Crystallography Open Database

Information card for entry 4108760

Preview

Coordinates	4108760.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41 H71 Al Li N O4
Calculated formula	C41 H71 Al Li N O4
Title of publication	Mixed Alkylamido Aluminate as a Kinetically Controlled Base
Authors of publication	Hiroshi Naka; James V. Morey; Joanna Haywood; Dana J. Eisler; Mary McPartlin; Felipe García; Hironaga Kudo; Yoshinori Kondo; Masanobu Uchiyama; Andrew E. H. Wheatley
Journal of publication	Journal of the American Chemical Society
Year of publication	2008
Journal volume	130
Pages of publication	16193 - 16200
a	10.514 ± 0.0001 Å
b	19.7762 ± 0.0003 Å
c	22.3649 ± 0.0004 Å
α	71.163 ± 0.005°
β	88.705 ± 0.005°
γ	80.96 ± 0.01°
Cell volume	4344.6 ± 0.2 Å³
Cell temperature	220 ± 2 K
Ambient diffraction temperature	220 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1066
Residual factor for significantly intense reflections	0.0928
Weighted residual factors for significantly intense reflections	0.2406
Weighted residual factors for all reflections included in the refinement	0.2569
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178833 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/87.	4108760.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4108760.cif
57130	2012-05-17	cif/ Adding structures of 4108760 via cif-deposit CGI script.	4108760.cif