Crystallography Open Database

Information card for entry 4110767

Preview

Coordinates	4110767.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	05052
Formula	C36 H82 Ho2 Si8
Calculated formula	C36 H82 Ho2 Si8
Title of publication	Generation of Dimethylsilylene and Allylidene Holmium Complexes from Trimethylsilylated Allyl Ligands
Authors of publication	Rosemary E. White; Timothy P. Hanusa; Benjamin E. Kucera
Journal of publication	Journal of the American Chemical Society
Year of publication	2006
Journal volume	128
Pages of publication	9622 - 9623
a	11.537 ± 0.005 Å
b	12.043 ± 0.005 Å
c	20.903 ± 0.005 Å
α	84.786 ± 0.005°
β	75.757 ± 0.005°
γ	69.666 ± 0.005°
Cell volume	2639.5 ± 1.7 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0439
Residual factor for significantly intense reflections	0.0302
Weighted residual factors for significantly intense reflections	0.0747
Weighted residual factors for all reflections included in the refinement	0.0819
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178878 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/07.	4110767.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4110767.cif
59609	2012-06-13	cif/ Adding structures of 4110767 via cif-deposit CGI script.	4110767.cif