Crystallography Open Database

Information card for entry 4109612

Preview

Coordinates	4109612.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C108 H120 F10 P4 Pt2
Calculated formula	C108 H120 F10 P4 Pt2
Title of publication	sp Carbon Chains Surrounded by sp3 Carbon Double Helices: Directed Syntheses of Wirelike Pt(C\τbC)nPt Moieties That Are Spanned by Two P(CH2)mP Linkages via Alkene Metathesis
Authors of publication	Laura de Quadras; Eike B. Bauer; Wolfgang Mohr; James C. Bohling; Thomas B. Peters; José Miguel Martín-Alvarez; Frank Hampel; John A. Gladysz
Journal of publication	Journal of the American Chemical Society
Year of publication	2007
Journal volume	129
Pages of publication	8296 - 8309
a	39.914 ± 0.008 Å
b	11.143 ± 0.002 Å
c	22.639 ± 0.005 Å
α	90°
β	102.57 ± 0.03°
γ	90°
Cell volume	9828 ± 4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.078
Residual factor for significantly intense reflections	0.0429
Weighted residual factors for significantly intense reflections	0.0998
Weighted residual factors for all reflections included in the refinement	0.1146
Goodness-of-fit parameter for all reflections included in the refinement	0.977
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178842 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/96.	4109612.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4109612.cif
58389	2012-05-28	cif/ Adding structures of 4109612 via cif-deposit CGI script.	4109612.cif