Crystallography Open Database

Information card for entry 4112150

Preview

Coordinates	4112150.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Compound 1
Formula	C12 H34 Ag B11
Calculated formula	C12 H34 Ag B11
Title of publication	Silver-Phosphine Complexes of the Highly Methylated Carborane Monoanion [closo-1-H-CB11Me11]-
Authors of publication	Adam J. Clarke; Michael J. Ingleson; Gabriele Kociok-Köhn; Mary F. Mahon; Nathan J. Patmore; Jonathan P. Rourke; Giuseppe D. Ruggiero; Andrew S. Weller
Journal of publication	Journal of the American Chemical Society
Year of publication	2004
Journal volume	126
Pages of publication	1503 - 1517
a	15.7 ± 0.0001 Å
b	8.993 ± 0.0001 Å
c	15.705 ± 0.0002 Å
α	90°
β	112.5°
γ	90°
Cell volume	2048.6 ± 0.04 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/a 1
Hall space group symbol	-P 2yab
Residual factor for all reflections	0.0402
Residual factor for significantly intense reflections	0.0337
Weighted residual factors for significantly intense reflections	0.0853
Weighted residual factors for all reflections included in the refinement	0.0895
Goodness-of-fit parameter for all reflections included in the refinement	1.077
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178892 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/21.	4112150.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4112150.cif
64515	2012-08-19	cif/ Adding structures of 4112150 via cif-deposit CGI script.	4112150.cif