Crystallography Open Database

Information card for entry 4111357

Preview

Coordinates	4111357.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H33 Li O6 Sn
Calculated formula	C37 H33 Li O6 Sn
Title of publication	Synthesis and Structure of Pentaorganostannate Having Five Carbon Substituents
Authors of publication	Masaichi Saito; Sanae Imaizumi; Tomoyuki Tajima; Kazuya Ishimura; Shigeru Nagase
Journal of publication	Journal of the American Chemical Society
Year of publication	2007
Journal volume	129
Pages of publication	10974 - 10975
a	11.585 ± 0.001 Å
b	20.8836 ± 0.0017 Å
c	15.2368 ± 0.0012 Å
α	90°
β	102.415 ± 0.002°
γ	90°
Cell volume	3600.1 ± 0.5 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0789
Residual factor for significantly intense reflections	0.067
Weighted residual factors for significantly intense reflections	0.139
Weighted residual factors for all reflections included in the refinement	0.1472
Goodness-of-fit parameter for all reflections included in the refinement	1.115
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4111357.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4111357.cif
60882	2012-06-18	cif/ Adding structures of 4111357 via cif-deposit CGI script.	4111357.cif