Crystallography Open Database

Information card for entry 4113860

Preview

Coordinates	4113860.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H68 Cr2 N8
Calculated formula	C32 H68 Cr2 N8
Title of publication	A Weak, Short Metal-Metal Bond in a Chromium(II) Amidinate Complex
Authors of publication	Azwana R. Sadique; Mary Jane Heeg; Charles H. Winter
Journal of publication	Journal of the American Chemical Society
Year of publication	2003
Journal volume	125
Pages of publication	7774 - 7775
a	13.107 ± 0.0015 Å
b	13.1084 ± 0.0015 Å
c	10.8607 ± 0.0011 Å
α	90°
β	90°
γ	90°
Cell volume	1866 ± 0.4 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	4
Space group number	114
Hermann-Mauguin space group symbol	P -4 21 c
Hall space group symbol	P -4 2n
Residual factor for all reflections	0.0534
Residual factor for significantly intense reflections	0.0341
Weighted residual factors for significantly intense reflections	0.0938
Weighted residual factors for all reflections included in the refinement	0.1
Goodness-of-fit parameter for all reflections included in the refinement	0.992
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178909 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/38.	4113860.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4113860.cif
67134	2012-09-19	cif/ Adding structures of 4113860 via cif-deposit CGI script.	4113860.cif