Crystallography Open Database

Information card for entry 4108383

Preview

Coordinates	4108383.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30.5 H58 N Ni P2
Calculated formula	C30.5 H58 N Ni P2
Title of publication	η2-Organoazide Complexes of Nickel and Their Conversion to Terminal Imido Complexes via Dinitrogen Extrusion
Authors of publication	Rory Waterman; Gregory L. Hillhouse
Journal of publication	Journal of the American Chemical Society
Year of publication	2008
Journal volume	130
Pages of publication	12628 - 12629
a	19.401 ± 0.003 Å
b	16.398 ± 0.002 Å
c	20.871 ± 0.003 Å
α	90°
β	101.635 ± 0.003°
γ	90°
Cell volume	6503.4 ± 1.6 Å³
Cell temperature	373 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0688
Residual factor for significantly intense reflections	0.0515
Weighted residual factors for significantly intense reflections	0.1195
Weighted residual factors for all reflections included in the refinement	0.1264
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4108383.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4108383.cif
56737	2012-05-15	cif/ Adding structures of 4108383 via cif-deposit CGI script.	4108383.cif