Crystallography Open Database

Information card for entry 4108189

Preview

Coordinates	4108189.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H26 B Cl N8 O Ru
Calculated formula	C24 H15 B Cl N8 O Ru
Title of publication	N-C Bond Formation of NO Ligands on Ruthenium Complexes with Concurrent Vinylic C-H Activation and Subsequent Proton-Induced Reactivities of the Resulting Nitrosovinyl Species
Authors of publication	Yasuhiro Arikawa; Taiki Asayama; Kazuki Itatani; Masayoshi Onishi
Journal of publication	Journal of the American Chemical Society
Year of publication	2008
Journal volume	130
Pages of publication	10508 - 10509
a	9.8644 ± 0.0005 Å
b	19.8973 ± 0.0009 Å
c	14.6625 ± 0.0008 Å
α	90°
β	106.73 ± 0.0005°
γ	90°
Cell volume	2756.1 ± 0.2 Å³
Cell temperature	296.1 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for significantly intense reflections	0.0419
Weighted residual factors for all reflections included in the refinement	0.1244
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4108189.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4108189.cif
56525	2012-05-11	cif/ Adding structures of 4108189 via cif-deposit CGI script.	4108189.cif