Crystallography Open Database

Information card for entry 4109314

Preview

Coordinates	4109314.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H17 Ag B F4 N4 O2
Calculated formula	C25 H17 Ag B F4 N4 O2
Title of publication	Temperature-Dependent Synthesis of Metal-Organic Frameworks Based on a Flexible Tetradentate Ligand with Bidirectional Coordination Donors
Authors of publication	Yu-Bin Dong; You-Yun Jiang; Jie Li; Jian-Ping Ma; Feng-Ling Liu; Bo Tang; Ru-Qi Huang; Stuart R. Batten
Journal of publication	Journal of the American Chemical Society
Year of publication	2007
Journal volume	129
Pages of publication	4520 - 4521
a	31.483 ± 0.003 Å
b	7.3937 ± 0.0008 Å
c	28.16 ± 0.003 Å
α	90°
β	113.377 ± 0.002°
γ	90°
Cell volume	6016.9 ± 1.1 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1196
Residual factor for significantly intense reflections	0.0733
Weighted residual factors for significantly intense reflections	0.1979
Weighted residual factors for all reflections included in the refinement	0.2177
Goodness-of-fit parameter for all reflections included in the refinement	1.085
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178839 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/93.	4109314.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4109314.cif
58079	2012-05-24	cif/ Adding structures of 4109314 via cif-deposit CGI script.	4109314.cif