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Information card for entry 4112091
Preview
| Coordinates | 4112091.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | Dipp*Sn(N-SiMe3)SnDipp*.0.5n-hexane |
|---|---|
| Formula | C66 H90 N Si Sn2 |
| Calculated formula | C66 H90 N Si Sn2 |
| Title of publication | Reactions of the Heavier Group 14 Element Alkyne Analogues Ar'EEAr' (Ar' = C6H3-2,6(C6H3-2,6-Pri2)2; E = Ge, Sn) with Unsaturated Molecules: Probing the Character of the EE Multiple Bonds |
| Authors of publication | Chunming Cui; Marilyn M. Olmstead; James C. Fettinger; Geoffrey H. Spikes; Philip P. Power |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2005 |
| Journal volume | 127 |
| Pages of publication | 17530 - 17541 |
| a | 21.694 ± 0.004 Å |
| b | 18.392 ± 0.004 Å |
| c | 32.292 ± 0.007 Å |
| α | 90° |
| β | 96.47 ± 0.03° |
| γ | 90° |
| Cell volume | 12802 ± 5 Å3 |
| Cell temperature | 93 ± 2 K |
| Ambient diffraction temperature | 93 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | I 1 2/a 1 |
| Hall space group symbol | -I 2ya |
| Residual factor for all reflections | 0.1207 |
| Residual factor for significantly intense reflections | 0.0577 |
| Weighted residual factors for significantly intense reflections | 0.1433 |
| Weighted residual factors for all reflections included in the refinement | 0.1736 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178891 (current) | 2016-03-22 | cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/20. |
4112091.cif |
| 120077 | 2014-07-12 | Adding DOIs to range 4/11 structures. | 4112091.cif |
| 63711 | 2012-08-06 | cif/ Adding structures of 4112091 via cif-deposit CGI script. |
4112091.cif |
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Users of the data should acknowledge the original authors of the
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