Crystallography Open Database

Information card for entry 4109844

Preview

Coordinates	4109844.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H36 N8 O U
Calculated formula	C24 H28 N8 O U
Title of publication	Magnetic Exchange Coupling in Chloride-Bridged 5f-3d Heterometallic Complexes Generated via Insertion into a Uranium(IV) Dimethylpyrazolate Dimer
Authors of publication	Stosh A. Kozimor; Bart M. Bartlett; Jeffrey D. Rinehart; Jeffrey R. Long
Journal of publication	Journal of the American Chemical Society
Year of publication	2007
Journal volume	129
Pages of publication	10672 - 10674
a	8.6148 ± 0.0008 Å
b	18.0404 ± 0.0017 Å
c	8.8525 ± 0.0008 Å
α	90°
β	91.258 ± 0.002°
γ	90°
Cell volume	1375.5 ± 0.2 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170 ± 2 K
Number of distinct elements	5
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0421
Residual factor for significantly intense reflections	0.0323
Weighted residual factors for significantly intense reflections	0.0721
Weighted residual factors for all reflections included in the refinement	0.0746
Goodness-of-fit parameter for all reflections included in the refinement	1.007
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178844 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/98.	4109844.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4109844.cif
58622	2012-05-29	cif/ Adding structures of 4109844 via cif-deposit CGI script.	4109844.cif