Crystallography Open Database

Information card for entry 4109848

Preview

Coordinates	4109848.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H42.67 K N10 O U
Calculated formula	C29 H42.6667 K N10 O U
Title of publication	Magnetic Exchange Coupling in Chloride-Bridged 5f-3d Heterometallic Complexes Generated via Insertion into a Uranium(IV) Dimethylpyrazolate Dimer
Authors of publication	Stosh A. Kozimor; Bart M. Bartlett; Jeffrey D. Rinehart; Jeffrey R. Long
Journal of publication	Journal of the American Chemical Society
Year of publication	2007
Journal volume	129
Pages of publication	10672 - 10674
a	11.813 ± 0.002 Å
b	18.933 ± 0.004 Å
c	46.577 ± 0.009 Å
α	90°
β	90°
γ	90°
Cell volume	10417 ± 3 Å³
Cell temperature	113 ± 2 K
Ambient diffraction temperature	113 ± 2 K
Number of distinct elements	6
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.1046
Residual factor for significantly intense reflections	0.0697
Weighted residual factors for significantly intense reflections	0.1252
Weighted residual factors for all reflections included in the refinement	0.1333
Goodness-of-fit parameter for all reflections included in the refinement	1.11
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178844 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/98.	4109848.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4109848.cif
58626	2012-05-29	cif/ Adding structures of 4109848 via cif-deposit CGI script.	4109848.cif