Crystallography Open Database

Information card for entry 4109089

Preview

Coordinates	4109089.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H56 Al Cl N2 O2
Calculated formula	C37 H47 Al Cl N2 O2
Title of publication	Synthesis of an Optically Active Al(salalen) Complex and Its Application to Catalytic Hydrophosphonylation of Aldehydes and Aldimines
Authors of publication	Bunnai Saito; Hiromichi Egami; Tsutomu Katsuki
Journal of publication	Journal of the American Chemical Society
Year of publication	2007
Journal volume	129
Pages of publication	1978 - 1986
a	10.7603 ± 0.0003 Å
b	16.7937 ± 0.0004 Å
c	20.2847 ± 0.0005 Å
α	90°
β	90°
γ	90°
Cell volume	3665.55 ± 0.16 Å³
Cell temperature	183.1 K
Number of distinct elements	6
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for significantly intense reflections	0.0672
Weighted residual factors for all reflections included in the refinement	0.1756
Goodness-of-fit parameter for all reflections included in the refinement	0.997
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4109089.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4109089.cif
57841	2012-05-22	cif/ Adding structures of 4109089 via cif-deposit CGI script.	4109089.cif