 27_566 28_566 Cu1 Sn1 Sn2 66.24(3) 12 28_566 Sn2 Sn1 Sn2 120.33(3) 11 28_566 Sn1 Sn1 Sn2 36.122(16) 19_566 28_566 Sn1 Sn1 Sn2 71.731(8) 37_665 28_566 Na1 Sn1 Sn2 139.55(11) . 28_566 Na4 Sn1 Sn2 105.072(16) 33_666 28_566 Na2 Sn1 Sn2 133.714(17) 9 28_566 Na1 Sn1 Sn2 99.41(12) 35_556 28_566 Na1 Sn1 Sn2 44.34(10) 4_556 28_566 Sn1 Sn1 Sn2 84.176(19) 4_556 28_566 Sn4 Sn1 Sn2 55.111(12) 4 28_566 Sn1 Sn1 Sn2 91.370(12) 18_545 28_566 Cu2 Sn1 Sn2 33.552(14) 12 28_566 Cu2 Sn1 Sn2 86.90(2) 29_566 28_566 Cu1 Sn1 Sn2 57.22(2) 5 28_566 Sn3 Sn1 Sn2 107.421(19) 4 28_566 Cu2 Sn1 Sn1 105.73(3) 27_566 38 Cu1 Sn1 Sn1 145.49(2) 27_566 38 Cu1 Sn1 Sn1 143.74(3) 12 38 Sn2 Sn1 Sn1 88.257(17) 11 38 Sn1 Sn1 Sn1 149.976(1) 19_566 38 Sn1 Sn1 Sn1 90.0 37_665 38 Na1 Sn1 Sn1 39.30(9) . 38 Na4 Sn1 Sn1 44.419(10) 33_666 38 Na2 Sn1 Sn1 44.86(9) 9 38 Na1 Sn1 Sn1 103.51(12) 35_556 38 Na1 Sn1 Sn1 105.88(10) 4_556 38 Sn1 Sn1 Sn1 76.444(12) 4_556 38 Sn4 Sn1 Sn1 140.794(8) 4 38 Sn1 Sn1 Sn1 90.144(13) 18_545 38 Cu2 Sn1 Sn1 174.506(18) 12 38 Cu2 Sn1 Sn1 117.446(19) 29_566 38 Cu1 Sn1 Sn1 118.684(19) 5 38 Sn3 Sn1 Sn1 88.774(15) 4 38 Sn2 Sn1 Sn1 149.484(11) 28_566 38 Cu2 Sn1 Sn1 66.19(2) 27_566 46_656 Cu1 Sn1 Sn1 84.36(3) 27_566 46_656 Cu1 Sn1 Sn1 25.02(3) 12 46_656 Sn2 Sn1 Sn1 35.434(17) 11 46_656 Sn1 Sn1 Sn1 72.149(19) 19_566 46_656 Sn1 Sn1 Sn1 120.0 37_665 46_656 Na1 Sn1 Sn1 104.62(13) . 46_656 Na4 Sn1 Sn1 164.048(10) 33_666 46_656 Na2 Sn1 Sn1 100.82(13) 9 46_656 Na1 Sn1 Sn1 44.78(7) 35_556 46_656 Na1 Sn1 Sn1 133.47(10) 4_556 46_656 Sn1 Sn1 Sn1 131.846(5) 4_556 46_656 Sn4 Sn1 Sn1 54.811(8) 4 46_656 Sn1 Sn1 Sn1 89.856(13) 18_545 46_656 Cu2 Sn1 Sn1 57.152(12) 12 46_656 Cu2 Sn1 Sn1 32.908(18) 29_566 46_656 Cu1 Sn1 Sn1 86.652(18) 5 46_656 Sn3 Sn1 Sn1 59.744(9) 4 46_656 Sn2 Sn1 Sn1 90.486(11) 28_566 46_656 Sn1 Sn1 Sn1 120.0 38 46_656 Cu2 Sn1 Sn1 65.61(2) 27_566 31_566 Cu1 Sn1 Sn1 24.81(2) 27_566 31_566 Cu1 Sn1 Sn1 84.22(3) 12 31_566 Sn2 Sn1 Sn1 120.476(19) 11 31_566 Sn1 Sn1 Sn1 71.98(2) 19_566 31_566 Sn1 Sn1 Sn1 35.875(12) 37_665 31_566 Na1 Sn1 Sn1 146.72(13) . 31_566 Na4 Sn1 Sn1 83.557(14) 33_666 31_566 Na2 Sn1 Sn1 98.77(3) 9 31_566 Na1 Sn1 Sn1 133.76(12) 35_556 31_566 Na1 Sn1 Sn1 44.73(7) 4_556 31_566 Sn1 Sn1 Sn1 94.89(2) 4_556 31_566 Sn4 Sn1 Sn1 54.772(4) 4 31_566 Sn1 Sn1 Sn1 121.378(12) 18_545 31_566 Cu2 Sn1 Sn1 57.440(16) 12 31_566 Cu2 Sn1 Sn1 86.627(16) 29_566 31_566 Cu1 Sn1 Sn1 32.915(16) 5 31_566 Sn3 Sn1 Sn1 89.342(12) 4 31_566 Sn2 Sn1 Sn1 35.857(11) 28_566 31_566 Sn1 Sn1 Sn1 122.212(10) 38 31_566 Sn1 Sn1 Sn1 108.107(7) 46_656 31_566 Cu2 Sn1 Sn1 84.31(3) 27_566 34_566 Cu1 Sn1 Sn1 66.14(2) 27_566 34_566 Cu1 Sn1 Sn1 24.76(3) 12 34_566 Sn2 Sn1 Sn1 71.307(15) 11 34_566 Sn1 Sn1 Sn1 36.27(2) 19_566 34_566 Sn1 Sn1 Sn1 119.968(8) 37_665 34_566 Na1 Sn1 Sn1 113.73(10) . 34_566 Na4 Sn1 Sn1 158.65(2) 33_666 34_566 Na2 Sn1 Sn1 135.38(13) 9 34_566 Na1 Sn1 Sn1 44.96(11) 35_556 34_566 Na1 Sn1 Sn1 99.01(10) 4_556 34_566 Sn1 Sn1 Sn1 105.407(10) 4_556 34_566 Sn4 Sn1 Sn1 54.772(4) 4 34_566 Sn1 Sn1 Sn1 72.70(2) 18_545 34_566 Cu2 Sn1 Sn1 32.928(16) 12 34_566 Cu2 Sn1 Sn1 56.983(18) 29_566 34_566 Cu1 Sn1 Sn1 86.561(19) 5 34_566 Sn3 Sn1 Sn1 89.341(12) 4 34_566 Sn2 Sn1 Sn1 60.526(14) 28_566 34_566 Sn1 Sn1 Sn1 147.546(10) 38 34_566 Sn1 Sn1 Sn1 35.875(12) 46_656 34_566 Sn1 Sn1 Sn1 90.154(17) 31_566 34_566 Cu2 Sn1 Sn2 24.97(2) 27_566 6 Cu1 Sn1 Sn2 65.18(3) 27_566 6 Cu1 Sn1 Sn2 84.42(3) 12 6 Sn2 Sn1 Sn2 73.42(3) 11 6 Sn1 Sn1 Sn2 119.655(14) 19_566 6 Sn1 Sn1 Sn2 35.339(12) 37_665 6 Na1 Sn1 Sn2 126.82(9) . 6 Na4 Sn1 Sn2 86.232(14) 33_666 6 Na2 Sn1 Sn2 46.22(4) 9 6 Na1 Sn1 Sn2 133.93(8) 35_556 6 Na1 Sn1 Sn2 98.09(6) 4_556 6 Sn1 Sn1 Sn2 137.079(16) 4_556 6 Sn4 Sn1 Sn2 54.617(10) 4 6 Sn1 Sn1 Sn2 179.07(2) 18_545 6 Cu2 Sn1 Sn2 86.44(2) 12 6 Cu2 Sn1 Sn2 57.77(2) 29_566 6 Cu1 Sn1 Sn2 32.59(2) 5 6 Sn3 Sn1 Sn2 36.393(11) 4 6 Sn2 Sn1 Sn2 89.497(16) 28_566 6 Sn1 Sn1 Sn2 88.936(10) 38 6 Sn1 Sn1 Sn2 90.479(11) 46_656 6 Sn1 Sn1 Sn2 59.314(11) 31_566 6 Sn1 Sn1 Sn2 108.047(10) 34_566 6 Cu2 Sn1 Na1 134.59(8) 27_566 33_566 Cu1 Sn1 Na1 76.68(8) 27_566 33_566 Cu1 Sn1 Na1 89.22(8) 12 33_566 Sn2 Sn1 Na1 133.12(8) 11 33_566 Sn1 Sn1 Na1 34.05(7) 19_566 33_566 Sn1 Sn1 Na1 109.48(8) 37_665 33_566 Na1 Sn1 Na1 88.58(18) . 33_566 Na4 Sn1 Na1 92.17(7) 33_666 33_566 Na2 Sn1 Na1 157.99(15) 9 33_566 Na1 Sn1 Na1 72.76(18) 35_556 33_566 Na1 Sn1 Na1 46.98(14) 4_556 33_566 Sn1 Sn1 Na1 41.96(7) 4_556 33_566 Sn4 Sn1 Na1 100.79(7) 4 33_566 Sn1 Sn1 Na1 41.71(8) 18_545 33_566 Cu2 Sn1 Na1 67.85(7) 12 33_566 Cu2 Sn1 Na1 121.72(7) 29_566 33_566 Cu1 Sn1 Na1 108.22(8) 5 33_566 Sn3 Sn1 Na1 153.32(7) 4 33_566 Sn2 Sn1 Na1 51.46(8) 28_566 33_566 Sn1 Sn1 Na1 117.65(7) 38 33_566 Sn1 Sn1 Na1 100.46(7) 46_656 33_566 Sn1 Sn1 Na1 79.81(8) 31_566 33_566 Sn1 Sn1 Na1 66.60(7) 34_566 33_566 Sn2 Sn1 Na1 139.03(8) 6 33_566 Cu2 Sn1 Na3 59.60(11) 27_566 2 Cu1 Sn1 Na3 118.22(10) 27_566 2 Cu1 Sn1 Na3 82.02(3) 12 2 Sn2 Sn1 Na3 27.57(3) 11 2 Sn1 Sn1 Na3 135.11(4) 19_566 2 Sn1 Sn1 Na3 96.21(11) 37_665 2 Na1 Sn1 Na3 77.75(15) . 2 Na4 Sn1 Na3 101.69(2) 33_666 2 Na2 Sn1 Na3 40.66(13) 9 2 Na1 Sn1 Na3 81.94(15) 35_556 2 Na1 Sn1 Na3 158.22(12) 4_556 2 Sn1 Sn1 Na3 134.75(8) 4_556 2 Sn4 Sn1 Na3 85.88(7) 4 2 Sn1 Sn1 Na3 115.01(12) 18_545 2 Cu2 Sn1 Na3 112.05(4) 12 2 Cu2 Sn1 Na3 55.05(5) 29_566 2 Cu1 Sn1 Na3 91.23(11) 5 2 Sn3 Sn1 Na3 35.28(10) 4 2 Sn2 Sn1 Na3 140.99(7) 28_566 2 Sn1 Sn1 Na3 63.12(3) 38 2 Sn1 Sn1 Na3 62.99(3) 46_656 2 Sn1 Sn1 Na3 122.97(12) 31_566 2 Sn1 Sn1 Na3 98.85(3) 34_566 2 Sn2 Sn1 Na3 64.40(12) 6 2 Na1 Sn1 Na3 154.20(13) 33_566 2 Cu2 Sn1 Sn1 99.18(2) 27_566 40_567 Cu1 Sn1 Sn1 72.52(3) 27_566 40_567 Cu1 Sn1 Sn1 132.25(3) 12 40_567 Sn2 Sn1 Sn1 149.58(2) 11 40_567 Sn1 Sn1 Sn1 95.76(3) 19_566 40_567 Sn1 Sn1 Sn1 43.749(11) 37_665 40_567 Na1 Sn1 Sn1 98.35(13) . 40_567 Na4 Sn1 Sn1 36.553(5) 33_666 40_567 Na2 Sn1 Sn1 86.00(11) 9 40_567 Na1 Sn1 Sn1 147.08(9) 35_556 40_567 Na1 Sn1 Sn1 32.20(8) 4_556 40_567 Sn1 Sn1 Sn1 59.808(17) 4_556 40_567 Sn4 Sn1 Sn1 102.682(15) 4 40_567 Sn1 Sn1 Sn1 101.783(14) 18_545 40_567 Cu2 Sn1 Sn1 101.506(18) 12 40_567 Cu2 Sn1 Sn1 130.24(2) 29_566 40_567 Cu1 Sn1 Sn1 72.860(19) 5 40_567 Sn3 Sn1 Sn1 114.021(14) 4 40_567 Sn2 Sn1 Sn1 69.458(15) 28_566 40_567 Sn1 Sn1 Sn1 80.403(9) 38 40_567 Sn1 Sn1 Sn1 156.794(9) 46_656 40_567 Sn1 Sn1 Sn1 48.711(15) 31_566 40_567 Sn1 Sn1 Sn1 129.280(19) 34_566 40_567 Sn2 Sn1 Sn1 78.205(14) 6 40_567 Na1 Sn1 Sn1 76.56(8) 33_566 40_567 Na3 Sn1 Sn1 126.65(7) 2 40_567 Cu2 Sn1 Sn1 144.38(3) 27_566 39_657 Cu1 Sn1 Sn1 131.28(4) 27_566 39_657 Cu1 Sn1 Sn1 154.59(4) 12 39_657 Sn2 Sn1 Sn1 124.02(2) 11 39_657 Sn1 Sn1 Sn1 107.996(11) 19_566 39_657 Sn1 Sn1 Sn1 99.598(9) 37_665 39_657 Na1 Sn1 Sn1 35.87(13) . 39_657 Na4 Sn1 Sn1 36.552(5) 33_666 39_657 Na2 Sn1 Sn1 86.00(11) 9 39_657 Na1 Sn1 Sn1 96.70(8) 35_556 39_657 Na1 Sn1 Sn1 72.36(10) 4_556 39_657 Sn1 Sn1 Sn1 32.696(15) 4_556 39_657 Sn4 Sn1 Sn1 165.673(17) 4 39_657 Sn1 Sn1 Sn1 58.593(18) 18_545 39_657 Cu2 Sn1 Sn1 141.68(2) 12 39_657 Cu2 Sn1 Sn1 159.07(2) 29_566 39_657 Cu1 Sn1 Sn1 134.27(2) 5 39_657 Sn3 Sn1 Sn1 132.370(19) 4 39_657 Sn2 Sn1 Sn1 113.986(19) 28_566 39_657 Sn1 Sn1 Sn1 43.748(11) 38 39_657 Sn1 Sn1 Sn1 138.795(9) 46_656 39_657 Sn1 Sn1 Sn1 110.903(14) 31_566 39_657 Sn1 Sn1 Sn1 131.137(16) 34_566 39_657 Sn2 Sn1 Sn1 120.701(13) 6 39_657 Na1 Sn1 Sn1 74.27(7) 33_566 39_657 Na3 Sn1 Sn1 104.45(6) 2 39_657 Sn1 Sn1 Sn1 63.233(12) 40_567 39_657 Cu2 Sn1 Na1 73.65(7) 27_566 2 Cu1 Sn1 Na1 81.73(4) 27_566 2 Cu1 Sn1 Na1 129.97(7) 12 2 Sn2 Sn1 Na1 113.26(7) 11 2 Sn1 Sn1 Na1 127.07(5) 19_566 2 Sn1 Sn1 Na1 27.37(4) 37_665 2 Na1 Sn1 Na1 98.86(14) . 2 Na4 Sn1 Na1 38.62(6) 33_666 2 Na2 Sn1 Na1 50.59(11) 9 2 Na1 Sn1 Na1 167.29(12) 35_556 2 Na1 Sn1 Na1 67.61(11) 4_556 2 Sn1 Sn1 Na1 88.99(7) 4_556 2 Sn4 Sn1 Na1 95.21(5) 4 2 Sn1 Sn1 Na1 130.71(7) 18_545 2 Cu2 Sn1 Na1 114.74(4) 12 2 Cu2 Sn1 Na1 106.65(7) 29_566 2 Cu1 Sn1 Na1 61.84(5) 5 2 Sn3 Sn1 Na1 80.52(8) 4 2 Sn2 Sn1 Na1 92.85(4) 28_566 2 Sn1 Sn1 Na1 63.83(3) 38 2 Sn1 Sn1 Na1 139.14(7) 46_656 2 Sn1 Sn1 Na1 58.93(3) 31_566 2 Sn1 Sn1 Na1 147.27(4) 34_566 2 Sn2 Sn1 Na1 48.88(7) 6 2 Na1 Sn1 Na1 113.22(7) 33_566 2 Na3 Sn1 Na1 90.66(11) 2 2 Sn1 Sn1 Na1 36.67(7) 40_567 2 Sn1 Sn1 Na1 75.07(6) 39_657 2 Cu2 Sn1 Sn2 86.22(3) 27_566 8 Cu1 Sn1 Sn2 144.76(3) 27_566 8 Cu1 Sn1 Sn2 111.71(3) 12 8 Sn2 Sn1 Sn2 56.13(2) 11 8 Sn1 Sn1 Sn2 151.63(3) 19_566 8 Sn1 Sn1 Sn2 99.848(10) 37_665 8 Na1 Sn1 Sn2 50.07(11) . 8 Na4 Sn1 Sn2 75.101(12) 33_666 8 Na2 Sn1 Sn2 36.78(2) 9 8 Na1 Sn1 Sn2 87.31(12) 35_556 8 Na1 Sn1 Sn2 137.53(10) 4_556 8 Sn1 Sn1 Sn2 103.674(19) 4_556 8 Sn4 Sn1 Sn2 117.095(14) 4 8 Sn1 Sn1 Sn2 98.766(13) 18_545 8 Cu2 Sn1 Sn2 143.563(18) 12 8 Cu2 Sn1 Sn2 87.14(2) 29_566 8 Cu1 Sn1 Sn2 112.63(2) 5 8 Sn3 Sn1 Sn2 63.738(17) 4 8 Sn2 Sn1 Sn2 169.847(18) 28_566 8 Sn1 Sn1 Sn2 32.123(9) 38 8 Sn1 Sn1 Sn2 88.963(9) 46_656 8 Sn1 Sn1 Sn2 135.449(18) 31_566 8 Sn1 Sn1 Sn2 122.038(16) 34_566 8 Sn2 Sn1 Sn2 80.371(18) 6 8 Na1 Sn1 Sn2 138.52(8) 33_566 8 Na3 Sn1 Sn2 32.10(5) 2 8 Sn1 Sn1 Sn2 108.678(11) 40_567 8 Sn1 Sn1 Sn2 72.396(12) 39_657 8 Na1 Sn1 Sn2 81.01(4) 2 8 Cu1 Sn2 Cu2 59.89(4) 2 34 Cu1 Sn2 Cu2 59.89(4) 2 30 Cu2 Sn2 Cu2 59.90(6) 34 30 Cu1 Sn2 Sn1 56.417(18) 2 42_566 Cu2 Sn2 Sn1 55.83(3) 34 42_566 Cu2 Sn2 Sn1 104.59(4) 30 42_566 Cu1 Sn2 Sn1 56.417(18) 2 8 Cu2 Sn2 Sn1 104.59(4) 34 8 Cu2 Sn2 Sn1 55.83(3) 30 8 Sn1 Sn2 Sn1 109.13(3) 42_566 8 Cu1 Sn2 Sn3 102.16(5) 2 . Cu2 Sn2 Sn3 54.21(4) 34 . Cu2 Sn2 Sn3 54.21(4) 30 . Sn1 Sn2 Sn3 106.64(3) 42_566 . Sn1 Sn2 Sn3 106.64(3) 8 . Cu1 Sn2 Na3 164.1(2) 2 2 Cu2 Sn2 Na3 106.81(17) 34 2 Cu2 Sn2 Na3 106.81(17) 30 2 Sn1 Sn2 Na3 125.420(17) 42_566 2 Sn1 Sn2 Na3 125.420(17) 8 2 Sn3 Sn2 Na3 62.0(2) . 2 Cu1 Sn2 Na1 60.35(13) 2 25_556 Cu2 Sn2 Na1 111.45(11) 34 25_556 Cu2 Sn2 Na1 111.45(11) 30 25_556 Sn1 Sn2 Na1 64.88(6) 42_566 25_556 Sn1 Sn2 Na1 64.88(6) 8 25_556 Sn3 Sn2 Na1 162.51(13) . 25_556 Na3 Sn2 Na1 135.5(2) 2 25_556 Cu1 Sn2 Na2 109.88(10) 2 6 Cu2 Sn2 Na2 59.03(4) 34 6 Cu2 Sn2 Na2 110.81(7) 30 6 Sn1 Sn2 Na2 62.61(14) 42_566 6 Sn1 Sn2 Na2 163.62(4) 8 6 Sn3 Sn2 Na2 65.29(11) . 6 Na3 Sn2 Na2 64.91(14) 2 6 Na1 Sn2 Na2 118.44(14) 25_556 6 Cu1 Sn2 Na2 109.88(10) 2 2 Cu2 Sn2 Na2 110.81(7) 34 2 Cu2 Sn2 Na2 59.03(4) 30 2 Sn1 Sn2 Na2 163.62(4) 42_566 2 Sn1 Sn2 Na2 62.61(14) 8 2 Sn3 Sn2 Na2 65.29(11) . 2 Na3 Sn2 Na2 64.91(14) 2 2 Na1 Sn2 Na2 118.44(14) 25_556 2 Na2 Sn2 Na2 121.2(3) 6 2 Cu1 Sn2 Sn4 35.00(3) 2 . Cu2 Sn2 Sn4 35.30(3) 34 . Cu2 Sn2 Sn4 35.30(3) 30 . Sn1 Sn2 Sn4 69.300(18) 42_566 . Sn1 Sn2 Sn4 69.300(18) 8 . Sn3 Sn2 Sn4 67.16(3) . . Na3 Sn2 Sn4 129.1(2) 2 . Na1 Sn2 Sn4 95.35(12) 25_556 . Na2 Sn2 Sn4 94.32(3) 6 . Na2 Sn2 Sn4 94.32(3) 2 . Cu1 Sn2 Na1 93.22(6) 2 11 Cu2 Sn2 Na1 97.27(10) 34 11 Cu2 Sn2 Na1 150.44(8) 30 11 Sn1 Sn2 Na1 46.29(8) 42_566 11 Sn1 Sn2 Na1 121.46(7) 8 11 Sn3 Sn2 Na1 129.69(8) . 11 Na3 Sn2 Na1 97.37(14) 2 11 Na1 Sn2 Na1 56.59(8) 25_556 11 Na2 Sn2 Na1 64.43(14) 6 11 Na2 Sn2 Na1 149.89(8) 2 11 Sn4 Sn2 Na1 115.32(8) . 11 Cu1 Sn2 Na1 93.22(6) 2 8 Cu2 Sn2 Na1 150.44(8) 34 8 Cu2 Sn2 Na1 97.27(10) 30 8 Sn1 Sn2 Na1 121.46(7) 42_566 8 Sn1 Sn2 Na1 46.29(8) 8 8 Sn3 Sn2 Na1 129.69(8) . 8 Na3 Sn2 Na1 97.37(14) 2 8 Na1 Sn2 Na1 56.59(8) 25_556 8 Na2 Sn2 Na1 149.89(8) 6 8 Na2 Sn2 Na1 64.43(14) 2 8 Sn4 Sn2 Na1 115.32(8) . 8 Na1 Sn2 Na1 96.20(18) 11 8 Cu1 Sn2 Cu1 33.00(3) 2 34 Cu2 Sn2 Cu1 33.00(3) 34 34 Cu2 Sn2 Cu1 69.19(4) 30 34 Sn1 Sn2 Cu1 35.41(2) 42_566 34 Sn1 Sn2 Cu1 88.51(3) 8 34 Sn3 Sn2 Cu1 86.15(3) . 34 Na3 Sn2 Cu1 137.59(14) 2 34 Na1 Sn2 Cu1 78.57(11) 25_556 34 Na2 Sn2 Cu1 77.00(9) 6 34 Na2 Sn2 Cu1 128.21(4) 2 34 Sn4 Sn2 Cu1 33.895(19) . 34 Na1 Sn2 Cu1 81.53(8) 11 34 Na1 Sn2 Cu1 124.99(5) 8 34 Cu1 Sn2 Cu1 33.00(3) 2 30 Cu2 Sn2 Cu1 69.19(4) 34 30 Cu2 Sn2 Cu1 33.00(3) 30 30 Sn1 Sn2 Cu1 88.51(3) 42_566 30 Sn1 Sn2 Cu1 35.41(2) 8 30 Sn3 Sn2 Cu1 86.15(3) . 30 Na3 Sn2 Cu1 137.59(14) 2 30 Na1 Sn2 Cu1 78.57(11) 25_556 30 Na2 Sn2 Cu1 128.21(4) 6 30 Na2 Sn2 Cu1 77.00(9) 2 30 Sn4 Sn2 Cu1 33.895(19) . 30 Na1 Sn2 Cu1 124.99(5) 11 30 Na1 Sn2 Cu1 81.53(8) 8 30 Cu1 Sn2 Cu1 57.92(4) 34 30 Cu1 Sn2 Cu2 68.50(4) 2 26 Cu2 Sn2 Cu2 32.74(3) 34 26 Cu2 Sn2 Cu2 32.74(3) 30 26 Sn1 Sn2 Cu2 87.64(2) 42_566 26 Sn1 Sn2 Cu2 87.64(2) 8 26 Sn3 Sn2 Cu2 33.66(3) . 26 Na3 Sn2 Cu2 95.6(2) 2 26 Na1 Sn2 Cu2 128.85(13) 25_556 26 Na2 Sn2 Cu2 78.17(5) 6 26 Na2 Sn2 Cu2 78.17(5) 2 26 Sn4 Sn2 Cu2 33.501(19) . 26 Na1 Sn2 Cu2 129.77(9) 11 26 Na1 Sn2 Cu2 129.77(9) 8 26 Cu1 Sn2 Cu2 57.36(2) 34 26 Cu1 Sn2 Cu2 57.36(2) 30 26 Cu1 Sn2 Sn2 147.936(12) 2 11 Cu2 Sn2 Sn2 143.21(3) 34 11 Cu2 Sn2 Sn2 107.55(3) 30 11 Sn1 Sn2 Sn2 147.690(18) 42_566 11 Sn1 Sn2 Sn2 91.742(17) 8 11 Sn3 Sn2 Sn2 89.76(2) . 11 Na3 Sn2 Sn2 39.98(13) 2 11 Na1 Sn2 Sn2 105.32(11) 25_556 11 Na2 Sn2 Sn2 102.16(10) 6 11 Na2 Sn2 Sn2 48.66(4) 2 11 Sn4 Sn2 Sn2 142.798(6) . 11 Na1 Sn2 Sn2 101.88(8) 11 11 Na1 Sn2 Sn2 57.42(5) 8 11 Cu1 Sn2 Sn2 175.799(17) 34 11 Cu1 Sn2 Sn2 120.873(18) 30 11 Cu2 Sn2 Sn2 118.460(17) 26 11 Cu1 Sn2 Sn2 147.936(12) 2 8 Cu2 Sn2 Sn2 107.55(3) 34 8 Cu2 Sn2 Sn2 143.21(3) 30 8 Sn1 Sn2 Sn2 91.742(17) 42_566 8 Sn1 Sn2 Sn2 147.690(18) 8 8 Sn3 Sn2 Sn2 89.76(2) . 8 Na3 Sn2 Sn2 39.98(13) 2 8 Na1 Sn2 Sn2 105.32(11) 25_556 8 Na2 Sn2 Sn2 48.66(4) 6 8 Na2 Sn2 Sn2 102.16(10) 2 8 Sn4 Sn2 Sn2 142.798(6) . 8 Na1 Sn2 Sn2 57.42(5) 11 8 Na1 Sn2 Sn2 101.88(8) 8 8 Cu1 Sn2 Sn2 120.873(18) 34 8 Cu1 Sn2 Sn2 175.799(17) 30 8 Cu2 Sn2 Sn2 118.460(17) 26 8 Sn2 Sn2 Sn2 60.0 11 8 Cu1 Sn2 Sn1 25.41(2) 2 15_454 Cu2 Sn2 Sn1 84.85(3) 34 15_454 Cu2 Sn2 Sn1 66.25(3) 30 15_454 Sn1 Sn2 Sn1 72.836(18) 42_566 15_454 Sn1 Sn2 Sn1 36.298(19) 8 15_454 Sn3 Sn2 Sn1 118.47(3) . 15_454 Na3 Sn2 Sn1 161.62(2) 2 15_454 Na1 Sn2 Sn1 45.45(11) 25_556 15_454 Na2 Sn2 Sn1 133.16(12) 6 15_454 Na2 Sn2 Sn1 97.93(13) 2 15_454 Sn4 Sn2 Sn1 55.122(11) . 15_454 Na1 Sn2 Sn1 95.11(5) 11 15_454 Na1 Sn2 Sn1 67.81(6) 8 15_454 Cu1 Sn2 Sn1 57.815(17) 34 15_454 Cu1 Sn2 Sn1 33.257(13) 30 15_454 Cu2 Sn2 Sn1 86.65(2) 26 15_454 Sn2 Sn2 Sn1 123.811(9) 11 15_454 Sn2 Sn2 Sn1 150.451(11) 8 15_454 Cu1 Sn2 Sn1 25.41(2) 2 28 Cu2 Sn2 Sn1 66.25(3) 34 28 Cu2 Sn2 Sn1 84.85(3) 30 28 Sn1 Sn2 Sn1 36.298(19) 42_566 28 Sn1 Sn2 Sn1 72.836(18) 8 28 Sn3 Sn2 Sn1 118.47(3) . 28 Na3 Sn2 Sn1 161.62(2) 2 28 Na1 Sn2 Sn1 45.45(11) 25_556 28 Na2 Sn2 Sn1 97.93(13) 6 28 Na2 Sn2 Sn1 133.16(12) 2 28 Sn4 Sn2 Sn1 55.122(11) . 28 Na1 Sn2 Sn1 67.81(6) 11 28 Na1 Sn2 Sn1 95.11(5) 8 28 Cu1 Sn2 Sn1 33.257(13) 34 28 Cu1 Sn2 Sn1 57.815(17) 30 28 Cu2 Sn2 Sn1 86.65(2) 26 28 Sn2 Sn2 Sn1 150.451(11) 11 28 Sn2 Sn2 Sn1 123.811(9) 8 28 Sn1 Sn2 Sn1 36.539(15) 15_454 28 Cu1 Sn2 Sn1 65.877(19) 2 12 Cu2 Sn2 Sn1 24.66(3) 34 12 Cu2 Sn2 Sn1 84.11(4) 30 12 Sn1 Sn2 Sn1 35.906(17) 42_566 12 Sn1 Sn2 Sn1 120.38(3) 8 12 Sn3 Sn2 Sn1 70.735(18) . 12 Na3 Sn2 Sn1 106.06(11) 2 12 Na1 Sn2 Sn1 99.65(7) 25_556 12 Na2 Sn2 Sn1 44.35(8) 6 12 Na2 Sn2 Sn1 133.75(8) 2 12 Sn4 Sn2 Sn1 54.628(10) . 12 Na1 Sn2 Sn1 72.85(9) 11 12 Na1 Sn2 Sn1 155.11(5) 8 12 Cu1 Sn2 Sn1 32.878(16) 34 12 Cu1 Sn2 Sn1 86.68(2) 30 12 Cu2 Sn2 Sn1 56.925(12) 26 12 Sn2 Sn2 Sn1 145.686(11) 11 12 Sn2 Sn2 Sn1 91.064(10) 8 12 Sn1 Sn2 Sn1 90.495(16) 15_454 12 Sn1 Sn2 Sn1 60.161(11) 28 12 Cu1 Sn2 Sn1 65.877(19) 2 45_665 Cu2 Sn2 Sn1 84.11(3) 34 45_665 Cu2 Sn2 Sn1 24.66(3) 30 45_665 Sn1 Sn2 Sn1 120.38(3) 42_566 45_665 Sn1 Sn2 Sn1 35.906(17) 8 45_665 Sn3 Sn2 Sn1 70.735(18) . 45_665 Na3 Sn2 Sn1 106.06(11) 2 45_665 Na1 Sn2 Sn1 99.65(7) 25_556 45_665 Na2 Sn2 Sn1 133.75(8) 6 45_665 Na2 Sn2 Sn1 44.35(8) 2 45_665 Sn4 Sn2 Sn1 54.628(10) . 45_665 Na1 Sn2 Sn1 155.11(5) 11 45_665 Na1 Sn2 Sn1 72.85(9) 8 45_665 Cu1 Sn2 Sn1 86.68(2) 34 45_665 Cu1 Sn2 Sn1 32.878(16) 30 45_665 Cu2 Sn2 Sn1 56.925(12) 26 45_665 Sn2 Sn2 Sn1 91.064(10) 11 45_665 Sn2 Sn2 Sn1 145.686(11) 8 45_665 Sn1 Sn2 Sn1 60.161(11) 15_454 45_665 Sn1 Sn2 Sn1 90.495(16) 28 45_665 Sn1 Sn2 Sn1 107.68(2) 12 45_665 Cu1 Sn2 Sn2 83.44(3) 2 9 Cu2 Sn2 Sn2 65.54(3) 34 9 Cu2 Sn2 Sn2 24.02(3) 30 9 Sn1 Sn2 Sn2 119.556(19) 42_566 9 Sn1 Sn2 Sn2 71.245(19) 8 9 Sn3 Sn2 Sn2 35.402(14) . 9 Na3 Sn2 Sn2 82.82(17) 2 9 Na1 Sn2 Sn2 133.59(9) 25_556 9 Na2 Sn2 Sn2 99.80(10) 6 9 Na2 Sn2 Sn2 45.50(4) 2 9 Sn4 Sn2 Sn2 54.124(9) . 9 Na1 Sn2 Sn2 161.77(9) 11 9 Na1 Sn2 Sn2 101.86(9) 8 9 Cu1 Sn2 Sn2 86.106(19) 34 9 Cu1 Sn2 Sn2 56.489(14) 30 9 Cu2 Sn2 Sn2 32.795(8) 26 9 Sn2 Sn2 Sn2 90.0 11 9 Sn2 Sn2 Sn2 120.0 8 9 Sn1 Sn2 Sn2 89.515(11) 15_454 9 Sn1 Sn2 Sn2 107.759(11) 28 9 Sn1 Sn2 Sn2 89.521(11) 12 9 Sn1 Sn2 Sn2 35.339(12) 45_665 9 Cu1 Sn2 Sn2 83.44(3) 2 5 Cu2 Sn2 Sn2 24.02(3) 34 5 Cu2 Sn2 Sn2 65.54(3) 30 5 Sn1 Sn2 Sn2 71.245(19) 42_566 5 Sn1 Sn2 Sn2 119.556(19) 8 5 Sn3 Sn2 Sn2 35.402(14) . 5 Na3 Sn2 Sn2 82.82(17) 2 5 Na1 Sn2 Sn2 133.59(9) 25_556 5 Na2 Sn2 Sn2 45.50(4) 6 5 Na2 Sn2 Sn2 99.80(10) 2 5 Sn4 Sn2 Sn2 54.124(9) . 5 Na1 Sn2 Sn2 101.86(9) 11 5 Na1 Sn2 Sn2 161.77(9) 8 5 Cu1 Sn2 Sn2 56.489(14) 34 5 Cu1 Sn2 Sn2 86.106(19) 30 5 Cu2 Sn2 Sn2 32.795(8) 26 5 Sn2 Sn2 Sn2 120.0 11 5 Sn2 Sn2 Sn2 90.0 8 5 Sn1 Sn2 Sn2 107.759(11) 15_454 5 Sn1 Sn2 Sn2 89.515(11) 28 5 Sn1 Sn2 Sn2 35.339(12) 12 5 Sn1 Sn2 Sn2 89.521(11) 45_665 5 Sn2 Sn2 Sn2 60.0 9 5 Cu1 Sn2 Na3 116.56(9) 2 4 Cu2 Sn2 Na3 57.47(10) 34 4 Cu2 Sn2 Na3 81.03(3) 30 4 Sn1 Sn2 Na3 94.37(11) 42_566 4 Sn1 Sn2 Na3 134.37(4) 8 4 Sn3 Sn2 Na3 27.79(3) . 4 Na3 Sn2 Na3 49.4(3) 2 4 Na1 Sn2 Na3 157.51(9) 25_556 4 Na2 Sn2 Na3 39.50(15) 6 4 Na2 Sn2 Na3 83.94(17) 2 4 Sn4 Sn2 Na3 84.40(7) . 4 Na1 Sn2 Na3 103.20(9) 11 4 Na1 Sn2 Na3 142.90(12) 8 4 Cu1 Sn2 Na3 89.32(10) 34 4 Cu1 Sn2 Na3 111.00(4) 30 4 Cu2 Sn2 Na3 53.95(4) 26 4 Sn2 Sn2 Na3 87.51(11) 11 4 Sn2 Sn2 Na3 64.80(3) 8 4 Sn1 Sn2 Na3 139.52(7) 15_454 4 Sn1 Sn2 Na3 121.40(11) 28 4 Sn1 Sn2 Na3 61.96(11) 12 4 Sn1 Sn2 Na3 98.47(3) 45_665 4 Sn2 Sn2 Na3 63.14(3) 9 4 Sn2 Sn2 Na3 33.46(9) 5 4 Cu1 Sn2 Na3 116.56(9) 2 3 Cu2 Sn2 Na3 81.03(3) 34 3 Cu2 Sn2 Na3 57.47(10) 30 3 Sn1 Sn2 Na3 134.37(4) 42_566 3 Sn1 Sn2 Na3 94.37(11) 8 3 Sn3 Sn2 Na3 27.79(3) . 3 Na3 Sn2 Na3 49.4(3) 2 3 Na1 Sn2 Na3 157.51(9) 25_556 3 Na2 Sn2 Na3 83.94(17) 6 3 Na2 Sn2 Na3 39.50(15) 2 3 Sn4 Sn2 Na3 84.40(7) . 3 Na1 Sn2 Na3 142.90(12) 11 3 Na1 Sn2 Na3 103.20(9) 8 3 Cu1 Sn2 Na3 111.00(4) 34 3 Cu1 Sn2 Na3 89.32(10) 30 3 Cu2 Sn2 Na3 53.95(4) 26 3 Sn2 Sn2 Na3 64.80(3) 11 3 Sn2 Sn2 Na3 87.51(11) 8 3 Sn1 Sn2 Na3 121.40(11) 15_454 3 Sn1 Sn2 Na3 139.52(7) 28 3 Sn1 Sn2 Na3 98.47(3) 12 3 Sn1 Sn2 Na3 61.96(11) 45_665 3 Sn2 Sn2 Na3 33.46(9) 9 3 Sn2 Sn2 Na3 63.14(3) 5 3 Na3 Sn2 Na3 44.96(17) 4 3 Cu1 Sn2 Sn3 145.38(3) 2 3 Cu2 Sn2 Sn3 86.11(3) 34 3 Cu2 Sn2 Sn3 110.44(4) 30 3 Sn1 Sn2 Sn3 100.478(17) 42_566 3 Sn1 Sn2 Sn3 149.58(2) 8 3 Sn3 Sn2 Sn3 56.64(3) . 3 Na3 Sn2 Sn3 26.24(7) 2 3 Na1 Sn2 Sn3 137.90(10) 25_556 3 Na2 Sn2 Sn3 38.73(13) 6 3 Na2 Sn2 Sn3 86.99(14) 2 3 Sn4 Sn2 Sn3 116.941(16) . 3 Na1 Sn2 Sn3 84.22(5) 11 3 Na1 Sn2 Sn3 121.40(6) 8 3 Cu1 Sn2 Sn3 113.068(16) 34 3 Cu1 Sn2 Sn3 142.77(2) 30 3 Cu2 Sn2 Sn3 86.74(2) 26 3 Sn2 Sn2 Sn3 65.176(7) 11 3 Sn2 Sn2 Sn3 33.130(13) 8 3 Sn1 Sn2 Sn3 170.785(16) 15_454 3 Sn1 Sn2 Sn3 136.491(11) 28 3 Sn1 Sn2 Sn3 80.513(11) 12 3 Sn1 Sn2 Sn3 120.63(2) 45_665 3 Sn2 Sn2 Sn3 88.403(14) 9 3 Sn2 Sn2 Sn3 63.546(9) 5 3 Na3 Sn2 Sn3 32.95(5) 4 3 Na3 Sn2 Sn3 58.68(11) 3 3 Cu1 Sn2 Sn3 145.38(3) 2 4 Cu2 Sn2 Sn3 110.44(4) 34 4 Cu2 Sn2 Sn3 86.11(3) 30 4 Sn1 Sn2 Sn3 149.58(2) 42_566 4 Sn1 Sn2 Sn3 100.478(17) 8 4 Sn3 Sn2 Sn3 56.64(3) . 4 Na3 Sn2 Sn3 26.24(7) 2 4 Na1 Sn2 Sn3 137.90(10) 25_556 4 Na2 Sn2 Sn3 86.99(14) 6 4 Na2 Sn2 Sn3 38.73(13) 2 4 Sn4 Sn2 Sn3 116.941(16) . 4 Na1 Sn2 Sn3 121.40(6) 11 4 Na1 Sn2 Sn3 84.22(5) 8 4 Cu1 Sn2 Sn3 142.77(2) 34 4 Cu1 Sn2 Sn3 113.068(16) 30 4 Cu2 Sn2 Sn3 86.74(2) 26 4 Sn2 Sn2 Sn3 33.130(13) 11 4 Sn2 Sn2 Sn3 65.176(7) 8 4 Sn1 Sn2 Sn3 136.491(11) 15_454 4 Sn1 Sn2 Sn3 170.785(16) 28 4 Sn1 Sn2 Sn3 120.63(2) 12 4 Sn1 Sn2 Sn3 80.513(11) 45_665 4 Sn2 Sn2 Sn3 63.546(9) 9 4 Sn2 Sn2 Sn3 88.403(14) 5 4 Na3 Sn2 Sn3 58.68(11) 4 4 Na3 Sn2 Sn3 32.95(5) 3 4 Sn3 Sn2 Sn3 49.37(2) 3 4 Cu1 Sn2 Sn1 115.922(14) 2 46_656 Cu2 Sn2 Sn1 145.61(4) 34 46_656 Cu2 Sn2 Sn1 87.79(3) 30 46_656 Sn1 Sn2 Sn1 154.66(3) 42_566 46_656 Sn1 Sn2 Sn1 59.618(16) 8 46_656 Sn3 Sn2 Sn1 98.555(17) . 46_656 Na3 Sn2 Sn1 69.33(8) 2 46_656 Na1 Sn2 Sn1 90.12(6) 25_556 46_656 Na2 Sn2 Sn1 133.80(11) 6 46_656 Na2 Sn2 Sn1 35.43(7) 2 46_656 Sn4 Sn2 Sn1 119.960(10) . 46_656 Na1 Sn2 Sn1 117.09(9) 11 46_656 Na1 Sn2 Sn1 33.66(6) 8 46_656 Cu1 Sn2 Sn1 147.87(2) 34 46_656 Cu1 Sn2 Sn1 90.530(19) 30 46_656 Cu2 Sn2 Sn1 112.918(13) 26 46_656 Sn2 Sn2 Sn1 32.124(9) 11 46_656 Sn2 Sn2 Sn1 91.036(9) 8 46_656 Sn1 Sn2 Sn1 92.952(12) 15_454 46_656 Sn1 Sn2 Sn1 126.429(16) 28 46_656 Sn1 Sn2 Sn1 169.075(19) 12 46_656 Sn1 Sn2 Sn1 65.488(12) 45_665 46_656 Sn2 Sn2 Sn1 80.151(10) 9 46_656 Sn2 Sn2 Sn1 133.944(10) 5 46_656 Na3 Sn2 Sn1 109.54(11) 4 46_656 Na3 Sn2 Sn1 70.91(4) 3 46_656 Sn3 Sn2 Sn1 95.533(14) 3 46_656 Sn3 Sn2 Sn1 51.242(14) 4 46_656 Cu1 Sn2 Sn1 115.922(14) 2 11 Cu2 Sn2 Sn1 87.79(3) 34 11 Cu2 Sn2 Sn1 145.61(4) 30 11 Sn1 Sn2 Sn1 59.618(16) 42_566 11 Sn1 Sn2 Sn1 154.66(3) 8 11 Sn3 Sn2 Sn1 98.555(17) . 11 Na3 Sn2 Sn1 69.33(8) 2 11 Na1 Sn2 Sn1 90.12(6) 25_556 11 Na2 Sn2 Sn1 35.43(7) 6 11 Na2 Sn2 Sn1 133.80(11) 2 11 Sn4 Sn2 Sn1 119.960(10) . 11 Na1 Sn2 Sn1 33.66(6) 11 11 Na1 Sn2 Sn1 117.09(9) 8 11 Cu1 Sn2 Sn1 90.530(19) 34 11 Cu1 Sn2 Sn1 147.87(2) 30 11 Cu2 Sn2 Sn1 112.918(13) 26 11 Sn2 Sn2 Sn1 91.036(9) 11 11 Sn2 Sn2 Sn1 32.124(9) 8 11 Sn1 Sn2 Sn1 126.429(16) 15_454 11 Sn1 Sn2 Sn1 92.952(12) 28 11 Sn1 Sn2 Sn1 65.488(12) 12 11 Sn1 Sn2 Sn1 169.075(19) 45_665 11 Sn2 Sn2 Sn1 133.944(10) 9 11 Sn2 Sn2 Sn1 80.151(10) 5 11 Na3 Sn2 Sn1 70.91(4) 4 11 Na3 Sn2 Sn1 109.54(11) 3 11 Sn3 Sn2 Sn1 51.242(14) 3 11 Sn3 Sn2 Sn1 95.533(14) 4 11 Sn1 Sn2 Sn1 119.764(19) 46_656 11 Cu2 Sn3 Cu2 61.81(6) 34 30 Cu2 Sn3 Cu2 61.81(6) 34 26 Cu2 Sn3 Cu2 61.81(6) 30 26 Cu2 Sn3 Sn2 56.56(2) 34 . Cu2 Sn3 Sn2 56.56(2) 30 . Cu2 Sn3 Sn2 106.63(5) 26 . Cu2 Sn3 Sn2 106.63(5) 34 9 Cu2 Sn3 Sn2 56.56(2) 30 9 Cu2 Sn3 Sn2 56.56(2) 26 9 Sn2 Sn3 Sn2 109.20(3) . 9 Cu2 Sn3 Sn2 56.56(2) 34 5 Cu2 Sn3 Sn2 106.63(5) 30 5 Cu2 Sn3 Sn2 56.56(2) 26 5 Sn2 Sn3 Sn2 109.20(3) . 5 Sn2 Sn3 Sn2 109.20(3) 9 5 Cu2 Sn3 Na3 106.37(16) 34 4 Cu2 Sn3 Na3 165.8(2) 30 4 Cu2 Sn3 Na3 106.37(16) 26 4 Sn2 Sn3 Na3 125.315(19) . 4 Sn2 Sn3 Na3 125.32(2) 9 4 Sn2 Sn3 Na3 59.15(19) 5 4 Cu2 Sn3 Na3 165.8(2) 34 3 Cu2 Sn3 Na3 106.37(16) 30 3 Cu2 Sn3 Na3 106.37(16) 26 3 Sn2 Sn3 Na3 125.32(2) . 3 Sn2 Sn3 Na3 59.15(19) 9 3 Sn2 Sn3 Na3 125.32(2) 5 3 Na3 Sn3 Na3 84.0(3) 4 3 Cu2 Sn3 Na3 106.37(16) 34 2 Cu2 Sn3 Na3 106.37(16) 30 2 Cu2 Sn3 Na3 165.8(2) 26 2 Sn2 Sn3 Na3 59.15(19) . 2 Sn2 Sn3 Na3 125.32(2) 9 2 Sn2 Sn3 Na3 125.32(2) 5 2 Na3 Sn3 Na3 84.0(3) 4 2 Na3 Sn3 Na3 84.0(3) 3 2 Cu2 Sn3 Na2 111.70(8) 34 10 Cu2 Sn3 Na2 111.70(8) 30 10 Cu2 Sn3 Na2 58.93(10) 26 10 Sn2 Sn3 Na2 165.56(11) . 10 Sn2 Sn3 Na2 64.06(4) 9 10 Sn2 Sn3 Na2 64.06(4) 5 10 Na3 Sn3 Na2 63.68(8) 4 10 Na3 Sn3 Na2 63.68(8) 3 10 Na3 Sn3 Na2 135.3(2) 2 10 Cu2 Sn3 Na2 58.93(10) 34 6 Cu2 Sn3 Na2 111.70(9) 30 6 Cu2 Sn3 Na2 111.70(8) 26 6 Sn2 Sn3 Na2 64.06(4) . 6 Sn2 Sn3 Na2 165.56(11) 9 6 Sn2 Sn3 Na2 64.06(4) 5 6 Na3 Sn3 Na2 63.68(8) 4 6 Na3 Sn3 Na2 135.3(2) 3 6 Na3 Sn3 Na2 63.68(8) 2 6 Na2 Sn3 Na2 119.16(3) 10 6 Cu2 Sn3 Na2 111.70(9) 34 2 Cu2 Sn3 Na2 58.93(10) 30 2 Cu2 Sn3 Na2 111.70(9) 26 2 Sn2 Sn3 Na2 64.06(4) . 2 Sn2 Sn3 Na2 64.06(4) 9 2 Sn2 Sn3 Na2 165.56(11) 5 2 Na3 Sn3 Na2 135.3(2) 4 2 Na3 Sn3 Na2 63.68(8) 3 2 Na3 Sn3 Na2 63.68(8) 2 2 Na2 Sn3 Na2 119.16(3) 10 2 Na2 Sn3 Na2 119.16(3) 6 2 Cu2 Sn3 Sn4 36.38(4) 34 . Cu2 Sn3 Sn4 36.38(4) 30 . Cu2 Sn3 Sn4 36.38(4) 26 . Sn2 Sn3 Sn4 70.26(3) . . Sn2 Sn3 Sn4 70.26(3) 9 . Sn2 Sn3 Sn4 70.26(3) 5 . Na3 Sn3 Sn4 129.40(19) 4 . Na3 Sn3 Sn4 129.40(19) 3 . Na3 Sn3 Sn4 129.40(19) 2 . Na2 Sn3 Sn4 95.30(10) 10 . Na2 Sn3 Sn4 95.30(10) 6 . Na2 Sn3 Sn4 95.30(10) 2 . Cu2 Sn3 Cu1 70.74(5) 34 10 Cu2 Sn3 Cu1 33.69(2) 30 10 Cu2 Sn3 Cu1 33.69(2) 26 10 Sn2 Sn3 Cu1 89.24(3) . 10 Sn2 Sn3 Cu1 35.89(3) 9 10 Sn2 Sn3 Cu1 89.24(3) 5 10 Na3 Sn3 Cu1 137.91(13) 4 10 Na3 Sn3 Cu1 95.04(19) 3 10 Na3 Sn3 Cu1 137.91(13) 2 10 Na2 Sn3 Cu1 78.19(8) 10 10 Na2 Sn3 Cu1 129.67(10) 6 10 Na2 Sn3 Cu1 78.19(8) 2 10 Sn4 Sn3 Cu1 34.36(2) . 10 Cu2 Sn3 Cu1 33.69(2) 34 6 Cu2 Sn3 Cu1 70.74(5) 30 6 Cu2 Sn3 Cu1 33.69(2) 26 6 Sn2 Sn3 Cu1 89.24(3) . 6 Sn2 Sn3 Cu1 89.24(3) 9 6 Sn2 Sn3 Cu1 35.89(3) 5 6 Na3 Sn3 Cu1 95.04(19) 4 6 Na3 Sn3 Cu1 137.91(13) 3 6 Na3 Sn3 Cu1 137.91(13) 2 6 Na2 Sn3 Cu1 78.19(8) 10 6 Na2 Sn3 Cu1 78.19(8) 6 6 Na2 Sn3 Cu1 129.67(10) 2 6 Sn4 Sn3 Cu1 34.36(2) . 6 Cu1 Sn3 Cu1 58.52(3) 10 6 Cu2 Sn3 Cu1 33.69(2) 34 2 Cu2 Sn3 Cu1 33.69(2) 30 2 Cu2 Sn3 Cu1 70.74(5) 26 2 Sn2 Sn3 Cu1 35.89(3) . 2 Sn2 Sn3 Cu1 89.24(3) 9 2 Sn2 Sn3 Cu1 89.24(3) 5 2 Na3 Sn3 Cu1 137.91(13) 4 2 Na3 Sn3 Cu1 137.91(13) 3 2 Na3 Sn3 Cu1 95.04(19) 2 2 Na2 Sn3 Cu1 129.67(10) 10 2 Na2 Sn3 Cu1 78.19(8) 6 2 Na2 Sn3 Cu1 78.19(8) 2 2 Sn4 Sn3 Cu1 34.36(2) . 2 Cu1 Sn3 Cu1 58.52(3) 10 2 Cu1 Sn3 Cu1 58.52(3) 6 2 Cu2 Sn3 Sn3 145.956(16) 34 4 Cu2 Sn3 Sn3 108.36(4) 30 4 Cu2 Sn3 Sn3 145.956(16) 26 4 Sn2 Sn3 Sn3 90.24(2) . 4 Sn2 Sn3 Sn3 90.24(2) 9 4 Sn2 Sn3 Sn3 145.01(3) 5 4 Na3 Sn3 Sn3 85.86(19) 4 4 Na3 Sn3 Sn3 42.15(13) 3 4 Na3 Sn3 Sn3 42.15(13) 2 4 Na2 Sn3 Sn3 102.24(8) 10 4 Na2 Sn3 Sn3 102.24(8) 6 4 Na2 Sn3 Sn3 49.43(10) 2 4 Sn4 Sn3 Sn3 144.7 . 4 Cu1 Sn3 Sn3 120.734(17) 10 4 Cu1 Sn3 Sn3 179.10(2) 6 4 Cu1 Sn3 Sn3 120.734(17) 2 4 Cu2 Sn3 Sn3 108.36(4) 34 3 Cu2 Sn3 Sn3 145.956(16) 30 3 Cu2 Sn3 Sn3 145.956(16) 26 3 Sn2 Sn3 Sn3 90.24(2) . 3 Sn2 Sn3 Sn3 145.01(3) 9 3 Sn2 Sn3 Sn3 90.24(2) 5 3 Na3 Sn3 Sn3 42.15(13) 4 3 Na3 Sn3 Sn3 85.86(19) 3 3 Na3 Sn3 Sn3 42.15(13) 2 3 Na2 Sn3 Sn3 102.24(8) 10 3 Na2 Sn3 Sn3 49.43(10) 6 3 Na2 Sn3 Sn3 102.24(8) 2 3 Sn4 Sn3 Sn3 144.7 . 3 Cu1 Sn3 Sn3 179.10(2) 10 3 Cu1 Sn3 Sn3 120.734(17) 6 3 Cu1 Sn3 Sn3 120.734(17) 2 3 Sn3 Sn3 Sn3 60.0 4 3 Cu2 Sn3 Sn3 145.956(16) 34 2 Cu2 Sn3 Sn3 145.956(16) 30 2 Cu2 Sn3 Sn3 108.36(4) 26 2 Sn2 Sn3 Sn3 145.01(3) . 2 Sn2 Sn3 Sn3 90.24(2) 9 2 Sn2 Sn3 Sn3 90.24(2) 5 2 Na3 Sn3 Sn3 42.15(13) 4 2 Na3 Sn3 Sn3 42.15(13) 3 2 Na3 Sn3 Sn3 85.86(19) 2 2 Na2 Sn3 Sn3 49.43(10) 10 2 Na2 Sn3 Sn3 102.24(8) 6 2 Na2 Sn3 Sn3 102.24(8) 2 2 Sn4 Sn3 Sn3 144.7 . 2 Cu1 Sn3 Sn3 120.734(17) 10 2 Cu1 Sn3 Sn3 120.734(17) 6 2 Cu1 Sn3 Sn3 179.10(2) 2 2 Sn3 Sn3 Sn3 60.0 4 2 Sn3 Sn3 Sn3 60.0 3 2 Cu2 Sn3 Sn1 67.03(2) 34 39_656 Cu2 Sn3 Sn1 86.09(4) 30 39_656 Cu2 Sn3 Sn1 24.80(2) 26 39_656 Sn2 Sn3 Sn1 121.80(4) . 39_656 Sn2 Sn3 Sn1 72.872(19) 9 39_656 Sn2 Sn3 Sn1 36.335(14) 5 39_656 Na3 Sn3 Sn1 81.63(16) 4 39_656 Na3 Sn3 Sn1 105.91(10) 3 39_656 Na3 Sn3 Sn1 161.52(3) 2 39_656 Na2 Sn3 Sn1 44.99(9) 10 39_656 Na2 Sn3 Sn1 99.31(6) 6 39_656 Na2 Sn3 Sn1 134.62(7) 2 39_656 Sn4 Sn3 Sn1 55.558(15) . 39_656 Cu1 Sn3 Sn1 58.069(16) 10 39_656 Cu1 Sn3 Sn1 33.345(12) 6 39_656 Cu1 Sn3 Sn1 87.92(3) 2 39_656 Sn3 Sn3 Sn1 147.007(13) 4 39_656 Sn3 Sn3 Sn1 121.684(12) 3 39_656 Sn3 Sn3 Sn1 91.225(15) 2 39_656 Cu2 Sn3 Sn1 24.80(2) 34 42_566 Cu2 Sn3 Sn1 67.03(2) 30 42_566 Cu2 Sn3 Sn1 86.09(4) 26 42_566 Sn2 Sn3 Sn1 36.335(14) . 42_566 Sn2 Sn3 Sn1 121.80(4) 9 42_566 Sn2 Sn3 Sn1 72.872(19) 5 42_566 Na3 Sn3 Sn1 105.91(10) 4 42_566 Na3 Sn3 Sn1 161.52(3) 3 42_566 Na3 Sn3 Sn1 81.63(16) 2 42_566 Na2 Sn3 Sn1 134.62(7) 10 42_566 Na2 Sn3 Sn1 44.99(9) 6 42_566 Na2 Sn3 Sn1 99.31(6) 2 42_566 Sn4 Sn3 Sn1 55.558(15) . 42_566 Cu1 Sn3 Sn1 87.92(3) 10 42_566 Cu1 Sn3 Sn1 58.069(16) 6 42_566 Cu1 Sn3 Sn1 33.345(12) 2 42_566 Sn3 Sn3 Sn1 121.684(12) 4 42_566 Sn3 Sn3 Sn1 91.225(15) 3 42_566 Sn3 Sn3 Sn1 147.007(13) 2 42_566 Sn1 Sn3 Sn1 91.16(2) 39_656 42_566 Cu2 Sn3 Sn1 86.09(4) 34 45_665 Cu2 Sn3 Sn1 24.80(2) 30 45_665 Cu2 Sn3 Sn1 67.03(2) 26 45_665 Sn2 Sn3 Sn1 72.872(19) . 45_665 Sn2 Sn3 Sn1 36.335(14) 9 45_665 Sn2 Sn3 Sn1 121.80(4) 5 45_665 Na3 Sn3 Sn1 161.52(3) 4 45_665 Na3 Sn3 Sn1 81.63(16) 3 45_665 Na3 Sn3 Sn1 105.91(10) 2 45_665 Na2 Sn3 Sn1 99.31(6) 10 45_665 Na2 Sn3 Sn1 134.62(7) 6 45_665 Na2 Sn3 Sn1 44.99(9) 2 45_665 Sn4 Sn3 Sn1 55.558(15) . 45_665 Cu1 Sn3 Sn1 33.345(12) 10 45_665 Cu1 Sn3 Sn1 87.92(3) 6 45_665 Cu1 Sn3 Sn1 58.069(16) 2 45_665 Sn3 Sn3 Sn1 91.225(15) 4 45_665 Sn3 Sn3 Sn1 147.007(13) 3 45_665 Sn3 Sn3 Sn1 121.684(12) 2 45_665 Sn1 Sn3 Sn1 91.16(2) 39_656 45_665 Sn1 Sn3 Sn1 91.16(2) 42_566 45_665 Cu2 Sn3 Sn1 67.03(2) 34 8 Cu2 Sn3 Sn1 24.80(2) 30 8 Cu2 Sn3 Sn1 86.09(4) 26 8 Sn2 Sn3 Sn1 36.335(14) . 8 Sn2 Sn3 Sn1 72.872(19) 9 8 Sn2 Sn3 Sn1 121.80(4) 5 8 Na3 Sn3 Sn1 161.52(3) 4 8 Na3 Sn3 Sn1 105.91(10) 3 8 Na3 Sn3 Sn1 81.63(16) 2 8 Na2 Sn3 Sn1 134.62(7) 10 8 Na2 Sn3 Sn1 99.31(6) 6 8 Na2 Sn3 Sn1 44.99(9) 2 8 Sn4 Sn3 Sn1 55.558(15) . 8 Cu1 Sn3 Sn1 58.069(16) 10 8 Cu1 Sn3 Sn1 87.92(3) 6 8 Cu1 Sn3 Sn1 33.345(12) 2 8 Sn3 Sn3 Sn1 91.225(15) 4 8 Sn3 Sn3 Sn1 121.684(12) 3 8 Sn3 Sn3 Sn1 147.007(13) 2 8 Sn1 Sn3 Sn1 109.64(3) 39_656 8 Sn1 Sn3 Sn1 60.510(18) 42_566 8 Sn1 Sn3 Sn1 36.540(15) 45_665 8 Cu2 Sn3 Sn1 24.80(2) 34 12 Cu2 Sn3 Sn1 86.09(4) 30 12 Cu2 Sn3 Sn1 67.03(2) 26 12 Sn2 Sn3 Sn1 72.872(19) . 12 Sn2 Sn3 Sn1 121.80(4) 9 12 Sn2 Sn3 Sn1 36.335(14) 5 12 Na3 Sn3 Sn1 81.63(16) 4 12 Na3 Sn3 Sn1 161.52(3) 3 12 Na3 Sn3 Sn1 105.91(10) 2 12 Na2 Sn3 Sn1 99.31(6) 10 12 Na2 Sn3 Sn1 44.99(9) 6 12 Na2 Sn3 Sn1 134.62(7) 2 12 Sn4 Sn3 Sn1 55.558(15) . 12 Cu1 Sn3 Sn1 87.92(3) 10 12 Cu1 Sn3 Sn1 33.345(12) 6 12 Cu1 Sn3 Sn1 58.069(16) 2 12 Sn3 Sn3 Sn1 147.007(13) 4 12 Sn3 Sn3 Sn1 91.225(15) 3 12 Sn3 Sn3 Sn1 121.684(12) 2 12 Sn1 Sn3 Sn1 60.510(18) 39_656 12 Sn1 Sn3 Sn1 36.540(15) 42_566 12 Sn1 Sn3 Sn1 109.64(3) 45_665 12 Sn1 Sn3 Sn1 91.16(2) 8 12 Cu2 Sn3 Sn1 86.09(4) 34 4 Cu2 Sn3 Sn1 67.03(2) 30 4 Cu2 Sn3 Sn1 24.80(2) 26 4 Sn2 Sn3 Sn1 121.80(4) . 4 Sn2 Sn3 Sn1 36.335(14) 9 4 Sn2 Sn3 Sn1 72.872(19) 5 4 Na3 Sn3 Sn1 105.91(10) 4 4 Na3 Sn3 Sn1 81.63(16) 3 4 Na3 Sn3 Sn1 161.52(3) 2 4 Na2 Sn3 Sn1 44.99(9) 10 4 Na2 Sn3 Sn1 134.62(7) 6 4 Na2 Sn3 Sn1 99.31(6) 2 4 Sn4 Sn3 Sn1 55.558(15) . 4 Cu1 Sn3 Sn1 33.345(12) 10 4 Cu1 Sn3 Sn1 58.069(16) 6 4 Cu1 Sn3 Sn1 87.92(3) 2 4 Sn3 Sn3 Sn1 121.684(12) 4 4 Sn3 Sn3 Sn1 147.007(13) 3 4 Sn3 Sn3 Sn1 91.225(15) 2 4 Sn1 Sn3 Sn1 36.540(15) 39_656 4 Sn1 Sn3 Sn1 109.64(3) 42_566 4 Sn1 Sn3 Sn1 60.510(18) 45_665 4 Sn1 Sn3 Sn1 91.16(2) 8 4 Sn1 Sn3 Sn1 91.16(2) 12 4 Cu2 Sn3 Na3 143.62(4) 34 . Cu2 Sn3 Na3 143.62(4) 30 . Cu2 Sn3 Na3 143.62(4) 26 . Sn2 Sn3 Na3 109.74(3) . . Sn2 Sn3 Na3 109.74(3) 9 . Sn2 Sn3 Na3 109.74(3) 5 . Na3 Sn3 Na3 50.60(19) 4 . Na3 Sn3 Na3 50.60(19) 3 . Na3 Sn3 Na3 50.60(19) 2 . Na2 Sn3 Na3 84.70(10) 10 . Na2 Sn3 Na3 84.70(10) 6 . Na2 Sn3 Na3 84.70(10) 2 . Sn4 Sn3 Na3 180.00(7) . . Cu1 Sn3 Na3 145.64(2) 10 . Cu1 Sn3 Na3 145.64(2) 6 . Cu1 Sn3 Na3 145.64(2) 2 . Sn3 Sn3 Na3 35.3 4 . Sn3 Sn3 Na3 35.3 3 . Sn3 Sn3 Na3 35.3 2 . Sn1 Sn3 Na3 124.442(15) 39_656 . Sn1 Sn3 Na3 124.442(15) 42_566 . Sn1 Sn3 Na3 124.442(15) 45_665 . Sn1 Sn3 Na3 124.442(15) 8 . Sn1 Sn3 Na3 124.442(15) 12 . Sn1 Sn3 Na3 124.442(15) 4 . Cu2 Sn3 Sn2 113.239(14) 34 12 Cu2 Sn3 Sn2 148.45(3) 30 12 Cu2 Sn3 Sn2 87.90(3) 26 12 Sn2 Sn3 Sn2 150.183(18) . 12 Sn2 Sn3 Sn2 100.555(8) 9 12 Sn2 Sn3 Sn2 57.11(2) 5 12 Na3 Sn3 Sn2 25.47(4) 4 12 Na3 Sn3 Sn2 72.15(8) 3 12 Na3 Sn3 Sn2 104.80(17) 2 12 Na2 Sn3 Sn2 38.27(7) 10 12 Na2 Sn3 Sn2 86.50(5) 6 12 Na2 Sn3 Sn2 135.01(8) 2 12 Sn4 Sn3 Sn2 120.064(14) . 12 Cu1 Sn3 Sn2 114.955(9) 10 12 Cu1 Sn3 Sn2 89.219(18) 6 12 Cu1 Sn3 Sn2 146.34(2) 2 12 Sn3 Sn3 Sn2 91.600(14) 4 12 Sn3 Sn3 Sn2 65.318(10) 3 12 Sn3 Sn3 Sn2 33.130(13) 2 12 Sn1 Sn3 Sn2 65.019(9) 39_656 12 Sn1 Sn3 Sn2 122.909(11) 42_566 12 Sn1 Sn3 Sn2 136.803(9) 45_665 12 Sn1 Sn3 Sn2 172.857(17) 8 12 Sn1 Sn3 Sn2 90.043(11) 12 12 Sn1 Sn3 Sn2 81.779(8) 4 12 Na3 Sn3 Sn2 59.936(14) . 12 Cu2 Sn3 Sn2 148.45(3) 34 7 Cu2 Sn3 Sn2 113.239(14) 30 7 Cu2 Sn3 Sn2 87.90(3) 26 7 Sn2 Sn3 Sn2 150.183(18) . 7 Sn2 Sn3 Sn2 57.11(2) 9 7 Sn2 Sn3 Sn2 100.555(8) 5 7 Na3 Sn3 Sn2 72.15(8) 4 7 Na3 Sn3 Sn2 25.47(4) 3 7 Na3 Sn3 Sn2 104.80(17) 2 7 Na2 Sn3 Sn2 38.27(7) 10 7 Na2 Sn3 Sn2 135.01(8) 6 7 Na2 Sn3 Sn2 86.50(5) 2 7 Sn4 Sn3 Sn2 120.064(14) . 7 Cu1 Sn3 Sn2 89.219(18) 10 7 Cu1 Sn3 Sn2 114.955(9) 6 7 Cu1 Sn3 Sn2 146.34(2) 2 7 Sn3 Sn3 Sn2 65.318(10) 4 7 Sn3 Sn3 Sn2 91.600(14) 3 7 Sn3 Sn3 Sn2 33.130(13) 2 7 Sn1 Sn3 Sn2 81.779(8) 39_656 7 Sn1 Sn3 Sn2 172.857(17) 42_566 7 Sn1 Sn3 Sn2 90.043(11) 45_665 7 Sn1 Sn3 Sn2 122.909(11) 8 7 Sn1 Sn3 Sn2 136.803(9) 12 7 Sn1 Sn3 Sn2 65.019(9) 4 7 Na3 Sn3 Sn2 59.936(14) . 7 Sn2 Sn3 Sn2 52.910(18) 12 7 Cu2 Sn3 Sn2 148.45(3) 34 4 Cu2 Sn3 Sn2 87.90(3) 30 4 Cu2 Sn3 Sn2 113.239(14) 26 4 Sn2 Sn3 Sn2 100.555(8) . 4 Sn2 Sn3 Sn2 57.11(2) 9 4 Sn2 Sn3 Sn2 150.183(18) 5 4 Na3 Sn3 Sn2 104.80(17) 4 4 Na3 Sn3 Sn2 25.47(4) 3 4 Na3 Sn3 Sn2 72.15(8) 2 4 Na2 Sn3 Sn2 86.50(5) 10 4 Na2 Sn3 Sn2 135.01(8) 6 4 Na2 Sn3 Sn2 38.27(7) 2 4 Sn4 Sn3 Sn2 120.064(14) . 4 Cu1 Sn3 Sn2 89.219(18) 10 4 Cu1 Sn3 Sn2 146.34(2) 6 4 Cu1 Sn3 Sn2 114.955(9) 2 4 Sn3 Sn3 Sn2 33.130(13) 4 4 Sn3 Sn3 Sn2 91.600(14) 3 4 Sn3 Sn3 Sn2 65.318(10) 2 4 Sn1 Sn3 Sn2 122.909(11) 39_656 4 Sn1 Sn3 Sn2 136.803(9) 42_566 4 Sn1 Sn3 Sn2 65.019(9) 45_665 4 Sn1 Sn3 Sn2 81.779(8) 8 4 Sn1 Sn3 Sn2 172.857(17) 12 4 Sn1 Sn3 Sn2 90.043(11) 4 4 Na3 Sn3 Sn2 59.936(14) . 4 Sn2 Sn3 Sn2 97.097(18) 12 4 Sn2 Sn3 Sn2 49.649(13) 7 4 Cu2 Sn3 Sn2 87.90(3) 34 3 Cu2 Sn3 Sn2 148.45(3) 30 3 Cu2 Sn3 Sn2 113.239(14) 26 3 Sn2 Sn3 Sn2 100.555(9) . 3 Sn2 Sn3 Sn2 150.183(18) 9 3 Sn2 Sn3 Sn2 57.11(2) 5 3 Na3 Sn3 Sn2 25.47(4) 4 3 Na3 Sn3 Sn2 104.80(17) 3 3 Na3 Sn3 Sn2 72.15(8) 2 3 Na2 Sn3 Sn2 86.50(5) 10 3 Na2 Sn3 Sn2 38.27(7) 6 3 Na2 Sn3 Sn2 135.01(8) 2 3 Sn4 Sn3 Sn2 120.064(14) . 3 Cu1 Sn3 Sn2 146.34(2) 10 3 Cu1 Sn3 Sn2 89.219(18) 6 3 Cu1 Sn3 Sn2 114.955(9) 2 3 Sn3 Sn3 Sn2 91.600(14) 4 3 Sn3 Sn3 Sn2 33.130(13) 3 3 Sn3 Sn3 Sn2 65.318(10) 2 3 Sn1 Sn3 Sn2 90.043(11) 39_656 3 Sn1 Sn3 Sn2 81.779(8) 42_566 3 Sn1 Sn3 Sn2 172.857(17) 45_665 3 Sn1 Sn3 Sn2 136.803(9) 8 3 Sn1 Sn3 Sn2 65.019(9) 12 3 Sn1 Sn3 Sn2 122.909(11) 4 3 Na3 Sn3 Sn2 59.936(14) . 3 Sn2 Sn3 Sn2 49.649(13) 12 3 Sn2 Sn3 Sn2 97.097(18) 7 3 Sn2 Sn3 Sn2 119.84(3) 4 3 Cu2 Sn4 Cu2 180.00(6) 34 10 Cu2 Sn4 Cu2 64.10(5) 34 30 Cu2 Sn4 Cu2 115.90(5) 10 30 Cu2 Sn4 Cu2 115.90(5) 34 6 Cu2 Sn4 Cu2 64.10(5) 10 6 Cu2 Sn4 Cu2 180.00(6) 30 6 Cu2 Sn4 Cu2 64.10(5) 34 26 Cu2 Sn4 Cu2 115.90(5) 10 26 Cu2 Sn4 Cu2 64.10(5) 30 26 Cu2 Sn4 Cu2 115.90(5) 6 26 Cu2 Sn4 Cu2 115.90(5) 34 2 Cu2 Sn4 Cu2 64.10(5) 10 2 Cu2 Sn4 Cu2 115.90(5) 30 2 Cu2 Sn4 Cu2 64.10(5) 6 2 Cu2 Sn4 Cu2 180.00(6) 26 2 Cu2 Sn4 Cu1 62.82(5) 34 34 Cu2 Sn4 Cu1 117.18(5) 10 34 Cu2 Sn4 Cu1 116.53(3) 30 34 Cu2 Sn4 Cu1 63.47(3) 6 34 Cu2 Sn4 Cu1 116.53(3) 26 34 Cu2 Sn4 Cu1 63.47(3) 2 34 Cu2 Sn4 Cu1 117.18(5) 34 10 Cu2 Sn4 Cu1 62.82(5) 10 10 Cu2 Sn4 Cu1 63.47(3) 30 10 Cu2 Sn4 Cu1 116.53(3) 6 10 Cu2 Sn4 Cu1 63.47(3) 26 10 Cu2 Sn4 Cu1 116.53(3) 2 10 Cu1 Sn4 Cu1 180.00(9) 34 10 Cu2 Sn4 Cu1 116.53(3) 34 30 Cu2 Sn4 Cu1 63.47(3) 10 30 Cu2 Sn4 Cu1 62.82(5) 30 30 Cu2 Sn4 Cu1 117.18(5) 6 30 Cu2 Sn4 Cu1 116.53(3) 26 30 Cu2 Sn4 Cu1 63.47(3) 2 30 Cu1 Sn4 Cu1 116.687(19) 34 30 Cu1 Sn4 Cu1 63.313(19) 10 30 Cu2 Sn4 Cu1 63.47(3) 34 6 Cu2 Sn4 Cu1 116.53(3) 10 6 Cu2 Sn4 Cu1 117.18(5) 30 6 Cu2 Sn4 Cu1 62.82(5) 6 6 Cu2 Sn4 Cu1 63.47(3) 26 6 Cu2 Sn4 Cu1 116.53(3) 2 6 Cu1 Sn4 Cu1 63.313(19) 34 6 Cu1 Sn4 Cu1 116.687(19) 10 6 Cu1 Sn4 Cu1 180.00(9) 30 6 Cu2 Sn4 Cu1 116.53(3) 34 26 Cu2 Sn4 Cu1 63.47(3) 10 26 Cu2 Sn4 Cu1 116.53(3) 30 26 Cu2 Sn4 Cu1 63.47(3) 6 26 Cu2 Sn4 Cu1 62.82(5) 26 26 Cu2 Sn4 Cu1 117.18(5) 2 26 Cu1 Sn4 Cu1 116.687(19) 34 26 Cu1 Sn4 Cu1 63.313(19) 10 26 Cu1 Sn4 Cu1 116.687(19) 30 26 Cu1 Sn4 Cu1 63.313(19) 6 26 Cu2 Sn4 Cu1 63.47(3) 34 2 Cu2 Sn4 Cu1 116.53(3) 10 2 Cu2 Sn4 Cu1 63.47(3) 30 2 Cu2 Sn4 Cu1 116.53(3) 6 2 Cu2 Sn4 Cu1 117.18(5) 26 2 Cu2 Sn4 Cu1 62.82(5) 2 2 Cu1 Sn4 Cu1 63.313(19) 34 2 Cu1 Sn4 Cu1 116.687(19) 10 2 Cu1 Sn4 Cu1 63.313(19) 30 2 Cu1 Sn4 Cu1 116.687(19) 6 2 Cu1 Sn4 Cu1 180.00(9) 26 2 Cu2 Sn4 Sn3 142.21(3) 34 25 Cu2 Sn4 Sn3 37.79(3) 10 25 Cu2 Sn4 Sn3 142.21(3) 30 25 Cu2 Sn4 Sn3 37.79(3) 6 25 Cu2 Sn4 Sn3 142.21(3) 26 25 Cu2 Sn4 Sn3 37.79(3) 2 25 Cu1 Sn4 Sn3 79.39(3) 34 25 Cu1 Sn4 Sn3 100.61(3) 10 25 Cu1 Sn4 Sn3 79.39(3) 30 25 Cu1 Sn4 Sn3 100.61(3) 6 25 Cu1 Sn4 Sn3 79.39(3) 26 25 Cu1 Sn4 Sn3 100.61(3) 2 25 Cu2 Sn4 Sn3 37.79(3) 34 . Cu2 Sn4 Sn3 142.21(3) 10 . Cu2 Sn4 Sn3 37.79(3) 30 . Cu2 Sn4 Sn3 142.21(3) 6 . Cu2 Sn4 Sn3 37.79(3) 26 . Cu2 Sn4 Sn3 142.21(3) 2 . Cu1 Sn4 Sn3 100.61(3) 34 . Cu1 Sn4 Sn3 79.39(3) 10 . Cu1 Sn4 Sn3 100.61(3) 30 . Cu1 Sn4 Sn3 79.39(3) 6 . Cu1 Sn4 Sn3 100.61(3) 26 . Cu1 Sn4 Sn3 79.39(3) 2 . Sn3 Sn4 Sn3 180.0 25 . Cu2 Sn4 Sn2 37.892(11) 34 . Cu2 Sn4 Sn2 142.108(11) 10 . Cu2 Sn4 Sn2 37.892(11) 30 . Cu2 Sn4 Sn2 142.108(11) 6 . Cu2 Sn4 Sn2 80.38(3) 26 . Cu2 Sn4 Sn2 99.62(3) 2 . Cu1 Sn4 Sn2 78.64(3) 34 . Cu1 Sn4 Sn2 101.36(3) 10 . Cu1 Sn4 Sn2 78.64(3) 30 . Cu1 Sn4 Sn2 101.36(3) 6 . Cu1 Sn4 Sn2 143.20(3) 26 . Cu1 Sn4 Sn2 36.80(3) 2 . Sn3 Sn4 Sn2 137.415(11) 25 . Sn3 Sn4 Sn2 42.585(11) . . Cu2 Sn4 Sn2 142.108(11) 34 25 Cu2 Sn4 Sn2 37.892(11) 10 25 Cu2 Sn4 Sn2 142.108(11) 30 25 Cu2 Sn4 Sn2 37.892(11) 6 25 Cu2 Sn4 Sn2 99.62(3) 26 25 Cu2 Sn4 Sn2 80.38(3) 2 25 Cu1 Sn4 Sn2 101.36(3) 34 25 Cu1 Sn4 Sn2 78.64(3) 10 25 Cu1 Sn4 Sn2 101.36(3) 30 25 Cu1 Sn4 Sn2 78.64(3) 6 25 Cu1 Sn4 Sn2 36.80(3) 26 25 Cu1 Sn4 Sn2 143.20(3) 2 25 Sn3 Sn4 Sn2 42.586(11) 25 25 Sn3 Sn4 Sn2 137.414(11) . 25 Sn2 Sn4 Sn2 180.0 . 25 Cu2 Sn4 Sn2 37.892(11) 34 5 Cu2 Sn4 Sn2 142.108(11) 10 5 Cu2 Sn4 Sn2 80.38(3) 30 5 Cu2 Sn4 Sn2 99.62(3) 6 5 Cu2 Sn4 Sn2 37.892(11) 26 5 Cu2 Sn4 Sn2 142.108(11) 2 5 Cu1 Sn4 Sn2 78.64(3) 34 5 Cu1 Sn4 Sn2 101.36(3) 10 5 Cu1 Sn4 Sn2 143.20(3) 30 5 Cu1 Sn4 Sn2 36.80(3) 6 5 Cu1 Sn4 Sn2 78.64(3) 26 5 Cu1 Sn4 Sn2 101.36(3) 2 5 Sn3 Sn4 Sn2 137.414(11) 25 5 Sn3 Sn4 Sn2 42.586(11) . 5 Sn2 Sn4 Sn2 71.752(18) . 5 Sn2 Sn4 Sn2 108.247(18) 25 5 Cu2 Sn4 Sn2 142.108(11) 34 29 Cu2 Sn4 Sn2 37.892(11) 10 29 Cu2 Sn4 Sn2 99.62(3) 30 29 Cu2 Sn4 Sn2 80.38(3) 6 29 Cu2 Sn4 Sn2 142.108(11) 26 29 Cu2 Sn4 Sn2 37.892(11) 2 29 Cu1 Sn4 Sn2 101.36(3) 34 29 Cu1 Sn4 Sn2 78.64(3) 10 29 Cu1 Sn4 Sn2 36.80(3) 30 29 Cu1 Sn4 Sn2 143.20(3) 6 29 Cu1 Sn4 Sn2 101.36(3) 26 29 Cu1 Sn4 Sn2 78.64(3) 2 29 Sn3 Sn4 Sn2 42.586(11) 25 29 Sn3 Sn4 Sn2 137.414(11) . 29 Sn2 Sn4 Sn2 108.248(18) . 29 Sn2 Sn4 Sn2 71.753(18) 25 29 Sn2 Sn4 Sn2 180.000(15) 5 29 Cu2 Sn4 Sn2 80.38(3) 34 9 Cu2 Sn4 Sn2 99.62(3) 10 9 Cu2 Sn4 Sn2 37.892(11) 30 9 Cu2 Sn4 Sn2 142.108(11) 6 9 Cu2 Sn4 Sn2 37.892(11) 26 9 Cu2 Sn4 Sn2 142.108(11) 2 9 Cu1 Sn4 Sn2 143.20(3) 34 9 Cu1 Sn4 Sn2 36.80(3) 10 9 Cu1 Sn4 Sn2 78.64(3) 30 9 Cu1 Sn4 Sn2 101.36(3) 6 9 Cu1 Sn4 Sn2 78.64(3) 26 9 Cu1 Sn4 Sn2 101.36(3) 2 9 Sn3 Sn4 Sn2 137.414(11) 25 9 Sn3 Sn4 Sn2 42.586(11) . 9 Sn2 Sn4 Sn2 71.752(18) . 9 Sn2 Sn4 Sn2 108.247(18) 25 9 Sn2 Sn4 Sn2 71.753(18) 5 9 Sn2 Sn4 Sn2 108.247(18) 29 9 Cu2 Sn4 Sn2 99.62(3) 34 33 Cu2 Sn4 Sn2 80.38(3) 10 33 Cu2 Sn4 Sn2 142.108(11) 30 33 Cu2 Sn4 Sn2 37.892(11) 6 33 Cu2 Sn4 Sn2 142.108(11) 26 33 Cu2 Sn4 Sn2 37.892(11) 2 33 Cu1 Sn4 Sn2 36.80(3) 34 33 Cu1 Sn4 Sn2 143.20(3) 10 33 Cu1 Sn4 Sn2 101.36(3) 30 33 Cu1 Sn4 Sn2 78.64(3) 6 33 Cu1 Sn4 Sn2 101.36(3) 26 33 Cu1 Sn4 Sn2 78.64(3) 2 33 Sn3 Sn4 Sn2 42.586(11) 25 33 Sn3 Sn4 Sn2 137.414(11) . 33 Sn2 Sn4 Sn2 108.248(18) . 33 Sn2 Sn4 Sn2 71.753(18) 25 33 Sn2 Sn4 Sn2 108.247(18) 5 33 Sn2 Sn4 Sn2 71.753(18) 29 33 Sn2 Sn4 Sn2 180.000(16) 9 33 Cu2 Sn4 Sn1 78.75(3) 34 21_445 Cu2 Sn4 Sn1 101.25(3) 10 21_445 Cu2 Sn4 Sn1 142.85(3) 30 21_445 Cu2 Sn4 Sn1 37.15(3) 6 21_445 Cu2 Sn4 Sn1 100.687(13) 26 21_445 Cu2 Sn4 Sn1 79.313(13) 2 21_445 Cu1 Sn4 Sn1 37.333(13) 34 21_445 Cu1 Sn4 Sn1 142.667(13) 10 21_445 Cu1 Sn4 Sn1 142.78(3) 30 21_445 Cu1 Sn4 Sn1 37.22(3) 6 21_445 Cu1 Sn4 Sn1 79.355(12) 26 21_445 Cu1 Sn4 Sn1 100.645(12) 2 21_445 Sn3 Sn4 Sn1 70.601(8) 25 21_445 Sn3 Sn4 Sn1 109.399(8) . 21_445 Sn2 Sn4 Sn1 109.245(8) . 21_445 Sn2 Sn4 Sn1 70.755(8) 25 21_445 Sn2 Sn4 Sn1 69.767(13) 5 21_445 Sn2 Sn4 Sn1 110.233(13) 29 21_445 Sn2 Sn4 Sn1 138.577(10) 9 21_445 Sn2 Sn4 Sn1 41.423(10) 33 21_445 Cu2 Sn4 Sn1 37.15(3) 34 42_566 Cu2 Sn4 Sn1 142.85(3) 10 42_566 Cu2 Sn4 Sn1 79.313(13) 30 42_566 Cu2 Sn4 Sn1 100.687(13) 6 42_566 Cu2 Sn4 Sn1 101.25(3) 26 42_566 Cu2 Sn4 Sn1 78.75(3) 2 42_566 Cu1 Sn4 Sn1 37.22(3) 34 42_566 Cu1 Sn4 Sn1 142.78(3) 10 42_566 Cu1 Sn4 Sn1 100.645(12) 30 42_566 Cu1 Sn4 Sn1 79.355(12) 6 42_566 Cu1 Sn4 Sn1 142.667(13) 26 42_566 Cu1 Sn4 Sn1 37.333(13) 2 42_566 Sn3 Sn4 Sn1 109.399(8) 25 42_566 Sn3 Sn4 Sn1 70.601(8) . 42_566 Sn2 Sn4 Sn1 41.423(10) . 42_566 Sn2 Sn4 Sn1 138.577(10) 25 42_566 Sn2 Sn4 Sn1 70.755(8) 5 42_566 Sn2 Sn4 Sn1 109.245(8) 29 42_566 Sn2 Sn4 Sn1 110.233(13) 9 42_566 Sn2 Sn4 Sn1 69.767(13) 33 42_566 Sn1 Sn4 Sn1 70.456(8) 21_445 42_566 Cu2 Sn4 Sn1 142.85(3) 34 18_544 Cu2 Sn4 Sn1 37.15(3) 10 18_544 Cu2 Sn4 Sn1 100.687(13) 30 18_544 Cu2 Sn4 Sn1 79.313(13) 6 18_544 Cu2 Sn4 Sn1 78.75(3) 26 18_544 Cu2 Sn4 Sn1 101.25(3) 2 18_544 Cu1 Sn4 Sn1 142.78(3) 34 18_544 Cu1 Sn4 Sn1 37.22(3) 10 18_544 Cu1 Sn4 Sn1 79.355(12) 30 18_544 Cu1 Sn4 Sn1 100.645(12) 6 18_544 Cu1 Sn4 Sn1 37.333(13) 26 18_544 Cu1 Sn4 Sn1 142.667(13) 2 18_544 Sn3 Sn4 Sn1 70.601(8) 25 18_544 Sn3 Sn4 Sn1 109.399(8) . 18_544 Sn2 Sn4 Sn1 138.577(10) . 18_544 Sn2 Sn4 Sn1 41.423(10) 25 18_544 Sn2 Sn4 Sn1 109.245(8) 5 18_544 Sn2 Sn4 Sn1 70.755(8) 29 18_544 Sn2 Sn4 Sn1 69.767(13) 9 18_544 Sn2 Sn4 Sn1 110.233(13) 33 18_544 Sn1 Sn4 Sn1 109.544(8) 21_445 18_544 Sn1 Sn4 Sn1 180.000(13) 42_566 18_544 Cu2 Sn4 Sn1 79.313(13) 34 39_656 Cu2 Sn4 Sn1 100.687(13) 10 39_656 Cu2 Sn4 Sn1 101.25(3) 30 39_656 Cu2 Sn4 Sn1 78.75(3) 6 39_656 Cu2 Sn4 Sn1 37.15(3) 26 39_656 Cu2 Sn4 Sn1 142.85(3) 2 39_656 Cu1 Sn4 Sn1 100.645(12) 34 39_656 Cu1 Sn4 Sn1 79.355(12) 10 39_656 Cu1 Sn4 Sn1 142.667(13) 30 39_656 Cu1 Sn4 Sn1 37.333(13) 6 39_656 Cu1 Sn4 Sn1 37.22(3) 26 39_656 Cu1 Sn4 Sn1 142.78(3) 2 39_656 Sn3 Sn4 Sn1 109.399(8) 25 39_656 Sn3 Sn4 Sn1 70.601(8) . 39_656 Sn2 Sn4 Sn1 110.232(13) . 39_656 Sn2 Sn4 Sn1 69.767(13) 25 39_656 Sn2 Sn4 Sn1 41.423(10) 5 39_656 Sn2 Sn4 Sn1 138.577(10) 29 39_656 Sn2 Sn4 Sn1 70.755(8) 9 39_656 Sn2 Sn4 Sn1 109.245(8) 33 39_656 Sn1 Sn4 Sn1 70.456(8) 21_445 39_656 Sn1 Sn4 Sn1 109.544(8) 42_566 39_656 Sn1 Sn4 Sn1 70.456(8) 18_544 39_656 Cu2 Sn4 Sn1 100.687(13) 34 15_454 Cu2 Sn4 Sn1 79.313(13) 10 15_454 Cu2 Sn4 Sn1 78.75(3) 30 15_454 Cu2 Sn4 Sn1 101.25(3) 6 15_454 Cu2 Sn4 Sn1 142.85(3) 26 15_454 Cu2 Sn4 Sn1 37.15(3) 2 15_454 Cu1 Sn4 Sn1 79.355(12) 34 15_454 Cu1 Sn4 Sn1 100.645(12) 10 15_454 Cu1 Sn4 Sn1 37.333(13) 30 15_454 Cu1 Sn4 Sn1 142.667(13) 6 15_454 Cu1 Sn4 Sn1 142.78(3) 26 15_454 Cu1 Sn4 Sn1 37.22(3) 2 15_454 Sn3 Sn4 Sn1 70.601(8) 25 15_454 Sn3 Sn4 Sn1 109.399(8) . 15_454 Sn2 Sn4 Sn1 69.768(13) . 15_454 Sn2 Sn4 Sn1 110.233(13) 25 15_454 Sn2 Sn4 Sn1 138.577(10) 5 15_454 Sn2 Sn4 Sn1 41.423(10) 29 15_454 Sn2 Sn4 Sn1 109.245(8) 9 15_454 Sn2 Sn4 Sn1 70.755(8) 33 15_454 Sn1 Sn4 Sn1 109.544(8) 21_445 15_454 Sn1 Sn4 Sn1 70.456(8) 42_566 15_454 Sn1 Sn4 Sn1 109.544(8) 18_544 15_454 Sn1 Sn4 Sn1 180.00(2) 39_656 15_454 Cu2 Sn4 Sn1 142.85(3) 34 36 Cu2 Sn4 Sn1 37.15(3) 10 36 Cu2 Sn4 Sn1 78.75(3) 30 36 Cu2 Sn4 Sn1 101.25(3) 6 36 Cu2 Sn4 Sn1 100.687(13) 26 36 Cu2 Sn4 Sn1 79.313(13) 2 36 Cu1 Sn4 Sn1 142.78(3) 34 36 Cu1 Sn4 Sn1 37.22(3) 10 36 Cu1 Sn4 Sn1 37.333(13) 30 36 Cu1 Sn4 Sn1 142.667(13) 6 36 Cu1 Sn4 Sn1 79.355(12) 26 36 Cu1 Sn4 Sn1 100.645(12) 2 36 Sn3 Sn4 Sn1 70.601(8) 25 36 Sn3 Sn4 Sn1 109.399(8) . 36 Sn2 Sn4 Sn1 109.245(8) . 36 Sn2 Sn4 Sn1 70.755(8) 25 36 Sn2 Sn4 Sn1 138.577(10) 5 36 Sn2 Sn4 Sn1 41.423(10) 29 36 Sn2 Sn4 Sn1 69.767(13) 9 36 Sn2 Sn4 Sn1 110.233(13) 33 36 Sn1 Sn4 Sn1 138.397(16) 21_445 36 Sn1 Sn4 Sn1 137.978(16) 42_566 36 Sn1 Sn4 Sn1 42.022(16) 18_544 36 Sn1 Sn4 Sn1 109.623(16) 39_656 36 Sn1 Sn4 Sn1 70.377(16) 15_454 36 Cu2 Sn4 Sn1 37.15(3) 34 12 Cu2 Sn4 Sn1 142.85(3) 10 12 Cu2 Sn4 Sn1 101.25(3) 30 12 Cu2 Sn4 Sn1 78.75(3) 6 12 Cu2 Sn4 Sn1 79.313(13) 26 12 Cu2 Sn4 Sn1 100.687(13) 2 12 Cu1 Sn4 Sn1 37.22(3) 34 12 Cu1 Sn4 Sn1 142.78(3) 10 12 Cu1 Sn4 Sn1 142.667(13) 30 12 Cu1 Sn4 Sn1 37.333(13) 6 12 Cu1 Sn4 Sn1 100.645(12) 26 12 Cu1 Sn4 Sn1 79.355(12) 2 12 Sn3 Sn4 Sn1 109.399(8) 25 12 Sn3 Sn4 Sn1 70.601(8) . 12 Sn2 Sn4 Sn1 70.755(8) . 12 Sn2 Sn4 Sn1 109.245(8) 25 12 Sn2 Sn4 Sn1 41.423(10) 5 12 Sn2 Sn4 Sn1 138.577(10) 29 12 Sn2 Sn4 Sn1 110.233(13) 9 12 Sn2 Sn4 Sn1 69.767(13) 33 12 Sn1 Sn4 Sn1 41.603(16) 21_445 12 Sn1 Sn4 Sn1 42.022(16) 42_566 12 Sn1 Sn4 Sn1 137.978(16) 18_544 12 Sn1 Sn4 Sn1 70.377(16) 39_656 12 Sn1 Sn4 Sn1 109.623(16) 15_454 12 Sn1 Sn4 Sn1 180.00(2) 36 12 Cu2 Sn4 Sn1 100.687(13) 34 32 Cu2 Sn4 Sn1 79.313(13) 10 32 Cu2 Sn4 Sn1 142.85(3) 30 32 Cu2 Sn4 Sn1 37.15(3) 6 32 Cu2 Sn4 Sn1 78.75(3) 26 32 Cu2 Sn4 Sn1 101.25(3) 2 32 Cu1 Sn4 Sn1 79.355(12) 34 32 Cu1 Sn4 Sn1 100.645(12) 10 32 Cu1 Sn4 Sn1 142.78(3) 30 32 Cu1 Sn4 Sn1 37.22(3) 6 32 Cu1 Sn4 Sn1 37.333(13) 26 32 Cu1 Sn4 Sn1 142.667(13) 2 32 Sn3 Sn4 Sn1 70.601(8) 25 32 Sn3 Sn4 Sn1 109.399(8) . 32 Sn2 Sn4 Sn1 138.577(10) . 32 Sn2 Sn4 Sn1 41.423(10) 25 32 Sn2 Sn4 Sn1 69.767(13) 5 32 Sn2 Sn4 Sn1 110.233(13) 29 32 Sn2 Sn4 Sn1 109.245(8) 9 32 Sn2 Sn4 Sn1 70.755(8) 33 32 Sn1 Sn4 Sn1 42.022(16) 21_445 32 Sn1 Sn4 Sn1 109.623(16) 42_566 32 Sn1 Sn4 Sn1 70.377(16) 18_544 32 Sn1 Sn4 Sn1 41.603(16) 39_656 32 Sn1 Sn4 Sn1 138.397(16) 15_454 32 Sn1 Sn4 Sn1 109.544(8) 36 32 Sn1 Sn4 Sn1 70.456(8) 12 32 Cu2 Sn4 Sn1 79.313(13) 34 8 Cu2 Sn4 Sn1 100.687(13) 10 8 Cu2 Sn4 Sn1 37.15(3) 30 8 Cu2 Sn4 Sn1 142.85(3) 6 8 Cu2 Sn4 Sn1 101.25(3) 26 8 Cu2 Sn4 Sn1 78.75(3) 2 8 Cu1 Sn4 Sn1 100.645(12) 34 8 Cu1 Sn4 Sn1 79.355(12) 10 8 Cu1 Sn4 Sn1 37.22(3) 30 8 Cu1 Sn4 Sn1 142.78(3) 6 8 Cu1 Sn4 Sn1 142.667(13) 26 8 Cu1 Sn4 Sn1 37.333(13) 2 8 Sn3 Sn4 Sn1 109.399(8) 25 8 Sn3 Sn4 Sn1 70.601(8) . 8 Sn2 Sn4 Sn1 41.423(10) . 8 Sn2 Sn4 Sn1 138.577(10) 25 8 Sn2 Sn4 Sn1 110.233(13) 5 8 Sn2 Sn4 Sn1 69.767(13) 29 8 Sn2 Sn4 Sn1 70.755(8) 9 8 Sn2 Sn4 Sn1 109.245(8) 33 8 Sn1 Sn4 Sn1 137.978(16) 21_445 8 Sn1 Sn4 Sn1 70.377(16) 42_566 8 Sn1 Sn4 Sn1 109.623(16) 18_544 8 Sn1 Sn4 Sn1 138.397(16) 39_656 8 Sn1 Sn4 Sn1 41.603(16) 15_454 8 Sn1 Sn4 Sn1 70.456(8) 36 8 Sn1 Sn4 Sn1 109.544(8) 12 8 Sn1 Sn4 Sn1 180.000(16) 32 8 Cu2 Sn4 Sn1 78.75(3) 34 28 Cu2 Sn4 Sn1 101.25(3) 10 28 Cu2 Sn4 Sn1 100.687(13) 30 28 Cu2 Sn4 Sn1 79.313(13) 6 28 Cu2 Sn4 Sn1 142.85(3) 26 28 Cu2 Sn4 Sn1 37.15(3) 2 28 Cu1 Sn4 Sn1 37.333(13) 34 28 Cu1 Sn4 Sn1 142.667(13) 10 28 Cu1 Sn4 Sn1 79.355(12) 30 28 Cu1 Sn4 Sn1 100.645(12) 6 28 Cu1 Sn4 Sn1 142.78(3) 26 28 Cu1 Sn4 Sn1 37.22(3) 2 28 Sn3 Sn4 Sn1 70.601(8) 25 28 Sn3 Sn4 Sn1 109.399(8) . 28 Sn2 Sn4 Sn1 69.768(13) . 28 Sn2 Sn4 Sn1 110.233(13) 25 28 Sn2 Sn4 Sn1 109.245(8) 5 28 Sn2 Sn4 Sn1 70.755(8) 29 28 Sn2 Sn4 Sn1 138.577(10) 9 28 Sn2 Sn4 Sn1 41.423(10) 33 28 Sn1 Sn4 Sn1 70.377(16) 21_445 28 Sn1 Sn4 Sn1 41.603(16) 42_566 28 Sn1 Sn4 Sn1 138.397(16) 18_544 28 Sn1 Sn4 Sn1 137.978(16) 39_656 28 Sn1 Sn4 Sn1 42.022(16) 15_454 28 Sn1 Sn4 Sn1 109.544(8) 36 28 Sn1 Sn4 Sn1 70.456(8) 12 28 Sn1 Sn4 Sn1 109.544(8) 32 28 Sn1 Sn4 Sn1 70.456(8) 8 28 Sn4 Cu1 Cu2 58.57(4) 2 . Sn4 Cu1 Sn2 108.20(5) 2 2 Cu2 Cu1 Sn2 166.77(7) . 2 Sn4 Cu1 Cu1 58.343(10) 2 35_665 Cu2 Cu1 Cu1 60.37(5) . 35_665 Sn2 Cu1 Cu1 114.19(6) 2 35_665 Sn4 Cu1 Cu1 58.343(9) 2 32_665 Cu2 Cu1 Cu1 60.37(5) . 32_665 Sn2 Cu1 Cu1 114.19(6) 2 32_665 Cu1 Cu1 Cu1 108.38(6) 35_665 32_665 Sn4 Cu1 Sn1 107.66(5) 2 16_654 Cu2 Cu1 Sn1 60.22(4) . 16_654 Sn2 Cu1 Sn1 129.36(4) 2 16_654 Cu1 Cu1 Sn1 114.76(8) 35_665 16_654 Cu1 Cu1 Sn1 60.18(4) 32_665 16_654 Sn4 Cu1 Sn1 107.66(5) 2 27_665 Cu2 Cu1 Sn1 60.22(4) . 27_665 Sn2 Cu1 Sn1 129.36(4) 2 27_665 Cu1 Cu1 Sn1 60.18(4) 35_665 27_665 Cu1 Cu1 Sn1 114.76(8) 32_665 27_665 Sn1 Cu1 Sn1 68.78(4) 16_654 27_665 Sn4 Cu1 Cu2 58.25(4) 2 35_665 Cu2 Cu1 Cu2 108.05(6) . 35_665 Sn2 Cu1 Cu2 60.92(4) 2 35_665 Cu1 Cu1 Cu2 59.46(4) 35_665 35_665 Cu1 Cu1 Cu2 108.06(5) 32_665 35_665 Sn1 Cu1 Cu2 165.92(6) 16_654 35_665 Sn1 Cu1 Cu2 113.59(3) 27_665 35_665 Sn4 Cu1 Cu2 58.25(4) 2 32_665 Cu2 Cu1 Cu2 108.05(6) . 32_665 Sn2 Cu1 Cu2 60.92(4) 2 32_665 Cu1 Cu1 Cu2 108.06(5) 35_665 32_665 Cu1 Cu1 Cu2 59.46(4) 32_665 32_665 Sn1 Cu1 Cu2 113.59(3) 16_654 32_665 Sn1 Cu1 Cu2 165.92(6) 27_665 32_665 Cu2 Cu1 Cu2 60.58(7) 35_665 32_665 Sn4 Cu1 Sn1 107.52(3) 2 6 Cu2 Cu1 Sn1 114.23(3) . 6 Sn2 Cu1 Sn1 67.90(3) 2 6 Cu1 Cu1 Sn1 165.86(3) 35_665 6 Cu1 Cu1 Sn1 60.00(4) 32_665 6 Sn1 Cu1 Sn1 67.96(3) 16_654 6 Sn1 Cu1 Sn1 130.43(5) 27_665 6 Cu2 Cu1 Sn1 114.33(6) 35_665 6 Cu2 Cu1 Sn1 59.86(4) 32_665 6 Sn4 Cu1 Sn1 107.52(3) 2 44_656 Cu2 Cu1 Sn1 114.23(3) . 44_656 Sn2 Cu1 Sn1 67.90(3) 2 44_656 Cu1 Cu1 Sn1 60.00(4) 35_665 44_656 Cu1 Cu1 Sn1 165.86(3) 32_665 44_656 Sn1 Cu1 Sn1 130.43(5) 16_654 44_656 Sn1 Cu1 Sn1 67.96(3) 27_665 44_656 Cu2 Cu1 Sn1 59.86(4) 35_665 44_656 Cu2 Cu1 Sn1 114.33(6) 32_665 44_656 Sn1 Cu1 Sn1 129.96(6) 6 44_656 Sn4 Cu1 Na1 179.50(15) 2 26_666 Cu2 Cu1 Na1 121.92(14) . 26_666 Sn2 Cu1 Na1 71.30(14) 2 26_666 Cu1 Cu1 Na1 121.81(4) 35_665 26_666 Cu1 Cu1 Na1 121.81(4) 32_665 26_666 Sn1 Cu1 Na1 72.73(11) 16_654 26_666 Sn1 Cu1 Na1 72.73(11) 27_665 26_666 Cu2 Cu1 Na1 121.35(12) 35_665 26_666 Cu2 Cu1 Na1 121.35(12) 32_665 26_666 Sn1 Cu1 Na1 72.33(5) 6 26_666 Sn1 Cu1 Na1 72.33(5) 44_656 26_666 Sn4 Cu2 Sn3 105.83(5) 2 26_665 Sn4 Cu2 Cu1 58.60(4) 2 . Sn3 Cu2 Cu1 164.44(7) 26_665 . Sn4 Cu2 Sn1 107.77(5) 2 27_665 Sn3 Cu2 Sn1 130.84(4) 26_665 27_665 Cu1 Cu2 Sn1 60.33(4) . 27_665 Sn4 Cu2 Sn1 107.77(5) 2 16_654 Sn3 Cu2 Sn1 130.84(4) 26_665 16_654 Cu1 Cu2 Sn1 60.33(4) . 16_654 Sn1 Cu2 Sn1 68.86(4) 27_665 16_654 Sn4 Cu2 Cu1 58.28(4) 2 35_665 Sn3 Cu2 Cu1 113.29(4) 26_665 35_665 Cu1 Cu2 Cu1 60.17(4) . 35_665 Sn1 Cu2 Cu1 60.14(3) 27_665 35_665 Sn1 Cu2 Cu1 114.67(5) 16_654 35_665 Sn4 Cu2 Cu1 58.28(4) 2 32_665 Sn3 Cu2 Cu1 113.29(4) 26_665 32_665 Cu1 Cu2 Cu1 60.17(4) . 32_665 Sn1 Cu2 Cu1 114.67(5) 27_665 32_665 Sn1 Cu2 Cu1 60.14(3) 16_654 32_665 Cu1 Cu2 Cu1 108.05(8) 35_665 32_665 Sn4 Cu2 Cu2 57.95(3) 2 11 Sn3 Cu2 Cu2 59.09(3) 26_665 11 Cu1 Cu2 Cu2 107.92(4) . 11 Sn1 Cu2 Cu2 165.72(3) 27_665 11 Sn1 Cu2 Cu2 113.81(2) 16_654 11 Cu1 Cu2 Cu2 107.75(4) 35_665 11 Cu1 Cu2 Cu2 59.71(3) 32_665 11 Sn4 Cu2 Cu2 57.95(3) 2 8 Sn3 Cu2 Cu2 59.09(3) 26_665 8 Cu1 Cu2 Cu2 107.92(4) . 8 Sn1 Cu2 Cu2 113.81(2) 27_665 8 Sn1 Cu2 Cu2 165.72(3) 16_654 8 Cu1 Cu2 Cu2 59.71(3) 35_665 8 Cu1 Cu2 Cu2 107.75(4) 32_665 8 Cu2 Cu2 Cu2 60.0 11 8 Sn4 Cu2 Sn2 106.81(3) 2 31_665 Sn3 Cu2 Sn2 69.24(3) 26_665 31_665 Cu1 Cu2 Sn2 113.28(3) . 31_665 Sn1 Cu2 Sn2 130.37(5) 27_665 31_665 Sn1 Cu2 Sn2 67.34(2) 16_654 31_665 Cu1 Cu2 Sn2 165.08(6) 35_665 31_665 Cu1 Cu2 Sn2 59.19(3) 32_665 31_665 Cu2 Cu2 Sn2 60.05(3) 11 31_665 Cu2 Cu2 Sn2 114.47(3) 8 31_665 Sn4 Cu2 Sn2 106.81(3) 2 36_665 Sn3 Cu2 Sn2 69.24(3) 26_665 36_665 Cu1 Cu2 Sn2 113.28(3) . 36_665 Sn1 Cu2 Sn2 67.34(2) 27_665 36_665 Sn1 Cu2 Sn2 130.37(5) 16_654 36_665 Cu1 Cu2 Sn2 59.19(3) 35_665 36_665 Cu1 Cu2 Sn2 165.08(6) 32_665 36_665 Cu2 Cu2 Sn2 114.47(3) 11 36_665 Cu2 Cu2 Sn2 60.05(3) 8 36_665 Sn2 Cu2 Sn2 131.96(6) 31_665 36_665 Sn4 Cu2 Na2 178.71(18) 2 34_665 Sn3 Cu2 Na2 75.45(17) 26_665 34_665 Cu1 Cu2 Na2 120.11(18) . 34_665 Sn1 Cu2 Na2 71.19(14) 27_665 34_665 Sn1 Cu2 Na2 71.19(14) 16_654 34_665 Cu1 Cu2 Na2 121.32(7) 35_665 34_665 Cu1 Cu2 Na2 121.32(7) 32_665 34_665 Cu2 Cu2 Na2 123.09(14) 11 34_665 Cu2 Cu2 Na2 123.09(14) 8 34_665 Sn2 Cu2 Na2 73.58(6) 31_665 34_665 Sn2 Cu2 Na2 73.58(6) 36_665 34_665 Cu1 Na1 Sn1 116.72(15) 26_556 38 Cu1 Na1 Sn1 116.72(15) 26_556 . Sn1 Na1 Sn1 101.41(18) 38 . Cu1 Na1 Sn2 48.34(9) 26_556 25_556 Sn1 Na1 Sn2 129.21(9) 38 25_556 Sn1 Na1 Sn2 129.21(9) . 25_556 Cu1 Na1 Sn1 48.27(8) 26_556 18_545 Sn1 Na1 Sn1 162.1(2) 38 18_545 Sn1 Na1 Sn1 81.54(4) . 18_545 Sn2 Na1 Sn1 52.07(8) 25_556 18_545 Cu1 Na1 Sn1 48.27(8) 26_556 32_556 Sn1 Na1 Sn1 81.54(4) 38 32_556 Sn1 Na1 Sn1 162.1(2) . 32_556 Sn2 Na1 Sn1 52.07(8) 25_556 32_556 Sn1 Na1 Sn1 90.44(15) 18_545 32_556 Cu1 Na1 Sn1 48.04(10) 26_556 4_556 Sn1 Na1 Sn1 111.9(2) 38 4_556 Sn1 Na1 Sn1 72.10(10) . 4_556 Sn2 Na1 Sn1 90.21(14) 25_556 4_556 Sn1 Na1 Sn1 51.77(8) 18_545 4_556 Sn1 Na1 Sn1 90.32(16) 32_556 4_556 Cu1 Na1 Sn1 48.04(10) 26_556 39_657 Sn1 Na1 Sn1 72.10(10) 38 39_657 Sn1 Na1 Sn1 111.9(2) . 39_657 Sn2 Na1 Sn1 90.21(14) 25_556 39_657 Sn1 Na1 Sn1 90.32(16) 18_545 39_657 Sn1 Na1 Sn1 51.77(8) 32_556 39_657 Sn1 Na1 Sn1 52.19(11) 4_556 39_657 Cu1 Na1 Na4 95.81(19) 26_556 33_666 Sn1 Na1 Na4 60.71(11) 38 33_666 Sn1 Na1 Na4 60.71(11) . 33_666 Sn2 Na1 Na4 144.1(2) 25_556 33_666 Sn1 Na1 Na4 107.26(16) 18_545 33_666 Sn1 Na1 Na4 107.26(16) 32_556 33_666 Sn1 Na1 Na4 58.07(11) 4_556 33_666 Sn1 Na1 Na4 58.07(11) 39_657 33_666 Cu1 Na1 Na1 98.7(2) 26_556 35_556 Sn1 Na1 Na1 144.6(3) 38 35_556 Sn1 Na1 Na1 58.97(14) . 35_556 Sn2 Na1 Na1 74.67(17) 25_556 35_556 Sn1 Na1 Na1 51.49(13) 18_545 35_556 Sn1 Na1 Na1 126.7(2) 32_556 35_556 Sn1 Na1 Na1 90.85(8) 4_556 35_556 Sn1 Na1 Na1 140.47(16) 39_657 35_556 Na4 Na1 Na1 118.04(13) 33_666 35_556 Cu1 Na1 Na1 98.7(2) 26_556 32_556 Sn1 Na1 Na1 58.97(14) 38 32_556 Sn1 Na1 Na1 144.6(3) . 32_556 Sn2 Na1 Na1 74.67(17) 25_556 32_556 Sn1 Na1 Na1 126.7(2) 18_545 32_556 Sn1 Na1 Na1 51.49(13) 32_556 32_556 Sn1 Na1 Na1 140.47(16) 4_556 32_556 Sn1 Na1 Na1 90.85(8) 39_657 32_556 Na4 Na1 Na1 118.04(13) 33_666 32_556 Na1 Na1 Na1 118.62(7) 35_556 32_556 Cu1 Na1 Na2 151.7(2) 26_556 9 Sn1 Na1 Na2 52.61(9) 38 9 Sn1 Na1 Na2 52.61(9) . 9 Sn2 Na1 Na2 159.9(2) 25_556 9 Sn1 Na1 Na2 134.06(8) 18_545 9 Sn1 Na1 Na2 134.06(8) 32_556 9 Sn1 Na1 Na2 107.75(18) 4_556 9 Sn1 Na1 Na2 107.75(18) 39_657 9 Na4 Na1 Na2 55.93(13) 33_666 9 Na1 Na1 Na2 95.6(2) 35_556 9 Na1 Na1 Na2 95.6(2) 32_556 9 Cu1 Na1 Sn2 146.07(7) 26_556 8 Sn1 Na1 Sn2 43.60(7) 38 8 Sn1 Na1 Sn2 96.27(15) . 8 Sn2 Na1 Sn2 116.21(16) 25_556 8 Sn1 Na1 Sn2 154.2(2) 18_545 8 Sn1 Na1 Sn2 97.83(6) 32_556 8 Sn1 Na1 Sn2 151.60(19) 4_556 8 Sn1 Na1 Sn2 113.96(7) 39_657 8 Na4 Na1 Sn2 93.57(12) 33_666 8 Na1 Na1 Sn2 105.45(14) 35_556 8 Na1 Na1 Sn2 48.73(12) 32_556 8 Na2 Na1 Sn2 48.61(10) 9 8 Cu1 Na1 Sn2 146.07(7) 26_556 11 Sn1 Na1 Sn2 96.27(15) 38 11 Sn1 Na1 Sn2 43.60(7) . 11 Sn2 Na1 Sn2 116.21(16) 25_556 11 Sn1 Na1 Sn2 97.83(6) 18_545 11 Sn1 Na1 Sn2 154.2(2) 32_556 11 Sn1 Na1 Sn2 113.96(7) 4_556 11 Sn1 Na1 Sn2 151.60(19) 39_657 11 Na4 Na1 Sn2 93.57(12) 33_666 11 Na1 Na1 Sn2 48.73(12) 35_556 11 Na1 Na1 Sn2 105.45(14) 32_556 11 Na2 Na1 Sn2 48.61(10) 9 11 Sn2 Na1 Sn2 65.15(10) 8 11 Cu1 Na1 Sn1 89.43(8) 26_556 19_566 Sn1 Na1 Sn1 132.17(16) 38 19_566 Sn1 Na1 Sn1 32.44(3) . 19_566 Sn2 Na1 Sn1 98.36(7) 25_556 19_566 Sn1 Na1 Sn1 49.11(2) 18_545 19_566 Sn1 Na1 Sn1 137.33(15) 32_556 19_566 Sn1 Na1 Sn1 55.99(3) 4_556 19_566 Sn1 Na1 Sn1 107.58(14) 39_657 19_566 Na4 Na1 Sn1 78.38(8) 33_666 19_566 Na1 Na1 Sn1 42.17(9) 35_556 19_566 Na1 Na1 Sn1 160.50(8) 32_556 19_566 Na2 Na1 Sn1 84.98(7) 9 19_566 Sn2 Na1 Sn1 124.42(12) 8 19_566 Sn2 Na1 Sn1 60.73(3) 11 19_566 Cu1 Na1 Sn1 89.43(8) 26_556 29_656 Sn1 Na1 Sn1 32.44(3) 38 29_656 Sn1 Na1 Sn1 132.17(16) . 29_656 Sn2 Na1 Sn1 98.36(7) 25_556 29_656 Sn1 Na1 Sn1 137.33(15) 18_545 29_656 Sn1 Na1 Sn1 49.11(2) 32_556 29_656 Sn1 Na1 Sn1 107.58(14) 4_556 29_656 Sn1 Na1 Sn1 55.99(3) 39_657 29_656 Na4 Na1 Sn1 78.38(8) 33_666 29_656 Na1 Na1 Sn1 160.50(8) 35_556 29_656 Na1 Na1 Sn1 42.17(9) 32_556 29_656 Na2 Na1 Sn1 84.98(7) 9 29_656 Sn2 Na1 Sn1 60.73(3) 8 29_656 Sn2 Na1 Sn1 124.42(12) 11 29_656 Sn1 Na1 Sn1 156.49(16) 19_566 29_656 Cu1 Na1 Na1 82.79(19) 26_556 3_556 Sn1 Na1 Na1 39.01(8) 38 3_556 Sn1 Na1 Na1 102.34(11) . 3_556 Sn2 Na1 Na1 118.87(16) 25_556 3_556 Sn1 Na1 Na1 123.1(2) 18_545 3_556 Sn1 Na1 Na1 68.71(13) 32_556 3_556 Sn1 Na1 Na1 75.12(15) 4_556 3_556 Sn1 Na1 Na1 34.92(9) 39_657 3_556 Na4 Na1 Na1 42.16(3) 33_666 3_556 Na1 Na1 Na1 159.89(7) 35_556 3_556 Na1 Na1 Na1 80.68(11) 32_556 3_556 Na2 Na1 Na1 75.62(11) 9 3_556 Sn2 Na1 Na1 82.58(12) 8 3_556 Sn2 Na1 Na1 124.07(14) 11 3_556 Sn1 Na1 Na1 118.12(11) 19_566 3_556 Sn1 Na1 Na1 38.54(8) 29_656 3_556 Cu1 Na1 Na1 82.79(19) 26_556 4_556 Sn1 Na1 Na1 102.34(11) 38 4_556 Sn1 Na1 Na1 39.00(8) . 4_556 Sn2 Na1 Na1 118.87(16) 25_556 4_556 Sn1 Na1 Na1 68.71(13) 18_545 4_556 Sn1 Na1 Na1 123.1(2) 32_556 4_556 Sn1 Na1 Na1 34.92(9) 4_556 4_556 Sn1 Na1 Na1 75.12(15) 39_657 4_556 Na4 Na1 Na1 42.16(3) 33_666 4_556 Na1 Na1 Na1 80.68(11) 35_556 4_556 Na1 Na1 Na1 159.89(7) 32_556 4_556 Na2 Na1 Na1 75.62(11) 9 4_556 Sn2 Na1 Na1 124.07(14) 8 4_556 Sn2 Na1 Na1 82.58(12) 11 4_556 Sn1 Na1 Na1 38.54(8) 19_566 4_556 Sn1 Na1 Na1 118.12(11) 29_656 4_556 Na1 Na1 Na1 79.61(11) 3_556 4_556 Cu1 Na1 Sn1 118.80(16) 26_556 37_665 Sn1 Na1 Sn1 77.70(12) 38 37_665 Sn1 Na1 Sn1 26.40(7) . 37_665 Sn2 Na1 Sn1 152.37(6) 25_556 37_665 Sn1 Na1 Sn1 100.50(8) 18_545 37_665 Sn1 Na1 Sn1 143.94(17) 32_556 37_665 Sn1 Na1 Sn1 70.98(10) 4_556 37_665 Sn1 Na1 Sn1 93.56(14) 39_657 37_665 Na4 Na1 Sn1 36.67(5) 33_666 37_665 Na1 Na1 Sn1 85.27(15) 35_556 37_665 Na1 Na1 Sn1 132.5(2) 32_556 37_665 Na2 Na1 Sn1 38.47(8) 9 37_665 Sn2 Na1 Sn1 87.07(10) 8 37_665 Sn2 Na1 Sn1 58.27(6) 11 37_665 Sn1 Na1 Sn1 54.48(4) 19_566 37_665 Sn1 Na1 Sn1 106.41(10) 29_656 37_665 Na1 Na1 Sn1 76.64(4) 3_556 37_665 Na1 Na1 Sn1 37.27(6) 4_556 37_665 Cu1 Na1 Sn1 118.80(16) 26_556 2 Sn1 Na1 Sn1 26.40(7) 38 2 Sn1 Na1 Sn1 77.70(12) . 2 Sn2 Na1 Sn1 152.37(6) 25_556 2 Sn1 Na1 Sn1 143.94(17) 18_545 2 Sn1 Na1 Sn1 100.50(8) 32_556 2 Sn1 Na1 Sn1 93.56(14) 4_556 2 Sn1 Na1 Sn1 70.98(10) 39_657 2 Na4 Na1 Sn1 36.67(5) 33_666 2 Na1 Na1 Sn1 132.5(2) 35_556 2 Na1 Na1 Sn1 85.27(15) 32_556 2 Na2 Na1 Sn1 38.47(8) 9 2 Sn2 Na1 Sn1 58.27(6) 8 2 Sn2 Na1 Sn1 87.07(10) 11 2 Sn1 Na1 Sn1 106.41(10) 19_566 2 Sn1 Na1 Sn1 54.48(4) 29_656 2 Na1 Na1 Sn1 37.27(6) 3_556 2 Na1 Na1 Sn1 76.64(4) 4_556 2 Sn1 Na1 Sn1 52.34(6) 37_665 2 Cu1 Na1 Na3 169.0(2) 26_556 2 Sn1 Na1 Na3 69.16(12) 38 2 Sn1 Na1 Na3 69.16(12) . 2 Sn2 Na1 Na3 120.61(19) 25_556 2 Sn1 Na1 Na3 127.52(12) 18_545 2 Sn1 Na1 Na3 127.52(12) 32_556 2 Sn1 Na1 Na3 140.45(13) 4_556 2 Sn1 Na1 Na3 140.45(13) 39_657 2 Na4 Na1 Na3 95.24(14) 33_666 2 Na1 Na1 Na3 76.04(14) 35_556 2 Na1 Na1 Na3 76.04(14) 32_556 2 Na2 Na1 Na3 39.32(14) 9 2 Sn2 Na1 Na3 32.59(5) 8 2 Sn2 Na1 Na3 32.59(5) 11 2 Sn1 Na1 Na3 92.80(8) 19_566 2 Sn1 Na1 Na3 92.80(8) 29_656 2 Na1 Na1 Na3 105.57(15) 3_556 2 Na1 Na1 Na3 105.57(15) 4_556 2 Sn1 Na1 Na3 70.87(10) 37_665 2 Sn1 Na1 Na3 70.87(10) 2 2 Cu1 Na1 Sn4 0.22(7) 26_556 1_556 Sn1 Na1 Sn4 116.83(13) 38 1_556 Sn1 Na1 Sn4 116.83(13) . 1_556 Sn2 Na1 Sn4 48.12(8) 25_556 1_556 Sn1 Na1 Sn4 48.21(8) 18_545 1_556 Sn1 Na1 Sn4 48.21(8) 32_556 1_556 Sn1 Na1 Sn4 48.22(8) 4_556 1_556 Sn1 Na1 Sn4 48.22(8) 39_657 1_556 Na4 Na1 Sn4 96.03(14) 33_666 1_556 Na1 Na1 Sn4 98.55(18) 35_556 1_556 Na1 Na1 Sn4 98.55(18) 32_556 1_556 Na2 Na1 Sn4 151.96(19) 9 1_556 Sn2 Na1 Sn4 146.01(6) 8 1_556 Sn2 Na1 Sn4 146.01(6) 11 1_556 Sn1 Na1 Sn4 89.47(8) 19_566 1_556 Sn1 Na1 Sn4 89.47(8) 29_656 1_556 Na1 Na1 Sn4 82.96(16) 3_556 1_556 Na1 Na1 Sn4 82.96(16) 4_556 1_556 Sn1 Na1 Sn4 119.00(12) 37_665 1_556 Sn1 Na1 Sn4 119.00(12) 2 1_556 Na3 Na1 Sn4 168.73(16) 2 1_556 Cu1 Na1 Na2 59.07(13) 26_556 10_556 Sn1 Na1 Na2 81.28(14) 38 10_556 Sn1 Na1 Na2 81.28(14) . 10_556 Sn2 Na1 Na2 107.41(16) 25_556 10_556 Sn1 Na1 Na2 81.70(13) 18_545 10_556 Sn1 Na1 Na2 81.70(13) 32_556 10_556 Sn1 Na1 Na2 30.91(7) 4_556 10_556 Sn1 Na1 Na2 30.91(7) 39_657 10_556 Na4 Na1 Na2 36.74(9) 33_666 10_556 Na1 Na1 Na2 119.72(2) 35_556 10_556 Na1 Na1 Na2 119.72(2) 32_556 10_556 Na2 Na1 Na2 92.67(19) 9 10_556 Sn2 Na1 Na2 123.54(12) 8 10_556 Sn2 Na1 Na2 123.54(12) 11 10_556 Sn1 Na1 Na2 79.65(8) 19_566 10_556 Sn1 Na1 Na2 79.65(8) 29_656 10_556 Na1 Na1 Na2 44.39(10) 3_556 10_556 Na1 Na1 Na2 44.39(10) 4_556 10_556 Sn1 Na1 Na2 66.31(9) 37_665 10_556 Sn1 Na1 Na2 66.31(9) 2 10_556 Na3 Na1 Na2 131.98(15) 2 10_556 Sn4 Na1 Na2 59.29(9) 1_556 10_556 Cu1 Na1 Na2 59.14(9) 26_556 30_556 Sn1 Na1 Na2 159.55(16) 38 30_556 Sn1 Na1 Na2 97.75(10) . 30_556 Sn2 Na1 Na2 31.55(9) 25_556 30_556 Sn1 Na1 Na2 29.87(9) 18_545 30_556 Sn1 Na1 Na2 82.45(13) 32_556 30_556 Sn1 Na1 Na2 80.76(10) 4_556 30_556 Sn1 Na1 Na2 107.18(13) 39_657 30_556 Na4 Na1 Na2 137.11(13) 33_666 30_556 Na1 Na1 Na2 45.39(16) 35_556 30_556 Na1 Na1 Na2 100.90(19) 32_556 30_556 Na2 Na1 Na2 140.88(10) 9 30_556 Sn2 Na1 Na2 127.17(16) 8 30_556 Sn2 Na1 Na2 92.64(9) 11 30_556 Sn1 Na1 Na2 68.08(10) 19_566 30_556 Sn1 Na1 Na2 129.91(13) 29_656 30_556 Na1 Na1 Na2 141.81(19) 3_556 30_556 Na1 Na1 Na2 97.03(11) 4_556 30_556 Sn1 Na1 Na2 122.46(9) 37_665 30_556 Sn1 Na1 Na2 173.65(13) 2 30_556 Na3 Na1 Na2 111.86(13) 2 30_556 Sn4 Na1 Na2 58.96(6) 1_556 30_556 Na2 Na1 Na2 108.86(9) 10_556 30_556 Cu1 Na1 Na2 59.14(9) 26_556 26_556 Sn1 Na1 Na2 97.75(10) 38 26_556 Sn1 Na1 Na2 159.55(16) . 26_556 Sn2 Na1 Na2 31.55(9) 25_556 26_556 Sn1 Na1 Na2 82.45(13) 18_545 26_556 Sn1 Na1 Na2 29.87(9) 32_556 26_556 Sn1 Na1 Na2 107.18(13) 4_556 26_556 Sn1 Na1 Na2 80.76(10) 39_657 26_556 Na4 Na1 Na2 137.11(13) 33_666 26_556 Na1 Na1 Na2 100.90(19) 35_556 26_556 Na1 Na1 Na2 45.39(16) 32_556 26_556 Na2 Na1 Na2 140.88(10) 9 26_556 Sn2 Na1 Na2 92.64(9) 8 26_556 Sn2 Na1 Na2 127.17(16) 11 26_556 Sn1 Na1 Na2 129.91(13) 19_566 26_556 Sn1 Na1 Na2 68.08(10) 29_656 26_556 Na1 Na1 Na2 97.03(11) 3_556 26_556 Na1 Na1 Na2 141.81(19) 4_556 26_556 Sn1 Na1 Na2 173.65(13) 37_665 26_556 Sn1 Na1 Na2 122.46(9) 2 26_556 Na3 Na1 Na2 111.86(13) 2 26_556 Sn4 Na1 Na2 58.96(6) 1_556 26_556 Na2 Na1 Na2 108.86(9) 10_556 26_556 Na2 Na1 Na2 62.43(18) 30_556 26_556 Cu1 Na1 Na1 58.19(4) 26_556 29_656 Sn1 Na1 Na1 59.63(11) 38 29_656 Sn1 Na1 Na1 138.2(3) . 29_656 Sn2 Na1 Na1 81.12(6) 25_556 29_656 Sn1 Na1 Na1 106.46(9) 18_545 29_656 Sn1 Na1 Na1 30.226(16) 32_556 29_656 Sn1 Na1 Na1 81.13(13) 4_556 29_656 Sn1 Na1 Na1 30.09(5) 39_657 29_656 Na4 Na1 Na1 78.01(15) 33_666 29_656 Na1 Na1 Na1 154.5(2) 35_556 29_656 Na1 Na1 Na1 60.80(14) 32_556 29_656 Na2 Na1 Na1 109.88(12) 9 29_656 Sn2 Na1 Na1 92.33(4) 8 29_656 Sn2 Na1 Na1 155.66(6) 11 29_656 Sn1 Na1 Na1 137.12(16) 19_566 29_656 Sn1 Na1 Na1 31.79(7) 29_656 29_656 Na1 Na1 Na1 38.52(14) 3_556 29_656 Na1 Na1 Na1 104.62(19) 4_556 29_656 Sn1 Na1 Na1 114.32(17) 37_665 29_656 Sn1 Na1 Na1 72.47(10) 2 29_656 Na3 Na1 Na1 124.58(2) 2 29_656 Sn4 Na1 Na1 58.26(2) 1_556 29_656 Na2 Na1 Na1 60.27(12) 10_556 29_656 Na2 Na1 Na1 109.15(9) 30_556 29_656 Na2 Na1 Na1 59.35(10) 26_556 29_656 Cu1 Na1 Na1 58.19(4) 26_556 33_566 Sn1 Na1 Na1 138.2(3) 38 33_566 Sn1 Na1 Na1 59.63(11) . 33_566 Sn2 Na1 Na1 81.12(6) 25_556 33_566 Sn1 Na1 Na1 30.226(16) 18_545 33_566 Sn1 Na1 Na1 106.46(9) 32_556 33_566 Sn1 Na1 Na1 30.09(5) 4_556 33_566 Sn1 Na1 Na1 81.13(13) 39_657 33_566 Na4 Na1 Na1 78.01(15) 33_666 33_566 Na1 Na1 Na1 60.80(14) 35_556 33_566 Na1 Na1 Na1 154.5(2) 32_556 33_566 Na2 Na1 Na1 109.88(12) 9 33_566 Sn2 Na1 Na1 155.66(6) 8 33_566 Sn2 Na1 Na1 92.33(4) 11 33_566 Sn1 Na1 Na1 31.79(7) 19_566 33_566 Sn1 Na1 Na1 137.12(16) 29_656 33_566 Na1 Na1 Na1 104.62(19) 3_556 33_566 Na1 Na1 Na1 38.52(14) 4_556 33_566 Sn1 Na1 Na1 72.47(10) 37_665 33_566 Sn1 Na1 Na1 114.32(17) 2 33_566 Na3 Na1 Na1 124.58(2) 2 33_566 Sn4 Na1 Na1 58.26(2) 1_556 33_566 Na2 Na1 Na1 60.27(12) 10_556 33_566 Na2 Na1 Na1 59.35(10) 30_556 33_566 Na2 Na1 Na1 109.15(9) 26_556 33_566 Na1 Na1 Na1 107.86(14) 29_656 33_566 Cu1 Na1 Na3 69.36(14) 26_556 26_556 Sn1 Na1 Na3 125.16(12) 38 26_556 Sn1 Na1 Na3 125.16(12) . 26_556 Sn2 Na1 Na3 21.02(10) 25_556 26_556 Sn1 Na1 Na3 63.23(11) 18_545 26_556 Sn1 Na1 Na3 63.23(11) 32_556 26_556 Sn1 Na1 Na3 109.00(14) 4_556 26_556 Sn1 Na1 Na3 109.00(14) 39_657 26_556 Na4 Na1 Na3 165.17(19) 33_666 26_556 Na1 Na1 Na3 66.21(14) 35_556 26_556 Na1 Na1 Na3 66.21(14) 32_556 26_556 Na2 Na1 Na3 138.9(2) 9 26_556 Sn2 Na1 Na3 98.91(13) 8 26_556 Sn2 Na1 Na3 98.91(13) 11 26_556 Sn1 Na1 Na3 100.77(7) 19_566 26_556 Sn1 Na1 Na3 100.77(7) 29_656 26_556 Na1 Na1 Na3 131.68(9) 3_556 26_556 Na1 Na1 Na3 131.68(9) 4_556 26_556 Sn1 Na1 Na3 151.45(7) 37_665 26_556 Sn1 Na1 Na3 151.45(7) 2 26_556 Na3 Na1 Na3 99.59(19) 2 26_556 Sn4 Na1 Na3 69.14(10) 1_556 26_556 Na2 Na1 Na3 128.43(14) 10_556 26_556 Na2 Na1 Na3 34.80(9) 30_556 26_556 Na2 Na1 Na3 34.80(9) 26_556 26_556 Na1 Na1 Na3 93.42(11) 29_656 26_556 Na1 Na1 Na3 93.42(11) 33_566 26_556 Cu1 Na1 Na4 71.62(6) 26_556 1_545 Sn1 Na1 Na4 63.65(4) 38 1_545 Sn1 Na1 Na4 164.93(14) . 1_545 Sn2 Na1 Na4 65.85(5) 25_556 1_545 Sn1 Na1 Na4 112.02(12) 18_545 1_545 Sn1 Na1 Na4 23.39(3) 32_556 1_545 Sn1 Na1 Na4 110.48(12) 4_556 1_545 Sn1 Na1 Na4 63.18(4) 39_657 1_545 Na4 Na1 Na4 107.31(8) 33_666 1_545 Na1 Na1 Na4 134.45(16) 35_556 1_545 Na1 Na1 Na4 30.02(10) 32_556 1_545 Na2 Na1 Na4 113.84(5) 9 1_545 Sn2 Na1 Na4 74.46(3) 8 1_545 Sn2 Na1 Na4 135.46(13) 11 1_545 Sn1 Na1 Na4 160.52(12) 19_566 1_545 Sn1 Na1 Na4 32.821(18) 29_656 1_545 Na1 Na1 Na4 65.15(6) 3_556 1_545 Na1 Na1 Na4 138.23(17) 4_556 1_545 Sn1 Na1 Na4 139.09(9) 37_665 1_545 Sn1 Na1 Na4 87.28(3) 2 1_545 Na3 Na1 Na4 104.97(8) 2 1_545 Sn4 Na1 Na4 71.56(6) 1_556 1_545 Na2 Na1 Na4 93.84(7) 10_556 1_545 Na2 Na1 Na4 97.33(12) 30_556 1_545 Na2 Na1 Na4 35.27(9) 26_556 1_545 Na1 Na1 Na4 33.67(7) 29_656 1_545 Na1 Na1 Na4 129.79(6) 33_566 1_545 Na3 Na1 Na4 68.84(6) 26_556 1_545 Cu1 Na1 Na4 71.62(6) 26_556 5_455 Sn1 Na1 Na4 164.93(14) 38 5_455 Sn1 Na1 Na4 63.65(4) . 5_455 Sn2 Na1 Na4 65.85(5) 25_556 5_455 Sn1 Na1 Na4 23.39(3) 18_545 5_455 Sn1 Na1 Na4 112.02(12) 32_556 5_455 Sn1 Na1 Na4 63.18(4) 4_556 5_455 Sn1 Na1 Na4 110.48(12) 39_657 5_455 Na4 Na1 Na4 107.31(8) 33_666 5_455 Na1 Na1 Na4 30.02(10) 35_556 5_455 Na1 Na1 Na4 134.45(16) 32_556 5_455 Na2 Na1 Na4 113.84(5) 9 5_455 Sn2 Na1 Na4 135.46(13) 8 5_455 Sn2 Na1 Na4 74.46(3) 11 5_455 Sn1 Na1 Na4 32.821(18) 19_566 5_455 Sn1 Na1 Na4 160.52(12) 29_656 5_455 Na1 Na1 Na4 138.23(17) 3_556 5_455 Na1 Na1 Na4 65.15(6) 4_556 5_455 Sn1 Na1 Na4 87.28(3) 37_665 5_455 Sn1 Na1 Na4 139.09(9) 2 5_455 Na3 Na1 Na4 104.97(8) 2 5_455 Sn4 Na1 Na4 71.56(6) 1_556 5_455 Na2 Na1 Na4 93.84(7) 10_556 5_455 Na2 Na1 Na4 35.27(9) 30_556 5_455 Na2 Na1 Na4 97.33(12) 26_556 5_455 Na1 Na1 Na4 129.79(6) 29_656 5_455 Na1 Na1 Na4 33.67(7) 33_566 5_455 Na3 Na1 Na4 68.84(6) 26_556 5_455 Na4 Na1 Na4 131.19(10) 1_545 5_455 Cu2 Na2 Cu2 172.4(3) 32_665 31_656 Cu2 Na2 Sn1 138.1(2) 32_665 47_566 Cu2 Na2 Sn1 47.87(5) 31_656 47_566 Cu2 Na2 Sn1 47.87(5) 32_665 6 Cu2 Na2 Sn1 138.1(2) 31_656 6 Sn1 Na2 Sn1 90.28(17) 47_566 6 Cu2 Na2 Sn1 138.1(2) 32_665 5 Cu2 Na2 Sn1 47.87(5) 31_656 5 Sn1 Na2 Sn1 52.59(9) 47_566 5 Sn1 Na2 Sn1 113.4(3) 6 5 Cu2 Na2 Sn1 47.87(5) 32_665 48 Cu2 Na2 Sn1 138.1(2) 31_656 48 Sn1 Na2 Sn1 113.4(3) 47_566 48 Sn1 Na2 Sn1 52.59(9) 6 48 Sn1 Na2 Sn1 90.28(17) 5 48 Cu2 Na2 Sn2 47.39(3) 32_665 12 Cu2 Na2 Sn2 129.88(12) 31_656 12 Sn1 Na2 Sn2 157.9(2) 47_566 12 Sn1 Na2 Sn2 89.43(4) 6 12 Sn1 Na2 Sn2 107.79(6) 5 12 Sn1 Na2 Sn2 50.88(2) 48 12 Cu2 Na2 Sn2 129.88(12) 32_665 3 Cu2 Na2 Sn2 47.39(3) 31_656 3 Sn1 Na2 Sn2 89.43(4) 47_566 3 Sn1 Na2 Sn2 157.9(2) 6 3 Sn1 Na2 Sn2 50.88(2) 5 3 Sn1 Na2 Sn2 107.79(6) 48 3 Sn2 Na2 Sn2 82.68(8) 12 3 Cu2 Na2 Sn2 129.88(12) 32_665 10 Cu2 Na2 Sn2 47.39(3) 31_656 10 Sn1 Na2 Sn2 50.88(2) 47_566 10 Sn1 Na2 Sn2 107.79(6) 6 10 Sn1 Na2 Sn2 89.43(4) 5 10 Sn1 Na2 Sn2 157.9(2) 48 10 Sn2 Na2 Sn2 148.8(3) 12 10 Sn2 Na2 Sn2 88.99(8) 3 10 Cu2 Na2 Sn2 47.39(3) 32_665 2 Cu2 Na2 Sn2 129.88(12) 31_656 2 Sn1 Na2 Sn2 107.79(6) 47_566 2 Sn1 Na2 Sn2 50.88(2) 6 2 Sn1 Na2 Sn2 157.9(2) 5 2 Sn1 Na2 Sn2 89.43(4) 48 2 Sn2 Na2 Sn2 88.99(8) 12 2 Sn2 Na2 Sn2 148.8(3) 3 2 Sn2 Na2 Sn2 82.68(8) 10 2 Cu2 Na2 Na3 86.92(14) 32_665 4 Cu2 Na2 Na3 86.92(14) 31_656 4 Sn1 Na2 Na3 134.79(10) 47_566 4 Sn1 Na2 Na3 134.79(10) 6 4 Sn1 Na2 Na3 100.50(14) 5 4 Sn1 Na2 Na3 100.50(14) 48 4 Sn2 Na2 Na3 50.90(13) 12 4 Sn2 Na2 Na3 50.90(13) 3 4 Sn2 Na2 Na3 101.3(2) 10 4 Sn2 Na2 Na3 101.3(2) 2 4 Cu2 Na2 Na3 86.92(14) 32_665 . Cu2 Na2 Na3 86.92(14) 31_656 . Sn1 Na2 Na3 100.50(14) 47_566 . Sn1 Na2 Na3 100.50(14) 6 . Sn1 Na2 Na3 134.79(10) 5 . Sn1 Na2 Na3 134.79(10) 48 . Sn2 Na2 Na3 101.3(2) 12 . Sn2 Na2 Na3 101.3(2) 3 . Sn2 Na2 Na3 50.90(13) 10 . Sn2 Na2 Na3 50.90(13) 2 . Na3 Na2 Na3 72.2(4) 4 . Cu2 Na2 Sn3 126.8(3) 32_665 3 Cu2 Na2 Sn3 45.62(8) 31_656 3 Sn1 Na2 Sn3 87.47(4) 47_566 3 Sn1 Na2 Sn3 151.40(13) 6 3 Sn1 Na2 Sn3 87.47(4) 5 3 Sn1 Na2 Sn3 151.40(13) 48 3 Sn2 Na2 Sn3 103.01(19) 12 3 Sn2 Na2 Sn3 50.65(7) 3 3 Sn2 Na2 Sn3 50.65(7) 10 3 Sn2 Na2 Sn3 103.01(19) 2 3 Na3 Na2 Sn3 52.15(16) 4 3 Na3 Na2 Sn3 52.15(16) . 3 Cu2 Na2 Sn3 45.62(8) 32_665 2 Cu2 Na2 Sn3 126.8(3) 31_656 2 Sn1 Na2 Sn3 151.40(13) 47_566 2 Sn1 Na2 Sn3 87.47(4) 6 2 Sn1 Na2 Sn3 151.40(13) 5 2 Sn1 Na2 Sn3 87.47(4) 48 2 Sn2 Na2 Sn3 50.65(7) 12 2 Sn2 Na2 Sn3 103.01(19) 3 2 Sn2 Na2 Sn3 103.01(19) 10 2 Sn2 Na2 Sn3 50.65(7) 2 2 Na3 Na2 Sn3 52.15(16) 4 2 Na3 Na2 Sn3 52.15(16) . 2 Sn3 Na2 Sn3 81.1(2) 3 2 Cu2 Na2 Na4 93.81(17) 32_665 25_666 Cu2 Na2 Na4 93.81(17) 31_656 25_666 Sn1 Na2 Na4 56.71(13) 47_566 25_666 Sn1 Na2 Na4 56.71(13) 6 25_666 Sn1 Na2 Na4 56.71(13) 5 25_666 Sn1 Na2 Na4 56.71(13) 48 25_666 Sn2 Na2 Na4 105.62(14) 12 25_666 Sn2 Na2 Na4 105.62(14) 3 25_666 Sn2 Na2 Na4 105.62(14) 10 25_666 Sn2 Na2 Na4 105.62(14) 2 25_666 Na3 Na2 Na4 143.9(2) 4 25_666 Na3 Na2 Na4 143.9(2) . 25_666 Sn3 Na2 Na4 139.43(10) 3 25_666 Sn3 Na2 Na4 139.43(10) 2 25_666 Cu2 Na2 Na1 92.32(10) 32_665 6 Cu2 Na2 Na1 92.32(10) 31_656 6 Sn1 Na2 Na1 46.70(8) 47_566 6 Sn1 Na2 Na1 46.70(8) 6 6 Sn1 Na2 Na1 90.94(18) 5 6 Sn1 Na2 Na1 90.94(18) 48 6 Sn2 Na2 Na1 136.03(12) 12 6 Sn2 Na2 Na1 136.03(12) 3 6 Sn2 Na2 Na1 66.97(8) 10 6 Sn2 Na2 Na1 66.97(8) 2 6 Na3 Na2 Na1 163.7(3) 4 6 Na3 Na2 Na1 91.5(2) . 6 Sn3 Na2 Na1 117.60(7) 3 6 Sn3 Na2 Na1 117.60(7) 2 6 Na4 Na2 Na1 52.42(14) 25_666 6 Cu2 Na2 Na1 92.32(10) 32_665 5 Cu2 Na2 Na1 92.32(10) 31_656 5 Sn1 Na2 Na1 90.94(18) 47_566 5 Sn1 Na2 Na1 90.94(18) 6 5 Sn1 Na2 Na1 46.70(8) 5 5 Sn1 Na2 Na1 46.70(8) 48 5 Sn2 Na2 Na1 66.97(8) 12 5 Sn2 Na2 Na1 66.97(8) 3 5 Sn2 Na2 Na1 136.03(12) 10 5 Sn2 Na2 Na1 136.03(12) 2 5 Na3 Na2 Na1 91.5(2) 4 5 Na3 Na2 Na1 163.7(3) . 5 Sn3 Na2 Na1 117.60(7) 3 5 Sn3 Na2 Na1 117.60(7) 2 5 Na4 Na2 Na1 52.42(14) 25_666 5 Na1 Na2 Na1 104.8(3) 6 5 Cu2 Na2 Sn4 0.58(8) 32_665 2 Cu2 Na2 Sn4 172.9(3) 31_656 2 Sn1 Na2 Sn4 137.62(15) 47_566 2 Sn1 Na2 Sn4 47.414(19) 6 2 Sn1 Na2 Sn4 137.62(15) 5 2 Sn1 Na2 Sn4 47.414(19) 48 2 Sn2 Na2 Sn4 47.572(14) 12 2 Sn2 Na2 Sn4 130.11(8) 3 2 Sn2 Na2 Sn4 130.11(8) 10 2 Sn2 Na2 Sn4 47.572(14) 2 2 Na3 Na2 Sn4 87.38(8) 4 2 Na3 Na2 Sn4 87.38(8) . 2 Sn3 Na2 Sn4 127.33(19) 3 2 Sn3 Na2 Sn4 46.19(2) 2 2 Na4 Na2 Sn4 93.24(9) 25_666 2 Na1 Na2 Sn4 91.97(5) 6 2 Na1 Na2 Sn4 91.97(5) 5 2 Cu2 Na2 Sn4 172.9(3) 32_665 3 Cu2 Na2 Sn4 0.58(8) 31_656 3 Sn1 Na2 Sn4 47.414(19) 47_566 3 Sn1 Na2 Sn4 137.62(15) 6 3 Sn1 Na2 Sn4 47.414(19) 5 3 Sn1 Na2 Sn4 137.62(15) 48 3 Sn2 Na2 Sn4 130.11(8) 12 3 Sn2 Na2 Sn4 47.572(14) 3 3 Sn2 Na2 Sn4 47.572(14) 10 3 Sn2 Na2 Sn4 130.11(8) 2 3 Na3 Na2 Sn4 87.38(8) 4 3 Na3 Na2 Sn4 87.38(8) . 3 Sn3 Na2 Sn4 46.19(2) 3 3 Sn3 Na2 Sn4 127.33(19) 2 3 Na4 Na2 Sn4 93.24(9) 25_666 3 Na1 Na2 Sn4 91.97(5) 6 3 Na1 Na2 Sn4 91.97(5) 5 3 Sn4 Na2 Sn4 173.52(18) 2 3 Cu2 Na2 Na1 128.7(2) 32_665 8_655 Cu2 Na2 Na1 58.90(13) 31_656 8_655 Sn1 Na2 Na1 31.15(9) 47_566 8_655 Sn1 Na2 Na1 87.45(18) 6 8_655 Sn1 Na2 Na1 31.15(8) 5 8_655 Sn1 Na2 Na1 87.45(18) 48 8_655 Sn2 Na2 Na1 126.78(15) 12 8_655 Sn2 Na2 Na1 80.95(10) 3 8_655 Sn2 Na2 Na1 80.95(10) 10 8_655 Sn2 Na2 Na1 126.78(15) 2 8_655 Na3 Na2 Na1 131.48(13) 4 8_655 Na3 Na2 Na1 131.48(13) . 8_655 Sn3 Na2 Na1 104.52(8) 3 8_655 Sn3 Na2 Na1 174.34(16) 2 8_655 Na4 Na2 Na1 34.91(8) 25_666 8_655 Na1 Na2 Na1 59.99(12) 6 8_655 Na1 Na2 Na1 59.99(12) 5 8_655 Sn4 Na2 Na1 128.15(15) 2 8_655 Sn4 Na2 Na1 58.33(7) 3 8_655 Cu2 Na2 Na1 58.90(13) 32_665 7_655 Cu2 Na2 Na1 128.7(2) 31_656 7_655 Sn1 Na2 Na1 87.45(18) 47_566 7_655 Sn1 Na2 Na1 31.15(9) 6 7_655 Sn1 Na2 Na1 87.45(18) 5 7_655 Sn1 Na2 Na1 31.15(8) 48 7_655 Sn2 Na2 Na1 80.95(10) 12 7_655 Sn2 Na2 Na1 126.78(15) 3 7_655 Sn2 Na2 Na1 126.78(15) 10 7_655 Sn2 Na2 Na1 80.95(10) 2 7_655 Na3 Na2 Na1 131.48(13) 4 7_655 Na3 Na2 Na1 131.48(13) . 7_655 Sn3 Na2 Na1 174.34(16) 3 7_655 Sn3 Na2 Na1 104.52(8) 2 7_655 Na4 Na2 Na1 34.91(8) 25_666 7_655 Na1 Na2 Na1 59.99(12) 6 7_655 Na1 Na2 Na1 59.99(12) 5 7_655 Sn4 Na2 Na1 58.33(7) 2 7_655 Sn4 Na2 Na1 128.15(15) 3 7_655 Na1 Na2 Na1 69.82(16) 8_655 7_655 Cu2 Na2 Na1 123.85(8) 32_665 34_666 Cu2 Na2 Na1 58.18(7) 31_656 34_666 Sn1 Na2 Na1 29.97(6) 47_566 34_666 Sn1 Na2 Na1 84.49(9) 6 34_666 Sn1 Na2 Na1 81.42(10) 5 34_666 Sn1 Na2 Na1 128.39(19) 48 34_666 Sn2 Na2 Na1 170.47(10) 12 34_666 Sn2 Na2 Na1 105.57(7) 3 34_666 Sn2 Na2 Na1 30.02(6) 10 34_666 Sn2 Na2 Na1 81.48(7) 2 34_666 Na3 Na2 Na1 131.11(19) 4 34_666 Na3 Na2 Na1 72.74(17) . 34_666 Sn3 Na2 Na1 79.42(4) 3 34_666 Sn3 Na2 Na1 121.54(11) 2 34_666 Na4 Na2 Na1 77.09(9) 25_666 34_666 Na1 Na2 Na1 38.96(8) 6 34_666 Na1 Na2 Na1 120.3(2) 5 34_666 Sn4 Na2 Na1 123.71(7) 2 34_666 Sn4 Na2 Na1 58.01(6) 3 34_666 Na1 Na2 Na1 60.39(8) 8_655 34_666 Na1 Na2 Na1 97.34(12) 7_655 34_666 Cu2 Na2 Na1 58.18(7) 32_665 26_666 Cu2 Na2 Na1 123.85(8) 31_656 26_666 Sn1 Na2 Na1 84.49(9) 47_566 26_666 Sn1 Na2 Na1 29.97(6) 6 26_666 Sn1 Na2 Na1 128.39(19) 5 26_666 Sn1 Na2 Na1 81.42(10) 48 26_666 Sn2 Na2 Na1 105.57(7) 12 26_666 Sn2 Na2 Na1 170.47(10) 3 26_666 Sn2 Na2 Na1 81.48(7) 10 26_666 Sn2 Na2 Na1 30.02(6) 2 26_666 Na3 Na2 Na1 131.11(19) 4 26_666 Na3 Na2 Na1 72.74(17) . 26_666 Sn3 Na2 Na1 121.54(11) 3 26_666 Sn3 Na2 Na1 79.42(4) 2 26_666 Na4 Na2 Na1 77.09(9) 25_666 26_666 Na1 Na2 Na1 38.96(8) 6 26_666 Na1 Na2 Na1 120.3(2) 5 26_666 Sn4 Na2 Na1 58.01(6) 2 26_666 Sn4 Na2 Na1 123.71(7) 3 26_666 Na1 Na2 Na1 97.34(12) 8_655 26_666 Na1 Na2 Na1 60.39(8) 7_655 26_666 Na1 Na2 Na1 65.82(13) 34_666 26_666 Cu2 Na2 Na1 58.18(7) 32_665 36_655 Cu2 Na2 Na1 123.85(8) 31_656 36_655 Sn1 Na2 Na1 128.39(19) 47_566 36_655 Sn1 Na2 Na1 81.42(10) 6 36_655 Sn1 Na2 Na1 84.49(9) 5 36_655 Sn1 Na2 Na1 29.97(6) 48 36_655 Sn2 Na2 Na1 30.02(6) 12 36_655 Sn2 Na2 Na1 81.48(7) 3 36_655 Sn2 Na2 Na1 170.47(10) 10 36_655 Sn2 Na2 Na1 105.57(7) 2 36_655 Na3 Na2 Na1 72.75(17) 4 36_655 Na3 Na2 Na1 131.12(19) . 36_655 Sn3 Na2 Na1 121.54(11) 3 36_655 Sn3 Na2 Na1 79.42(4) 2 36_655 Na4 Na2 Na1 77.09(9) 25_666 36_655 Na1 Na2 Na1 120.3(2) 6 36_655 Na1 Na2 Na1 38.96(8) 5 36_655 Sn4 Na2 Na1 58.01(6) 2 36_655 Sn4 Na2 Na1 123.71(7) 3 36_655 Na1 Na2 Na1 97.34(12) 8_655 36_655 Na1 Na2 Na1 60.39(8) 7_655 36_655 Na1 Na2 Na1 154.18(19) 34_666 36_655 Na1 Na2 Na1 108.05(15) 26_666 36_655 Cu2 Na2 Na1 123.85(8) 32_665 27_655 Cu2 Na2 Na1 58.18(7) 31_656 27_655 Sn1 Na2 Na1 81.42(10) 47_566 27_655 Sn1 Na2 Na1 128.39(19) 6 27_655 Sn1 Na2 Na1 29.97(6) 5 27_655 Sn1 Na2 Na1 84.49(9) 48 27_655 Sn2 Na2 Na1 81.48(7) 12 27_655 Sn2 Na2 Na1 30.02(6) 3 27_655 Sn2 Na2 Na1 105.57(7) 10 27_655 Sn2 Na2 Na1 170.47(10) 2 27_655 Na3 Na2 Na1 72.75(17) 4 27_655 Na3 Na2 Na1 131.12(19) . 27_655 Sn3 Na2 Na1 79.42(4) 3 27_655 Sn3 Na2 Na1 121.54(11) 2 27_655 Na4 Na2 Na1 77.09(9) 25_666 27_655 Na1 Na2 Na1 120.3(2) 6 27_655 Na1 Na2 Na1 38.96(8) 5 27_655 Sn4 Na2 Na1 123.71(7) 2 27_655 Sn4 Na2 Na1 58.01(6) 3 27_655 Na1 Na2 Na1 60.39(8) 8_655 27_655 Na1 Na2 Na1 97.34(12) 7_655 27_655 Na1 Na2 Na1 108.05(15) 34_666 27_655 Na1 Na2 Na1 154.18(19) 26_666 27_655 Na1 Na2 Na1 65.82(13) 36_655 27_655 Cu2 Na2 Na2 56.91(14) 32_665 10 Cu2 Na2 Na2 116.86(14) 31_656 10 Sn1 Na2 Na2 164.59(10) 47_566 10 Sn1 Na2 Na2 104.79(9) 6 10 Sn1 Na2 Na2 121.40(8) 5 10 Sn1 Na2 Na2 79.18(13) 48 10 Sn2 Na2 Na2 29.42(14) 12 10 Sn2 Na2 Na2 77.84(10) 3 10 Sn2 Na2 Na2 119.36(14) 10 10 Sn2 Na2 Na2 80.20(10) 2 10 Na3 Na2 Na2 30.011(6) 4 10 Na3 Na2 Na2 73.96(18) . 10 Sn3 Na2 Na2 77.76(8) 3 10 Sn3 Na2 Na2 30.423(16) 2 10 Na4 Na2 Na2 135.0 25_666 10 Na1 Na2 Na2 145.84(6) 6 10 Na1 Na2 Na2 92.00(12) 5 10 Sn4 Na2 Na2 57.37(7) 2 10 Sn4 Na2 Na2 117.34(8) 3 10 Na1 Na2 Na2 149.998(1) 8_655 10 Na1 Na2 Na2 107.08(7) 7_655 10 Na1 Na2 Na2 146.54(9) 34_666 10 Na1 Na2 Na2 106.92(7) 26_666 10 Na1 Na2 Na2 58.78(9) 36_655 10 Na1 Na2 Na2 91.43(9) 27_655 10 Cu2 Na2 Na2 116.86(14) 32_665 6 Cu2 Na2 Na2 56.91(14) 31_656 6 Sn1 Na2 Na2 104.79(9) 47_566 6 Sn1 Na2 Na2 164.59(10) 6 6 Sn1 Na2 Na2 79.18(13) 5 6 Sn1 Na2 Na2 121.40(8) 48 6 Sn2 Na2 Na2 77.84(10) 12 6 Sn2 Na2 Na2 29.42(14) 3 6 Sn2 Na2 Na2 80.20(10) 10 6 Sn2 Na2 Na2 119.36(14) 2 6 Na3 Na2 Na2 30.011(5) 4 6 Na3 Na2 Na2 73.96(18) . 6 Sn3 Na2 Na2 30.423(16) 3 6 Sn3 Na2 Na2 77.76(8) 2 6 Na4 Na2 Na2 135.0 25_666 6 Na1 Na2 Na2 145.84(6) 6 6 Na1 Na2 Na2 92.00(12) 5 6 Sn4 Na2 Na2 117.34(8) 2 6 Sn4 Na2 Na2 57.37(7) 3 6 Na1 Na2 Na2 107.08(7) 8_655 6 Na1 Na2 Na2 149.998(1) 7_655 6 Na1 Na2 Na2 106.92(7) 34_666 6 Na1 Na2 Na2 146.54(9) 26_666 6 Na1 Na2 Na2 91.43(9) 36_655 6 Na1 Na2 Na2 58.78(9) 27_655 6 Na2 Na2 Na2 60.0 10 6 Cu2 Na2 Na2 116.86(14) 32_665 9 Cu2 Na2 Na2 56.91(14) 31_656 9 Sn1 Na2 Na2 79.18(13) 47_566 9 Sn1 Na2 Na2 121.40(8) 6 9 Sn1 Na2 Na2 104.79(9) 5 9 Sn1 Na2 Na2 164.59(10) 48 9 Sn2 Na2 Na2 119.36(14) 12 9 Sn2 Na2 Na2 80.20(10) 3 9 Sn2 Na2 Na2 29.42(14) 10 9 Sn2 Na2 Na2 77.84(10) 2 9 Na3 Na2 Na2 73.96(18) 4 9 Na3 Na2 Na2 30.011(5) . 9 Sn3 Na2 Na2 30.423(16) 3 9 Sn3 Na2 Na2 77.76(8) 2 9 Na4 Na2 Na2 135.0 25_666 9 Na1 Na2 Na2 92.00(12) 6 9 Na1 Na2 Na2 145.84(6) 5 9 Sn4 Na2 Na2 117.34(8) 2 9 Sn4 Na2 Na2 57.37(7) 3 9 Na1 Na2 Na2 107.08(7) 8_655 9 Na1 Na2 Na2 149.998(1) 7_655 9 Na1 Na2 Na2 58.78(9) 34_666 9 Na1 Na2 Na2 91.43(9) 26_666 9 Na1 Na2 Na2 146.54(9) 36_655 9 Na1 Na2 Na2 106.92(7) 27_655 9 Na2 Na2 Na2 90.0 10 9 Na2 Na2 Na2 60.0 6 9 Cu2 Na2 Na2 56.91(14) 32_665 5 Cu2 Na2 Na2 116.86(14) 31_656 5 Sn1 Na2 Na2 121.40(8) 47_566 5 Sn1 Na2 Na2 79.18(13) 6 5 Sn1 Na2 Na2 164.59(10) 5 5 Sn1 Na2 Na2 104.79(9) 48 5 Sn2 Na2 Na2 80.20(10) 12 5 Sn2 Na2 Na2 119.36(14) 3 5 Sn2 Na2 Na2 77.84(10) 10 5 Sn2 Na2 Na2 29.42(14) 2 5 Na3 Na2 Na2 73.96(18) 4 5 Na3 Na2 Na2 30.011(5) . 5 Sn3 Na2 Na2 77.76(8) 3 5 Sn3 Na2 Na2 30.423(16) 2 5 Na4 Na2 Na2 135.0 25_666 5 Na1 Na2 Na2 92.00(12) 6 5 Na1 Na2 Na2 145.84(6) 5 5 Sn4 Na2 Na2 57.37(7) 2 5 Sn4 Na2 Na2 117.34(8) 3 5 Na1 Na2 Na2 149.998(1) 8_655 5 Na1 Na2 Na2 107.08(7) 7_655 5 Na1 Na2 Na2 91.43(9) 34_666 5 Na1 Na2 Na2 58.78(9) 26_666 5 Na1 Na2 Na2 106.92(7) 36_655 5 Na1 Na2 Na2 146.54(9) 27_655 5 Na2 Na2 Na2 60.0 10 5 Na2 Na2 Na2 90.0 6 5 Na2 Na2 Na2 60.0 9 5 Cu2 Na2 Na3 66.43(15) 32_665 3 Cu2 Na2 Na3 105.9(2) 31_656 3 Sn1 Na2 Na3 139.13(15) 47_566 3 Sn1 Na2 Na3 106.08(12) 6 3 Sn1 Na2 Na3 139.13(15) 5 3 Sn1 Na2 Na3 106.08(12) 48 3 Sn2 Na2 Na3 61.53(13) 12 3 Sn2 Na2 Na3 88.27(17) 3 3 Sn2 Na2 Na3 88.27(17) 10 3 Sn2 Na2 Na3 61.53(13) 2 3 Na3 Na2 Na3 40.5(2) 4 3 Na3 Na2 Na3 40.5(2) . 3 Sn3 Na2 Na3 60.33(14) 3 3 Sn3 Na2 Na3 20.81(10) 2 3 Na4 Na2 Na3 160.24(7) 25_666 3 Na1 Na2 Na3 125.03(12) 6 3 Na1 Na2 Na3 125.03(12) 5 3 Sn4 Na2 Na3 67.01(9) 2 3 Sn4 Na2 Na3 106.52(14) 3 3 Na1 Na2 Na3 164.84(12) 8_655 3 Na1 Na2 Na3 125.33(9) 7_655 3 Na1 Na2 Na3 113.20(11) 34_666 3 Na1 Na2 Na3 91.53(8) 26_666 3 Na1 Na2 Na3 91.53(8) 36_655 3 Na1 Na2 Na3 113.20(11) 27_655 3 Na2 Na2 Na3 33.44(3) 10 3 Na2 Na2 Na3 60.23(6) 6 3 Na2 Na2 Na3 60.23(6) 9 3 Na2 Na2 Na3 33.44(3) 5 3 Sn2 Na3 Sn2 100.0(3) 10 6 Sn2 Na3 Sn2 100.0(3) 10 2 Sn2 Na3 Sn2 100.0(3) 6 2 Sn2 Na3 Sn3 128.29(3) 10 4 Sn2 Na3 Sn3 58.90(3) 6 4 Sn2 Na3 Sn3 128.29(3) 2 4 Sn2 Na3 Sn3 58.90(3) 10 3 Sn2 Na3 Sn3 128.29(3) 6 3 Sn2 Na3 Sn3 128.29(3) 2 3 Sn3 Na3 Sn3 95.7(3) 4 3 Sn2 Na3 Sn3 128.29(3) 10 2 Sn2 Na3 Sn3 128.29(3) 6 2 Sn2 Na3 Sn3 58.90(3) 2 2 Sn3 Na3 Sn3 95.7(3) 4 2 Sn3 Na3 Sn3 95.7(3) 3 2 Sn2 Na3 Na2 64.19(7) 10 . Sn2 Na3 Na2 153.1(4) 6 . Sn2 Na3 Na2 64.19(7) 2 . Sn3 Na3 Na2 148.0(4) 4 . Sn3 Na3 Na2 64.17(8) 3 . Sn3 Na3 Na2 64.17(8) 2 . Sn2 Na3 Na2 64.19(7) 10 9 Sn2 Na3 Na2 64.19(7) 6 9 Sn2 Na3 Na2 153.1(4) 2 9 Sn3 Na3 Na2 64.17(8) 4 9 Sn3 Na3 Na2 64.17(8) 3 9 Sn3 Na3 Na2 148.0(4) 2 9 Na2 Na3 Na2 119.978(11) . 9 Sn2 Na3 Na2 153.1(4) 10 5 Sn2 Na3 Na2 64.19(7) 6 5 Sn2 Na3 Na2 64.19(7) 2 5 Sn3 Na3 Na2 64.17(8) 4 5 Sn3 Na3 Na2 148.0(4) 3 5 Sn3 Na3 Na2 64.17(8) 2 5 Na2 Na3 Na2 119.978(11) . 5 Na2 Na3 Na2 119.978(11) 9 5 Sn2 Na3 Na3 97.19(17) 10 4 Sn2 Na3 Na3 153.0(2) 6 4 Sn2 Na3 Na3 97.19(17) 2 4 Sn3 Na3 Na3 94.14(19) 4 4 Sn3 Na3 Na3 47.99(14) 3 4 Sn3 Na3 Na3 47.99(14) 2 4 Na2 Na3 Na3 53.9(2) . 4 Na2 Na3 Na3 106.04(18) 9 4 Na2 Na3 Na3 106.04(18) 5 4 Sn2 Na3 Na3 153.0(2) 10 3 Sn2 Na3 Na3 97.19(17) 6 3 Sn2 Na3 Na3 97.19(17) 2 3 Sn3 Na3 Na3 47.99(14) 4 3 Sn3 Na3 Na3 94.14(19) 3 3 Sn3 Na3 Na3 47.99(14) 2 3 Na2 Na3 Na3 106.04(18) . 3 Na2 Na3 Na3 106.04(18) 9 3 Na2 Na3 Na3 53.9(2) 5 3 Na3 Na3 Na3 60.0 4 3 Sn2 Na3 Na3 97.19(17) 10 2 Sn2 Na3 Na3 97.19(17) 6 2 Sn2 Na3 Na3 153.0(2) 2 2 Sn3 Na3 Na3 47.99(14) 4 2 Sn3 Na3 Na3 47.99(14) 3 2 Sn3 Na3 Na3 94.14(19) 2 2 Na2 Na3 Na3 106.04(18) . 2 Na2 Na3 Na3 53.9(2) 9 2 Na2 Na3 Na3 106.04(18) 5 2 Na3 Na3 Na3 60.0 4 2 Na3 Na3 Na3 60.0 3 2 Sn2 Na3 Cu2 131.64(17) 10 36_566 Sn2 Na3 Cu2 34.13(4) 6 36_566 Sn2 Na3 Cu2 102.48(9) 2 36_566 Sn3 Na3 Cu2 33.13(4) 4 36_566 Sn3 Na3 Cu2 127.3(2) 3 36_566 Sn3 Na3 Cu2 99.94(11) 2 36_566 Na2 Na3 Cu2 162.71(6) . 36_566 Na2 Na3 Cu2 77.003(18) 9 36_566 Na2 Na3 Cu2 42.978(18) 5 36_566 Na3 Na3 Cu2 121.39(14) 4 36_566 Na3 Na3 Cu2 63.07(13) 3 36_566 Na3 Na3 Cu2 80.77(12) 2 36_566 Sn2 Na3 Cu2 131.64(17) 10 35_665 Sn2 Na3 Cu2 102.48(9) 6 35_665 Sn2 Na3 Cu2 34.13(4) 2 35_665 Sn3 Na3 Cu2 99.94(11) 4 35_665 Sn3 Na3 Cu2 127.3(2) 3 35_665 Sn3 Na3 Cu2 33.13(4) 2 35_665 Na2 Na3 Cu2 77.003(18) . 35_665 Na2 Na3 Cu2 162.71(6) 9 35_665 Na2 Na3 Cu2 42.978(18) 5 35_665 Na3 Na3 Cu2 80.77(12) 4 35_665 Na3 Na3 Cu2 63.07(13) 3 35_665 Na3 Na3 Cu2 121.39(14) 2 35_665 Cu2 Na3 Cu2 85.87(3) 36_566 35_665 Sn2 Na3 Cu2 102.48(9) 10 32_665 Sn2 Na3 Cu2 131.64(17) 6 32_665 Sn2 Na3 Cu2 34.13(4) 2 32_665 Sn3 Na3 Cu2 127.3(2) 4 32_665 Sn3 Na3 Cu2 99.94(11) 3 32_665 Sn3 Na3 Cu2 33.13(4) 2 32_665 Na2 Na3 Cu2 42.978(18) . 32_665 Na2 Na3 Cu2 162.71(6) 9 32_665 Na2 Na3 Cu2 77.003(18) 5 32_665 Na3 Na3 Cu2 63.07(13) 4 32_665 Na3 Na3 Cu2 80.77(12) 3 32_665 Na3 Na3 Cu2 121.39(14) 2 32_665 Cu2 Na3 Cu2 119.859(19) 36_566 32_665 Cu2 Na3 Cu2 34.03(3) 35_665 32_665 Sn2 Na3 Cu2 34.13(4) 10 31_656 Sn2 Na3 Cu2 131.64(17) 6 31_656 Sn2 Na3 Cu2 102.48(9) 2 31_656 Sn3 Na3 Cu2 127.3(2) 4 31_656 Sn3 Na3 Cu2 33.13(4) 3 31_656 Sn3 Na3 Cu2 99.94(11) 2 31_656 Na2 Na3 Cu2 42.978(18) . 31_656 Na2 Na3 Cu2 77.003(18) 9 31_656 Na2 Na3 Cu2 162.71(6) 5 31_656 Na3 Na3 Cu2 63.07(13) 4 31_656 Na3 Na3 Cu2 121.39(14) 3 31_656 Na3 Na3 Cu2 80.77(12) 2 31_656 Cu2 Na3 Cu2 153.70(6) 36_566 31_656 Cu2 Na3 Cu2 119.859(19) 35_665 31_656 Cu2 Na3 Cu2 85.87(3) 32_665 31_656 Sn2 Na3 Cu2 34.13(4) 10 28_656 Sn2 Na3 Cu2 102.48(9) 6 28_656 Sn2 Na3 Cu2 131.64(17) 2 28_656 Sn3 Na3 Cu2 99.94(11) 4 28_656 Sn3 Na3 Cu2 33.13(4) 3 28_656 Sn3 Na3 Cu2 127.3(2) 2 28_656 Na2 Na3 Cu2 77.003(18) . 28_656 Na2 Na3 Cu2 42.978(18) 9 28_656 Na2 Na3 Cu2 162.71(6) 5 28_656 Na3 Na3 Cu2 80.77(12) 4 28_656 Na3 Na3 Cu2 121.39(14) 3 28_656 Na3 Na3 Cu2 63.07(13) 2 28_656 Cu2 Na3 Cu2 119.859(19) 36_566 28_656 Cu2 Na3 Cu2 153.70(6) 35_665 28_656 Cu2 Na3 Cu2 119.859(19) 32_665 28_656 Cu2 Na3 Cu2 34.03(3) 31_656 28_656 Sn2 Na3 Cu2 102.48(9) 10 27_566 Sn2 Na3 Cu2 34.13(4) 6 27_566 Sn2 Na3 Cu2 131.64(17) 2 27_566 Sn3 Na3 Cu2 33.13(4) 4 27_566 Sn3 Na3 Cu2 99.94(11) 3 27_566 Sn3 Na3 Cu2 127.3(2) 2 27_566 Na2 Na3 Cu2 162.71(6) . 27_566 Na2 Na3 Cu2 42.978(18) 9 27_566 Na2 Na3 Cu2 77.003(18) 5 27_566 Na3 Na3 Cu2 121.39(14) 4 27_566 Na3 Na3 Cu2 80.77(12) 3 27_566 Na3 Na3 Cu2 63.07(13) 2 27_566 Cu2 Na3 Cu2 34.03(3) 36_566 27_566 Cu2 Na3 Cu2 119.859(19) 35_665 27_566 Cu2 Na3 Cu2 153.70(6) 32_665 27_566 Cu2 Na3 Cu2 119.859(19) 31_656 27_566 Cu2 Na3 Cu2 85.87(3) 28_656 27_566 Sn2 Na3 Sn1 119.9(3) 10 44_656 Sn2 Na3 Sn1 78.58(13) 6 44_656 Sn2 Na3 Sn1 27.01(3) 2 44_656 Sn3 Na3 Sn1 102.568(17) 4 44_656 Sn3 Na3 Sn1 152.98(6) 3 44_656 Sn3 Na3 Sn1 63.08(6) 2 44_656 Na2 Na3 Sn1 90.43(9) . 44_656 Na2 Na3 Sn1 142.2(2) 9 44_656 Na2 Na3 Sn1 38.84(9) 5 44_656 Na3 Na3 Sn1 110.24(9) 4 44_656 Na3 Na3 Sn1 83.79(11) 3 44_656 Na3 Na3 Sn1 142.94(10) 2 44_656 Cu2 Na3 Sn1 75.51(5) 36_566 44_656 Cu2 Na3 Sn1 29.98(4) 35_665 44_656 Cu2 Na3 Sn1 53.10(4) 32_665 44_656 Cu2 Na3 Sn1 129.35(12) 31_656 44_656 Cu2 Na3 Sn1 154.0(2) 28_656 44_656 Cu2 Na3 Sn1 106.26(8) 27_566 44_656 Sn2 Na3 Sn1 119.9(3) 10 10 Sn2 Na3 Sn1 27.01(3) 6 10 Sn2 Na3 Sn1 78.58(13) 2 10 Sn3 Na3 Sn1 63.08(6) 4 10 Sn3 Na3 Sn1 152.98(6) 3 10 Sn3 Na3 Sn1 102.568(17) 2 10 Na2 Na3 Sn1 142.2(2) . 10 Na2 Na3 Sn1 90.43(9) 9 10 Na2 Na3 Sn1 38.84(9) 5 10 Na3 Na3 Sn1 142.94(10) 4 10 Na3 Na3 Sn1 83.79(11) 3 10 Na3 Na3 Sn1 110.24(9) 2 10 Cu2 Na3 Sn1 29.98(4) 36_566 10 Cu2 Na3 Sn1 75.51(5) 35_665 10 Cu2 Na3 Sn1 106.26(8) 32_665 10 Cu2 Na3 Sn1 154.0(2) 31_656 10 Cu2 Na3 Sn1 129.35(12) 28_656 10 Cu2 Na3 Sn1 53.10(4) 27_566 10 Sn1 Na3 Sn1 53.76(6) 44_656 10 Sn2 Na3 Sn1 78.58(13) 10 6 Sn2 Na3 Sn1 119.9(3) 6 6 Sn2 Na3 Sn1 27.01(3) 2 6 Sn3 Na3 Sn1 152.98(6) 4 6 Sn3 Na3 Sn1 102.568(17) 3 6 Sn3 Na3 Sn1 63.08(6) 2 6 Na2 Na3 Sn1 38.84(9) . 6 Na2 Na3 Sn1 142.2(2) 9 6 Na2 Na3 Sn1 90.43(9) 5 6 Na3 Na3 Sn1 83.79(11) 4 6 Na3 Na3 Sn1 110.24(9) 3 6 Na3 Na3 Sn1 142.94(10) 2 6 Cu2 Na3 Sn1 129.35(12) 36_566 6 Cu2 Na3 Sn1 53.10(4) 35_665 6 Cu2 Na3 Sn1 29.98(4) 32_665 6 Cu2 Na3 Sn1 75.51(5) 31_656 6 Cu2 Na3 Sn1 106.26(8) 28_656 6 Cu2 Na3 Sn1 154.0(2) 27_566 6 Sn1 Na3 Sn1 54.01(6) 44_656 6 Sn1 Na3 Sn1 103.40(14) 10 6 Sn2 Na3 Sn1 78.58(13) 10 37_665 Sn2 Na3 Sn1 27.01(3) 6 37_665 Sn2 Na3 Sn1 119.9(3) 2 37_665 Sn3 Na3 Sn1 63.08(6) 4 37_665 Sn3 Na3 Sn1 102.568(17) 3 37_665 Sn3 Na3 Sn1 152.98(6) 2 37_665 Na2 Na3 Sn1 142.2(2) . 37_665 Na2 Na3 Sn1 38.84(9) 9 37_665 Na2 Na3 Sn1 90.43(9) 5 37_665 Na3 Na3 Sn1 142.94(10) 4 37_665 Na3 Na3 Sn1 110.24(9) 3 37_665 Na3 Na3 Sn1 83.79(11) 2 37_665 Cu2 Na3 Sn1 53.10(4) 36_566 37_665 Cu2 Na3 Sn1 129.35(12) 35_665 37_665 Cu2 Na3 Sn1 154.0(2) 32_665 37_665 Cu2 Na3 Sn1 106.26(8) 31_656 37_665 Cu2 Na3 Sn1 75.51(5) 28_656 37_665 Cu2 Na3 Sn1 29.98(4) 27_566 37_665 Sn1 Na3 Sn1 103.40(14) 44_656 37_665 Sn1 Na3 Sn1 54.01(6) 10 37_665 Sn1 Na3 Sn1 130.0(2) 6 37_665 Sn2 Na3 Sn1 27.01(3) 10 47_566 Sn2 Na3 Sn1 119.9(3) 6 47_566 Sn2 Na3 Sn1 78.58(13) 2 47_566 Sn3 Na3 Sn1 152.98(6) 4 47_566 Sn3 Na3 Sn1 63.08(6) 3 47_566 Sn3 Na3 Sn1 102.568(17) 2 47_566 Na2 Na3 Sn1 38.84(9) . 47_566 Na2 Na3 Sn1 90.43(9) 9 47_566 Na2 Na3 Sn1 142.2(2) 5 47_566 Na3 Na3 Sn1 83.79(11) 4 47_566 Na3 Na3 Sn1 142.94(10) 3 47_566 Na3 Na3 Sn1 110.24(9) 2 47_566 Cu2 Na3 Sn1 154.0(2) 36_566 47_566 Cu2 Na3 Sn1 106.26(8) 35_665 47_566 Cu2 Na3 Sn1 75.51(5) 32_665 47_566 Cu2 Na3 Sn1 29.98(4) 31_656 47_566 Cu2 Na3 Sn1 53.10(4) 28_656 47_566 Cu2 Na3 Sn1 129.35(12) 27_566 47_566 Sn1 Na3 Sn1 103.40(14) 44_656 47_566 Sn1 Na3 Sn1 130.0(2) 10 47_566 Sn1 Na3 Sn1 53.76(6) 6 47_566 Sn1 Na3 Sn1 103.40(14) 37_665 47_566 Sn2 Na3 Sn1 27.01(3) 10 2 Sn2 Na3 Sn1 78.58(13) 6 2 Sn2 Na3 Sn1 119.9(3) 2 2 Sn3 Na3 Sn1 102.568(17) 4 2 Sn3 Na3 Sn1 63.08(6) 3 2 Sn3 Na3 Sn1 152.98(6) 2 2 Na2 Na3 Sn1 90.43(9) . 2 Na2 Na3 Sn1 38.84(9) 9 2 Na2 Na3 Sn1 142.2(2) 5 2 Na3 Na3 Sn1 110.24(9) 4 2 Na3 Na3 Sn1 142.94(10) 3 2 Na3 Na3 Sn1 83.79(11) 2 2 Cu2 Na3 Sn1 106.26(8) 36_566 2 Cu2 Na3 Sn1 154.0(2) 35_665 2 Cu2 Na3 Sn1 129.35(12) 32_665 2 Cu2 Na3 Sn1 53.10(4) 31_656 2 Cu2 Na3 Sn1 29.98(4) 28_656 2 Cu2 Na3 Sn1 75.51(5) 27_566 2 Sn1 Na3 Sn1 130.0(2) 44_656 2 Sn1 Na3 Sn1 103.40(14) 10 2 Sn1 Na3 Sn1 103.40(14) 6 2 Sn1 Na3 Sn1 53.76(6) 37_665 2 Sn1 Na3 Sn1 54.01(6) 47_566 2 Sn2 Na3 Sn3 117.8(2) 10 . Sn2 Na3 Sn3 117.8(2) 6 . Sn2 Na3 Sn3 117.8(2) 2 . Sn3 Na3 Sn3 58.87(19) 4 . Sn3 Na3 Sn3 58.87(19) 3 . Sn3 Na3 Sn3 58.87(19) 2 . Na2 Na3 Sn3 89.1(2) . . Na2 Na3 Sn3 89.1(2) 9 . Na2 Na3 Sn3 89.1(2) 5 . Na3 Na3 Sn3 35.3 4 . Na3 Na3 Sn3 35.3 3 . Na3 Na3 Sn3 35.3 2 . Cu2 Na3 Sn3 87.84(15) 36_566 . Cu2 Na3 Sn3 87.84(15) 35_665 . Cu2 Na3 Sn3 87.84(15) 32_665 . Cu2 Na3 Sn3 87.84(15) 31_656 . Cu2 Na3 Sn3 87.84(15) 28_656 . Cu2 Na3 Sn3 87.84(15) 27_566 . Sn1 Na3 Sn3 115.02(12) 44_656 . Sn1 Na3 Sn3 115.02(12) 10 . Sn1 Na3 Sn3 115.02(12) 6 . Sn1 Na3 Sn3 115.02(12) 37_665 . Sn1 Na3 Sn3 115.02(12) 47_566 . Sn1 Na3 Sn3 115.02(12) 2 . Sn2 Na3 Sn2 63.72(8) 10 3 Sn2 Na3 Sn2 154.47(2) 6 3 Sn2 Na3 Sn2 102.12(4) 2 3 Sn3 Na3 Sn2 114.2(3) 4 3 Sn3 Na3 Sn2 26.90(3) 3 3 Sn3 Na3 Sn2 74.90(13) 2 3 Na2 Na3 Sn2 39.22(10) . 3 Na2 Na3 Sn2 90.45(10) 9 3 Na2 Na3 Sn2 138.2(2) 5 3 Na3 Na3 Sn2 33.46(9) 4 3 Na3 Na3 Sn2 92.49(10) 3 3 Na3 Na3 Sn2 67.52(9) 2 3 Cu2 Na3 Sn2 147.1(2) 36_566 3 Cu2 Na3 Sn2 102.97(9) 35_665 3 Cu2 Na3 Sn2 73.19(6) 32_665 3 Cu2 Na3 Sn2 29.61(4) 31_656 3 Cu2 Na3 Sn2 52.77(5) 28_656 3 Cu2 Na3 Sn2 126.21(14) 27_566 3 Sn1 Na3 Sn2 126.108(17) 44_656 3 Sn1 Na3 Sn2 176.3(2) 10 3 Sn1 Na3 Sn2 78.004(10) 6 3 Sn1 Na3 Sn2 127.671(18) 37_665 3 Sn1 Na3 Sn2 53.637(10) 47_566 3 Sn1 Na3 Sn2 79.485(13) 2 3 Sn3 Na3 Sn2 61.39(11) . 3 Sn2 Na3 Sn2 154.47(2) 10 7 Sn2 Na3 Sn2 102.12(4) 6 7 Sn2 Na3 Sn2 63.72(8) 2 7 Sn3 Na3 Sn2 74.90(13) 4 7 Sn3 Na3 Sn2 114.2(3) 3 7 Sn3 Na3 Sn2 26.90(3) 2 7 Na2 Na3 Sn2 90.45(10) . 7 Na2 Na3 Sn2 138.2(2) 9 7 Na2 Na3 Sn2 39.22(10) 5 7 Na3 Na3 Sn2 67.52(9) 4 7 Na3 Na3 Sn2 33.46(9) 3 7 Na3 Na3 Sn2 92.49(10) 2 7 Cu2 Na3 Sn2 73.19(6) 36_566 7 Cu2 Na3 Sn2 29.61(4) 35_665 7 Cu2 Na3 Sn2 52.77(5) 32_665 7 Cu2 Na3 Sn2 126.21(14) 31_656 7 Cu2 Na3 Sn2 147.1(2) 28_656 7 Cu2 Na3 Sn2 102.97(9) 27_566 7 Sn1 Na3 Sn2 53.637(10) 44_656 7 Sn1 Na3 Sn2 78.004(11) 10 7 Sn1 Na3 Sn2 79.485(13) 6 7 Sn1 Na3 Sn2 126.108(17) 37_665 7 Sn1 Na3 Sn2 127.671(18) 47_566 7 Sn1 Na3 Sn2 176.3(2) 2 7 Sn3 Na3 Sn2 61.39(11) . 7 Sn2 Na3 Sn2 98.97(14) 3 7 Sn2 Na3 Sn2 154.47(2) 10 4 Sn2 Na3 Sn2 63.72(8) 6 4 Sn2 Na3 Sn2 102.12(4) 2 4 Sn3 Na3 Sn2 26.90(3) 4 4 Sn3 Na3 Sn2 114.2(3) 3 4 Sn3 Na3 Sn2 74.90(13) 2 4 Na2 Na3 Sn2 138.2(2) . 4 Na2 Na3 Sn2 90.45(10) 9 4 Na2 Na3 Sn2 39.22(10) 5 4 Na3 Na3 Sn2 92.49(10) 4 4 Na3 Na3 Sn2 33.46(10) 3 4 Na3 Na3 Sn2 67.52(9) 2 4 Cu2 Na3 Sn2 29.61(4) 36_566 4 Cu2 Na3 Sn2 73.19(6) 35_665 4 Cu2 Na3 Sn2 102.97(9) 32_665 4 Cu2 Na3 Sn2 147.1(2) 31_656 4 Cu2 Na3 Sn2 126.21(14) 28_656 4 Cu2 Na3 Sn2 52.77(5) 27_566 4 Sn1 Na3 Sn2 78.004(11) 44_656 4 Sn1 Na3 Sn2 53.637(10) 10 4 Sn1 Na3 Sn2 126.108(17) 6 4 Sn1 Na3 Sn2 79.485(13) 37_665 4 Sn1 Na3 Sn2 176.3(2) 47_566 4 Sn1 Na3 Sn2 127.671(18) 2 4 Sn3 Na3 Sn2 61.39(11) . 4 Sn2 Na3 Sn2 122.7(2) 3 4 Sn2 Na3 Sn2 50.41(6) 7 4 Sn2 Na3 Sn2 102.12(4) 10 12 Sn2 Na3 Sn2 154.47(2) 6 12 Sn2 Na3 Sn2 63.72(8) 2 12 Sn3 Na3 Sn2 114.2(3) 4 12 Sn3 Na3 Sn2 74.90(13) 3 12 Sn3 Na3 Sn2 26.90(3) 2 12 Na2 Na3 Sn2 39.22(10) . 12 Na2 Na3 Sn2 138.2(2) 9 12 Na2 Na3 Sn2 90.45(10) 5 12 Na3 Na3 Sn2 33.46(9) 4 12 Na3 Na3 Sn2 67.52(9) 3 12 Na3 Na3 Sn2 92.49(10) 2 12 Cu2 Na3 Sn2 126.21(14) 36_566 12 Cu2 Na3 Sn2 52.77(5) 35_665 12 Cu2 Na3 Sn2 29.61(4) 32_665 12 Cu2 Na3 Sn2 73.19(6) 31_656 12 Cu2 Na3 Sn2 102.97(9) 28_656 12 Cu2 Na3 Sn2 147.1(2) 27_566 12 Sn1 Na3 Sn2 79.485(13) 44_656 12 Sn1 Na3 Sn2 127.671(18) 10 12 Sn1 Na3 Sn2 53.637(10) 6 12 Sn1 Na3 Sn2 176.3(2) 37_665 12 Sn1 Na3 Sn2 78.004(11) 47_566 12 Sn1 Na3 Sn2 126.108(17) 2 12 Sn3 Na3 Sn2 61.39(11) . 12 Sn2 Na3 Sn2 50.41(6) 3 12 Sn2 Na3 Sn2 53.73(6) 7 12 Sn2 Na3 Sn2 98.97(14) 4 12 Sn2 Na3 Sn2 102.12(4) 10 11 Sn2 Na3 Sn2 63.72(8) 6 11 Sn2 Na3 Sn2 154.47(2) 2 11 Sn3 Na3 Sn2 26.90(3) 4 11 Sn3 Na3 Sn2 74.90(13) 3 11 Sn3 Na3 Sn2 114.2(3) 2 11 Na2 Na3 Sn2 138.2(2) . 11 Na2 Na3 Sn2 39.22(10) 9 11 Na2 Na3 Sn2 90.45(10) 5 11 Na3 Na3 Sn2 92.49(10) 4 11 Na3 Na3 Sn2 67.52(9) 3 11 Na3 Na3 Sn2 33.46(9) 2 11 Cu2 Na3 Sn2 52.77(5) 36_566 11 Cu2 Na3 Sn2 126.21(14) 35_665 11 Cu2 Na3 Sn2 147.1(2) 32_665 11 Cu2 Na3 Sn2 102.97(9) 31_656 11 Cu2 Na3 Sn2 73.19(6) 28_656 11 Cu2 Na3 Sn2 29.61(4) 27_566 11 Sn1 Na3 Sn2 127.671(18) 44_656 11 Sn1 Na3 Sn2 79.485(13) 10 11 Sn1 Na3 Sn2 176.3(2) 6 11 Sn1 Na3 Sn2 53.637(10) 37_665 11 Sn1 Na3 Sn2 126.108(17) 47_566 11 Sn1 Na3 Sn2 78.004(11) 2 11 Sn3 Na3 Sn2 61.39(11) . 11 Sn2 Na3 Sn2 98.97(14) 3 11 Sn2 Na3 Sn2 98.97(14) 7 11 Sn2 Na3 Sn2 53.73(6) 4 11 Sn2 Na3 Sn2 122.7(2) 12 11 Sn1 Na4 Sn1 53.02(2) 22_465 31_566 Sn1 Na4 Sn1 158.16(2) 22_465 24_666 Sn1 Na4 Sn1 106.895(9) 31_566 24_666 Sn1 Na4 Sn1 106.895(10) 22_465 29_666 Sn1 Na4 Sn1 158.16(2) 31_566 29_666 Sn1 Na4 Sn1 91.16(2) 24_666 29_666 Sn1 Na4 Sn1 91.16(2) 22_465 32_566 Sn1 Na4 Sn1 114.76(2) 31_566 32_566 Sn1 Na4 Sn1 106.895(9) 24_666 32_566 Sn1 Na4 Sn1 69.70(2) 29_666 32_566 Sn1 Na4 Sn1 114.76(2) 22_465 21_456 Sn1 Na4 Sn1 91.16(2) 31_566 21_456 Sn1 Na4 Sn1 69.70(2) 24_666 21_456 Sn1 Na4 Sn1 106.895(9) 29_666 21_456 Sn1 Na4 Sn1 53.02(2) 32_566 21_456 Sn1 Na4 Sn1 106.895(9) 22_465 30_666 Sn1 Na4 Sn1 69.70(2) 31_566 30_666 Sn1 Na4 Sn1 53.02(2) 24_666 30_666 Sn1 Na4 Sn1 114.76(2) 29_666 30_666 Sn1 Na4 Sn1 158.16(2) 32_566 30_666 Sn1 Na4 Sn1 106.895(9) 21_456 30_666 Sn1 Na4 Sn1 69.70(2) 22_465 23_655 Sn1 Na4 Sn1 106.895(9) 31_566 23_655 Sn1 Na4 Sn1 114.76(2) 24_666 23_655 Sn1 Na4 Sn1 53.02(2) 29_666 23_655 Sn1 Na4 Sn1 106.895(9) 32_566 23_655 Sn1 Na4 Sn1 158.16(2) 21_456 23_655 Sn1 Na4 Sn1 91.16(2) 30_666 23_655 Sn1 Na4 Na1 147.96(6) 22_465 29_666 Sn1 Na4 Na1 147.96(6) 31_566 29_666 Sn1 Na4 Na1 53.60(5) 24_666 29_666 Sn1 Na4 Na1 53.60(5) 29_666 29_666 Sn1 Na4 Na1 59.46(9) 32_566 29_666 Sn1 Na4 Na1 59.46(9) 21_456 29_666 Sn1 Na4 Na1 104.71(7) 30_666 29_666 Sn1 Na4 Na1 104.71(7) 23_655 29_666 Sn1 Na4 Na1 59.46(9) 22_465 30_666 Sn1 Na4 Na1 59.46(9) 31_566 30_666 Sn1 Na4 Na1 104.71(7) 24_666 30_666 Sn1 Na4 Na1 104.71(7) 29_666 30_666 Sn1 Na4 Na1 147.96(6) 32_566 30_666 Sn1 Na4 Na1 147.96(6) 21_456 30_666 Sn1 Na4 Na1 53.60(5) 30_666 30_666 Sn1 Na4 Na1 53.60(5) 23_655 30_666 Na1 Na4 Na1 143.3(2) 29_666 30_666 Sn1 Na4 Na1 53.60(5) 22_465 32_566 Sn1 Na4 Na1 104.71(7) 31_566 32_566 Sn1 Na4 Na1 147.96(6) 24_666 32_566 Sn1 Na4 Na1 59.46(9) 29_666 32_566 Sn1 Na4 Na1 53.60(5) 32_566 32_566 Sn1 Na4 Na1 104.71(7) 21_456 32_566 Sn1 Na4 Na1 147.96(6) 30_666 32_566 Sn1 Na4 Na1 59.46(9) 23_655 32_566 Na1 Na4 Na1 95.69(6) 29_666 32_566 Na1 Na4 Na1 95.69(6) 30_666 32_566 Sn1 Na4 Na1 104.71(7) 22_465 31_566 Sn1 Na4 Na1 53.60(5) 31_566 31_566 Sn1 Na4 Na1 59.46(9) 24_666 31_566 Sn1 Na4 Na1 147.96(6) 29_666 31_566 Sn1 Na4 Na1 104.71(7) 32_566 31_566 Sn1 Na4 Na1 53.60(5) 21_456 31_566 Sn1 Na4 Na1 59.46(9) 30_666 31_566 Sn1 Na4 Na1 147.96(6) 23_655 31_566 Na1 Na4 Na1 95.69(6) 29_666 31_566 Na1 Na4 Na1 95.69(6) 30_666 31_566 Na1 Na4 Na1 143.3(2) 32_566 31_566 Sn1 Na4 Na2 57.378(10) 22_465 26_566 Sn1 Na4 Na2 57.378(10) 31_566 26_566 Sn1 Na4 Na2 122.622(10) 24_666 26_566 Sn1 Na4 Na2 122.622(10) 29_666 26_566 Sn1 Na4 Na2 57.378(10) 32_566 26_566 Sn1 Na4 Na2 57.378(10) 21_456 26_566 Sn1 Na4 Na2 122.622(10) 30_666 26_566 Sn1 Na4 Na2 122.622(10) 23_655 26_566 Na1 Na4 Na2 108.35(11) 29_666 26_566 Na1 Na4 Na2 108.35(11) 30_666 26_566 Na1 Na4 Na2 71.65(11) 32_566 26_566 Na1 Na4 Na2 71.65(11) 31_566 26_566 Sn1 Na4 Na2 122.622(10) 22_465 25_666 Sn1 Na4 Na2 122.622(10) 31_566 25_666 Sn1 Na4 Na2 57.378(10) 24_666 25_666 Sn1 Na4 Na2 57.378(10) 29_666 25_666 Sn1 Na4 Na2 122.622(10) 32_566 25_666 Sn1 Na4 Na2 122.622(10) 21_456 25_666 Sn1 Na4 Na2 57.378(10) 30_666 25_666 Sn1 Na4 Na2 57.378(10) 23_655 25_666 Na1 Na4 Na2 71.65(11) 29_666 25_666 Na1 Na4 Na2 71.65(11) 30_666 25_666 Na1 Na4 Na2 108.35(11) 32_566 25_666 Na1 Na4 Na2 108.35(11) 31_566 25_666 Na2 Na4 Na2 180.0 26_566 25_666 Sn1 Na4 Sn1 26.671(14) 22_465 10 Sn1 Na4 Sn1 59.555(13) 31_566 10 Sn1 Na4 Sn1 140.375(10) 24_666 10 Sn1 Na4 Sn1 98.695(9) 29_666 10 Sn1 Na4 Sn1 112.541(6) 32_566 10 Sn1 Na4 Sn1 140.375(10) 21_456 10 Sn1 Na4 Sn1 88.407(14) 30_666 10 Sn1 Na4 Sn1 49.694(14) 23_655 10 Na1 Na4 Sn1 152.19(4) 29_666 10 Na1 Na4 Sn1 35.66(7) 30_666 10 Na1 Na4 Sn1 63.426(7) 32_566 10 Na1 Na4 Sn1 112.04(3) 31_566 10 Na2 Na4 Sn1 83.430(6) 26_566 10 Na2 Na4 Sn1 96.570(6) 25_666 10 Sn1 Na4 Sn1 59.555(13) 22_465 37_665 Sn1 Na4 Sn1 26.671(14) 31_566 37_665 Sn1 Na4 Sn1 98.695(9) 24_666 37_665 Sn1 Na4 Sn1 140.375(10) 29_666 37_665 Sn1 Na4 Sn1 140.375(10) 32_566 37_665 Sn1 Na4 Sn1 112.541(6) 21_456 37_665 Sn1 Na4 Sn1 49.694(14) 30_666 37_665 Sn1 Na4 Sn1 88.407(14) 23_655 37_665 Na1 Na4 Sn1 152.19(4) 29_666 37_665 Na1 Na4 Sn1 35.66(7) 30_666 37_665 Na1 Na4 Sn1 112.04(3) 32_566 37_665 Na1 Na4 Sn1 63.426(7) 31_566 37_665 Na2 Na4 Sn1 83.430(6) 26_566 37_665 Na2 Na4 Sn1 96.570(6) 25_666 37_665 Sn1 Na4 Sn1 51.364(12) 10 37_665 Sn1 Na4 Sn1 140.375(10) 22_465 12_566 Sn1 Na4 Sn1 112.541(6) 31_566 12_566 Sn1 Na4 Sn1 49.694(14) 24_666 12_566 Sn1 Na4 Sn1 88.407(14) 29_666 12_566 Sn1 Na4 Sn1 59.555(13) 32_566 12_566 Sn1 Na4 Sn1 26.671(14) 21_456 12_566 Sn1 Na4 Sn1 98.695(9) 30_666 12_566 Sn1 Na4 Sn1 140.375(10) 23_655 12_566 Na1 Na4 Sn1 35.66(7) 29_666 12_566 Na1 Na4 Sn1 152.19(4) 30_666 12_566 Na1 Na4 Sn1 112.04(3) 32_566 12_566 Na1 Na4 Sn1 63.426(7) 31_566 12_566 Na2 Na4 Sn1 83.430(6) 26_566 12_566 Na2 Na4 Sn1 96.570(6) 25_666 12_566 Sn1 Na4 Sn1 166.860(12) 10 12_566 Sn1 Na4 Sn1 126.740(12) 37_665 12_566 Sn1 Na4 Sn1 112.541(6) 22_465 39_667 Sn1 Na4 Sn1 140.375(10) 31_566 39_667 Sn1 Na4 Sn1 88.407(14) 24_666 39_667 Sn1 Na4 Sn1 49.694(14) 29_666 39_667 Sn1 Na4 Sn1 26.671(14) 32_566 39_667 Sn1 Na4 Sn1 59.555(13) 21_456 39_667 Sn1 Na4 Sn1 140.375(10) 30_666 39_667 Sn1 Na4 Sn1 98.695(9) 23_655 39_667 Na1 Na4 Sn1 35.66(7) 29_666 39_667 Na1 Na4 Sn1 152.19(4) 30_666 39_667 Na1 Na4 Sn1 63.426(7) 32_566 39_667 Na1 Na4 Sn1 112.04(3) 31_566 39_667 Na2 Na4 Sn1 83.430(6) 26_566 39_667 Na2 Na4 Sn1 96.570(6) 25_666 39_667 Sn1 Na4 Sn1 126.740(12) 10 39_667 Sn1 Na4 Sn1 166.860(12) 37_665 39_667 Sn1 Na4 Sn1 51.364(12) 12_566 39_667 Sn1 Na4 Sn1 140.375(10) 22_465 9_556 Sn1 Na4 Sn1 88.407(14) 31_566 9_556 Sn1 Na4 Sn1 26.671(14) 24_666 9_556 Sn1 Na4 Sn1 112.541(6) 29_666 9_556 Sn1 Na4 Sn1 98.695(9) 32_566 9_556 Sn1 Na4 Sn1 49.694(14) 21_456 9_556 Sn1 Na4 Sn1 59.555(13) 30_666 9_556 Sn1 Na4 Sn1 140.375(10) 23_655 9_556 Na1 Na4 Sn1 63.426(7) 29_666 9_556 Na1 Na4 Sn1 112.04(3) 30_666 9_556 Na1 Na4 Sn1 152.19(4) 32_566 9_556 Na1 Na4 Sn1 35.66(7) 31_566 9_556 Na2 Na4 Sn1 96.570(6) 26_566 9_556 Na2 Na4 Sn1 83.430(6) 25_666 9_556 Sn1 Na4 Sn1 141.989(12) 10 9_556 Sn1 Na4 Sn1 90.750(1) 37_665 9_556 Sn1 Na4 Sn1 40.385(12) 12_566 9_556 Sn1 Na4 Sn1 90.750(1) 39_667 9_556 Sn1 Na4 Sn1 88.407(14) 22_465 38_565 Sn1 Na4 Sn1 140.375(10) 31_566 38_565 Sn1 Na4 Sn1 112.541(6) 24_666 38_565 Sn1 Na4 Sn1 26.671(14) 29_666 38_565 Sn1 Na4 Sn1 49.694(14) 32_566 38_565 Sn1 Na4 Sn1 98.695(9) 21_456 38_565 Sn1 Na4 Sn1 140.375(10) 30_666 38_565 Sn1 Na4 Sn1 59.555(13) 23_655 38_565 Na1 Na4 Sn1 63.426(7) 29_666 38_565 Na1 Na4 Sn1 112.04(3) 30_666 38_565 Na1 Na4 Sn1 35.66(7) 32_566 38_565 Na1 Na4 Sn1 152.19(4) 31_566 38_565 Na2 Na4 Sn1 96.570(6) 26_566 38_565 Na2 Na4 Sn1 83.430(6) 25_666 38_565 Sn1 Na4 Sn1 90.750(1) 10 38_565 Sn1 Na4 Sn1 141.989(12) 37_665 38_565 Sn1 Na4 Sn1 90.750(1) 12_566 38_565 Sn1 Na4 Sn1 40.385(12) 39_667 38_565 Sn1 Na4 Sn1 126.740(12) 9_556 38_565 Sn1 Na4 Sn1 98.695(9) 22_465 40_567 Sn1 Na4 Sn1 49.694(14) 31_566 40_567 Sn1 Na4 Sn1 59.555(13) 24_666 40_567 Sn1 Na4 Sn1 140.375(10) 29_666 40_567 Sn1 Na4 Sn1 140.375(10) 32_566 40_567 Sn1 Na4 Sn1 88.407(14) 21_456 40_567 Sn1 Na4 Sn1 26.671(14) 30_666 40_567 Sn1 Na4 Sn1 112.541(6) 23_655 40_567 Na1 Na4 Sn1 112.04(3) 29_666 40_567 Na1 Na4 Sn1 63.426(7) 30_666 40_567 Na1 Na4 Sn1 152.19(4) 32_566 40_567 Na1 Na4 Sn1 35.66(7) 31_566 40_567 Na2 Na4 Sn1 96.570(6) 26_566 40_567 Na2 Na4 Sn1 83.430(6) 25_666 40_567 Sn1 Na4 Sn1 90.750(1) 10 40_567 Sn1 Na4 Sn1 40.385(12) 37_665 40_567 Sn1 Na4 Sn1 90.750(1) 12_566 40_567 Sn1 Na4 Sn1 141.989(12) 39_667 40_567 Sn1 Na4 Sn1 51.364(12) 9_556 40_567 Sn1 Na4 Sn1 166.860(12) 38_565 40_567 Sn1 Na4 Sn1 49.694(14) 22_465 11_565 Sn1 Na4 Sn1 98.695(9) 31_566 11_565 Sn1 Na4 Sn1 140.375(10) 24_666 11_565 Sn1 Na4 Sn1 59.555(13) 29_666 11_565 Sn1 Na4 Sn1 88.407(14) 32_566 11_565 Sn1 Na4 Sn1 140.375(10) 21_456 11_565 Sn1 Na4 Sn1 112.541(6) 30_666 11_565 Sn1 Na4 Sn1 26.671(14) 23_655 11_565 Na1 Na4 Sn1 112.04(3) 29_666 11_565 Na1 Na4 Sn1 63.426(7) 30_666 11_565 Na1 Na4 Sn1 35.66(7) 32_566 11_565 Na1 Na4 Sn1 152.19(4) 31_566 11_565 Na2 Na4 Sn1 96.570(6) 26_566 11_565 Na2 Na4 Sn1 83.430(6) 25_666 11_565 Sn1 Na4 Sn1 40.385(12) 10 11_565 Sn1 Na4 Sn1 90.750(1) 37_665 11_565 Sn1 Na4 Sn1 141.989(12) 12_566 11_565 Sn1 Na4 Sn1 90.750(1) 39_667 11_565 Sn1 Na4 Sn1 166.860(12) 9_556 11_565 Sn1 Na4 Sn1 51.364(12) 38_565 11_565 Sn1 Na4 Sn1 126.740(12) 40_567 11_565 Sn1 Na4 Sn2 124.150(13) 22_465 27_666 Sn1 Na4 Sn2 157.291(13) 31_566 27_666 Sn1 Na4 Sn2 70.244(13) 24_666 27_666 Sn1 Na4 Sn2 23.672(13) 29_666 27_666 Sn1 Na4 Sn2 87.031(13) 32_566 27_666 Sn1 Na4 Sn2 108.019(13) 21_456 27_666 Sn1 Na4 Sn2 92.589(13) 30_666 27_666 Sn1 Na4 Sn2 57.814(13) 23_655 27_666 Na1 Na4 Sn2 48.58(9) 29_666 27_666 Na1 Na4 Sn2 98.81(10) 30_666 27_666 Na1 Na4 Sn2 82.55(10) 32_566 27_666 Na1 Na4 Sn2 129.66(9) 31_566 27_666 Na2 Na4 Sn2 143.857(8) 26_566 27_666 Na2 Na4 Sn2 36.143(8) 25_666 27_666 Sn1 Na4 Sn2 107.505(10) 10 27_666 Sn1 Na4 Sn2 130.648(10) 37_665 27_666 Sn1 Na4 Sn2 83.339(10) 12_566 27_666 Sn1 Na4 Sn2 62.186(10) 39_667 27_666 Sn1 Na4 Sn2 94.772(10) 9_556 27_666 Sn1 Na4 Sn2 50.207(10) 38_565 27_666 Sn1 Na4 Sn2 117.079(10) 40_567 27_666 Sn1 Na4 Sn2 74.456(10) 11_565 27_666 Sn1 Na4 Sn2 157.291(13) 22_465 36_666 Sn1 Na4 Sn2 124.150(13) 31_566 36_666 Sn1 Na4 Sn2 23.672(13) 24_666 36_666 Sn1 Na4 Sn2 70.244(13) 29_666 36_666 Sn1 Na4 Sn2 108.019(13) 32_566 36_666 Sn1 Na4 Sn2 87.031(13) 21_456 36_666 Sn1 Na4 Sn2 57.814(13) 30_666 36_666 Sn1 Na4 Sn2 92.589(13) 23_655 36_666 Na1 Na4 Sn2 48.58(9) 29_666 36_666 Na1 Na4 Sn2 98.81(10) 30_666 36_666 Na1 Na4 Sn2 129.66(9) 32_566 36_666 Na1 Na4 Sn2 82.55(10) 31_566 36_666 Na2 Na4 Sn2 143.857(8) 26_566 36_666 Na2 Na4 Sn2 36.143(8) 25_666 36_666 Sn1 Na4 Sn2 130.648(10) 10 36_666 Sn1 Na4 Sn2 107.505(10) 37_665 36_666 Sn1 Na4 Sn2 62.186(10) 12_566 36_666 Sn1 Na4 Sn2 83.339(10) 39_667 36_666 Sn1 Na4 Sn2 50.207(10) 9_556 36_666 Sn1 Na4 Sn2 94.772(10) 38_565 36_666 Sn1 Na4 Sn2 74.456(10) 40_567 36_666 Sn1 Na4 Sn2 117.079(10) 11_565 36_666 Sn2 Na4 Sn2 47.721(16) 27_666 36_666 Sn1 Na4 Sn2 23.672(13) 22_465 35_566 Sn1 Na4 Sn2 57.814(13) 31_566 35_566 Sn1 Na4 Sn2 157.291(13) 24_666 35_566 Sn1 Na4 Sn2 108.019(13) 29_666 35_566 Sn1 Na4 Sn2 70.244(13) 32_566 35_566 Sn1 Na4 Sn2 92.589(13) 21_456 35_566 Sn1 Na4 Sn2 124.150(13) 30_666 35_566 Sn1 Na4 Sn2 87.031(13) 23_655 35_566 Na1 Na4 Sn2 129.66(9) 29_666 35_566 Na1 Na4 Sn2 82.55(10) 30_666 35_566 Na1 Na4 Sn2 48.58(9) 32_566 35_566 Na1 Na4 Sn2 98.81(10) 31_566 35_566 Na2 Na4 Sn2 36.143(8) 26_566 35_566 Na2 Na4 Sn2 143.857(8) 25_666 35_566 Sn1 Na4 Sn2 50.207(10) 10 35_566 Sn1 Na4 Sn2 74.456(10) 37_665 35_566 Sn1 Na4 Sn2 117.079(10) 12_566 35_566 Sn1 Na4 Sn2 94.772(10) 39_667 35_566 Sn1 Na4 Sn2 130.648(10) 9_556 35_566 Sn1 Na4 Sn2 83.339(10) 38_565 35_566 Sn1 Na4 Sn2 107.505(10) 40_567 35_566 Sn1 Na4 Sn2 62.186(10) 11_565 35_566 Sn2 Na4 Sn2 130.702(10) 27_666 35_566 Sn2 Na4 Sn2 177.997(17) 36_666 35_566 Sn1 Na4 Sn2 57.814(13) 22_465 28_566 Sn1 Na4 Sn2 23.672(13) 31_566 28_566 Sn1 Na4 Sn2 108.019(13) 24_666 28_566 Sn1 Na4 Sn2 157.291(13) 29_666 28_566 Sn1 Na4 Sn2 92.589(13) 32_566 28_566 Sn1 Na4 Sn2 70.244(13) 21_456 28_566 Sn1 Na4 Sn2 87.031(13) 30_666 28_566 Sn1 Na4 Sn2 124.149(13) 23_655 28_566 Na1 Na4 Sn2 129.66(9) 29_666 28_566 Na1 Na4 Sn2 82.55(10) 30_666 28_566 Na1 Na4 Sn2 98.81(10) 32_566 28_566 Na1 Na4 Sn2 48.58(9) 31_566 28_566 Na2 Na4 Sn2 36.143(8) 26_566 28_566 Na2 Na4 Sn2 143.857(8) 25_666 28_566 Sn1 Na4 Sn2 74.456(10) 10 28_566 Sn1 Na4 Sn2 50.207(10) 37_665 28_566 Sn1 Na4 Sn2 94.772(10) 12_566 28_566 Sn1 Na4 Sn2 117.079(10) 39_667 28_566 Sn1 Na4 Sn2 83.339(10) 9_556 28_566 Sn1 Na4 Sn2 130.648(10) 38_565 28_566 Sn1 Na4 Sn2 62.186(10) 40_567 28_566 Sn1 Na4 Sn2 107.505(10) 11_565 28_566 Sn2 Na4 Sn2 177.997(16) 27_666 28_566 Sn2 Na4 Sn2 130.702(10) 36_666 28_566 Sn2 Na4 Sn2 50.838(17) 35_566 28_566 Sn1 Na4 Sn2 70.244(13) 22_465 25_566 Sn1 Na4 Sn2 92.589(13) 31_566 25_566 Sn1 Na4 Sn2 124.150(13) 24_666 25_566 Sn1 Na4 Sn2 87.031(13) 29_666 25_566 Sn1 Na4 Sn2 23.672(13) 32_566 25_566 Sn1 Na4 Sn2 57.814(13) 21_456 25_566 Sn1 Na4 Sn2 157.291(13) 30_666 25_566 Sn1 Na4 Sn2 108.019(13) 23_655 25_566 Na1 Na4 Sn2 82.55(10) 29_666 25_566 Na1 Na4 Sn2 129.66(9) 30_666 25_566 Na1 Na4 Sn2 48.58(9) 32_566 25_566 Na1 Na4 Sn2 98.81(10) 31_566 25_566 Na2 Na4 Sn2 36.143(8) 26_566 25_566 Na2 Na4 Sn2 143.857(8) 25_666 25_566 Sn1 Na4 Sn2 94.772(10) 10 25_566 Sn1 Na4 Sn2 117.079(10) 37_665 25_566 Sn1 Na4 Sn2 74.456(10) 12_566 25_566 Sn1 Na4 Sn2 50.207(10) 39_667 25_566 Sn1 Na4 Sn2 107.505(10) 9_556 25_566 Sn1 Na4 Sn2 62.186(10) 38_565 25_566 Sn1 Na4 Sn2 130.648(10) 40_567 25_566 Sn1 Na4 Sn2 83.339(10) 11_565 25_566 Sn2 Na4 Sn2 107.750(16) 27_666 25_566 Sn2 Na4 Sn2 130.702(10) 36_666 25_566 Sn2 Na4 Sn2 47.721(16) 35_566 25_566 Sn2 Na4 Sn2 72.287(16) 28_566 25_566 Sn1 Na4 Sn2 108.019(13) 22_465 26_666 Sn1 Na4 Sn2 87.031(13) 31_566 26_666 Sn1 Na4 Sn2 57.814(13) 24_666 26_666 Sn1 Na4 Sn2 92.589(13) 29_666 26_666 Sn1 Na4 Sn2 157.291(13) 32_566 26_666 Sn1 Na4 Sn2 124.150(13) 21_456 26_666 Sn1 Na4 Sn2 23.672(13) 30_666 26_666 Sn1 Na4 Sn2 70.244(13) 23_655 26_666 Na1 Na4 Sn2 98.81(10) 29_666 26_666 Na1 Na4 Sn2 48.58(9) 30_666 26_666 Na1 Na4 Sn2 129.66(9) 32_566 26_666 Na1 Na4 Sn2 82.55(10) 31_566 26_666 Na2 Na4 Sn2 143.857(8) 26_566 26_666 Na2 Na4 Sn2 36.143(8) 25_666 26_666 Sn1 Na4 Sn2 83.339(10) 10 26_666 Sn1 Na4 Sn2 62.186(10) 37_665 26_666 Sn1 Na4 Sn2 107.505(10) 12_566 26_666 Sn1 Na4 Sn2 130.648(10) 39_667 26_666 Sn1 Na4 Sn2 74.456(10) 9_556 26_666 Sn1 Na4 Sn2 117.079(10) 38_565 26_666 Sn1 Na4 Sn2 50.207(10) 40_567 26_666 Sn1 Na4 Sn2 94.772(10) 11_565 26_666 Sn2 Na4 Sn2 72.287(16) 27_666 26_666 Sn2 Na4 Sn2 50.838(17) 36_666 26_666 Sn2 Na4 Sn2 130.702(10) 35_566 26_666 Sn2 Na4 Sn2 107.750(16) 28_566 26_666 Sn2 Na4 Sn2 177.997(16) 25_566 26_666 Sn1 Na4 Sn2 92.589(13) 22_465 33_566 Sn1 Na4 Sn2 70.244(13) 31_566 33_566 Sn1 Na4 Sn2 87.031(13) 24_666 33_566 Sn1 Na4 Sn2 124.150(13) 29_666 33_566 Sn1 Na4 Sn2 57.814(13) 32_566 33_566 Sn1 Na4 Sn2 23.672(13) 21_456 33_566 Sn1 Na4 Sn2 108.019(13) 30_666 33_566 Sn1 Na4 Sn2 157.291(13) 23_655 33_566 Na1 Na4 Sn2 82.55(10) 29_666 33_566 Na1 Na4 Sn2 129.66(9) 30_666 33_566 Na1 Na4 Sn2 98.81(10) 32_566 33_566 Na1 Na4 Sn2 48.58(9) 31_566 33_566 Na2 Na4 Sn2 36.143(8) 26_566 33_566 Na2 Na4 Sn2 143.857(8) 25_666 33_566 Sn1 Na4 Sn2 117.079(10) 10 33_566 Sn1 Na4 Sn2 94.772(10) 37_665 33_566 Sn1 Na4 Sn2 50.207(10) 12_566 33_566 Sn1 Na4 Sn2 74.456(10) 39_667 33_566 Sn1 Na4 Sn2 62.186(10) 9_556 33_566 Sn1 Na4 Sn2 107.505(10) 38_565 33_566 Sn1 Na4 Sn2 83.339(10) 40_567 33_566 Sn1 Na4 Sn2 130.648(10) 11_565 33_566 Sn2 Na4 Sn2 130.702(10) 27_666 33_566 Sn2 Na4 Sn2 107.750(16) 36_666 33_566 Sn2 Na4 Sn2 72.287(16) 35_566 33_566 Sn2 Na4 Sn2 47.721(16) 28_566 33_566 Sn2 Na4 Sn2 50.838(17) 25_566 33_566 Sn2 Na4 Sn2 130.702(10) 26_666 33_566 Sn1 Na4 Sn2 87.031(13) 22_465 34_666 Sn1 Na4 Sn2 108.019(13) 31_566 34_666 Sn1 Na4 Sn2 92.589(13) 24_666 34_666 Sn1 Na4 Sn2 57.814(13) 29_666 34_666 Sn1 Na4 Sn2 124.150(13) 32_566 34_666 Sn1 Na4 Sn2 157.291(13) 21_456 34_666 Sn1 Na4 Sn2 70.244(13) 30_666 34_666 Sn1 Na4 Sn2 23.672(13) 23_655 34_666 Na1 Na4 Sn2 98.81(10) 29_666 34_666 Na1 Na4 Sn2 48.58(9) 30_666 34_666 Na1 Na4 Sn2 82.55(10) 32_566 34_666 Na1 Na4 Sn2 129.66(9) 31_566 34_666 Na2 Na4 Sn2 143.857(8) 26_566 34_666 Na2 Na4 Sn2 36.143(8) 25_666 34_666 Sn1 Na4 Sn2 62.186(10) 10 34_666 Sn1 Na4 Sn2 83.339(10) 37_665 34_666 Sn1 Na4 Sn2 130.648(10) 12_566 34_666 Sn1 Na4 Sn2 107.505(10) 39_667 34_666 Sn1 Na4 Sn2 117.079(10) 9_556 34_666 Sn1 Na4 Sn2 74.456(10) 38_565 34_666 Sn1 Na4 Sn2 94.772(10) 40_567 34_666 Sn1 Na4 Sn2 50.207(10) 11_565 34_666 Sn2 Na4 Sn2 50.838(17) 27_666 34_666 Sn2 Na4 Sn2 72.287(16) 36_666 34_666 Sn2 Na4 Sn2 107.750(16) 35_566 34_666 Sn2 Na4 Sn2 130.702(10) 28_566 34_666 Sn2 Na4 Sn2 130.702(10) 25_566 34_666 Sn2 Na4 Sn2 47.721(16) 26_666 34_666 Sn2 Na4 Sn2 177.997(17) 33_566 34_666 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Sn1 Cu2 2.7639(14) 27_566 Sn1 Cu1 2.7668(13) 27_566 Sn1 Cu1 2.7718(9) 12 Sn1 Sn2 3.0827(8) 11 Sn1 Sn1 3.0957(12) 19_566 Sn1 Sn1 3.1255(12) 37_665 Sn1 Na1 3.231(4) . Sn1 Na4 3.5010(6) 33_666 Sn1 Na2 3.528(5) 9 Sn1 Na1 3.539(5) 35_556 Sn1 Na1 3.553(7) 4_556 Sn1 Sn1 4.0010(12) 4_556 Sn1 Sn1 5.0012(12) 38 Sn2 Cu1 2.7480(16) 2 Sn2 Cu2 2.7960(9) 34 Sn2 Cu2 2.7960(9) 30 Sn2 Sn1 3.0827(8) 42_566 Sn2 Sn1 3.0827(8) 8 Sn2 Sn3 3.1331(10) . Sn2 Na3 3.141(6) 2 Sn2 Na1 3.484(6) 25_556 Sn2 Na2 3.644(3) 6 Sn2 Na2 3.644(3) 2 Sn2 Sn2 4.8137(14) 11 Sn2 Sn2 4.8137(14) 8 Sn3 Cu2 2.7178(19) 34 Sn3 Cu2 2.7178(19) 30 Sn3 Cu2 2.7178(19) 26 Sn3 Sn2 3.1332(10) 9 Sn3 Sn2 3.1332(10) 5 Sn3 Na3 3.229(6) 4 Sn3 Na3 3.229(6) 3 Sn3 Na3 3.229(6) 2 Sn3 Na2 3.681(7) 10 Sn3 Na2 3.681(7) 6 Sn3 Na2 3.681(7) 2 Sn3 Sn3 4.788(2) 4 Sn3 Sn3 4.788(2) 3 Sn3 Sn3 4.788(2) 2 Sn4 Cu2 2.6305(14) 34 Sn4 Cu2 2.6305(14) 10 Sn4 Cu2 2.6305(14) 30 Sn4 Cu2 2.6305(14) 6 Sn4 Cu2 2.6305(14) 26 Sn4 Cu2 2.6305(14) 2 Sn4 Cu1 2.6312(15) 34 Sn4 Cu1 2.6312(15) 10 Sn4 Cu1 2.6312(15) 30 Sn4 Cu1 2.6312(15) 6 Sn4 Cu1 2.6312(15) 26 Sn4 Cu1 2.6312(15) 2 Cu1 Sn4 2.6312(15) 2 Cu1 Cu2 2.742(2) . Cu1 Sn2 2.7480(16) 2 Cu1 Cu1 2.7619(17) 35_665 Cu1 Cu1 2.7619(17) 32_665 Cu1 Sn1 2.7668(13) 16_654 Cu1 Sn1 2.7668(13) 27_665 Cu1 Cu2 2.7675(15) 35_665 Cu1 Cu2 2.7675(15) 32_665 Cu1 Sn1 2.7718(9) 6 Cu1 Sn1 2.7718(9) 44_656 Cu1 Na1 3.196(7) 26_666 Cu2 Sn4 2.6305(14) 2 Cu2 Sn3 2.7178(19) 26_665 Cu2 Sn1 2.7639(14) 27_665 Cu2 Sn1 2.7639(14) 16_654 Cu2 Cu1 2.7675(15) 35_665 Cu2 Cu1 2.7675(15) 32_665 Cu2 Cu2 2.792(3) 11 Cu2 Cu2 2.792(3) 8 Cu2 Sn2 2.7961(9) 31_665 Cu2 Sn2 2.7961(9) 36_665 Cu2 Na2 3.2572(16) 34_665 Na1 Cu1 3.197(7) 26_556 Na1 Sn1 3.231(4) 38 Na1 Sn2 3.484(6) 25_556 Na1 Sn1 3.539(5) 18_545 Na1 Sn1 3.539(5) 32_556 Na1 Sn1 3.553(7) 4_556 Na1 Sn1 3.553(7) 39_657 Na1 Na4 3.658(7) 33_666 Na1 Na1 3.869(8) 35_556 Na1 Na1 3.869(8) 32_556 Na2 Cu2 3.2572(16) 32_665 Na2 Cu2 3.2572(16) 31_656 Na2 Sn1 3.528(5) 47_566 Na2 Sn1 3.528(5) 6 Na2 Sn1 3.528(5) 5 Na2 Sn1 3.528(5) 48 Na2 Sn2 3.644(3) 12 Na2 Sn2 3.644(3) 3 Na2 Sn2 3.644(3) 10 Na2 Sn2 3.644(3) 2 Na2 Na3 3.666(8) 4 Na2 Na3 3.666(8) . Na2 Sn3 3.681(7) 3 Na2 Sn3 3.681(7) 2 Na2 Na4 3.824(9) 25_666 Na3 Sn2 3.141(6) 10 Na3 Sn2 3.141(6) 6 Na3 Sn2 3.141(6) 2 Na3 Sn3 3.229(6) 4 Na3 Sn3 3.229(6) 3 Na3 Sn3 3.229(6) 2 Na3 Na2 3.666(8) 9 Na3 Na2 3.666(8) 5 Na4 Sn1 3.5010(6) 22_465 Na4 Sn1 3.5010(6) 31_566 Na4 Sn1 3.5010(6) 24_666 Na4 Sn1 3.5010(6) 29_666 Na4 Sn1 3.5010(6) 32_566 Na4 Sn1 3.5010(6) 21_456 Na4 Sn1 3.5010(6) 30_666 Na4 Sn1 3.5010(6) 23_655 Na4 Na1 3.658(7) 29_666 Na4 Na1 3.658(7) 30_666 Na4 Na1 3.658(7) 32_566 Na4 Na1 3.658(7) 31_566 Na4 Na2 3.824(10) 26_566 Na4 Na2 3.824(10) 25_666 _journal_paper_doi 10.1021/ja205934p