Crystallography Open Database

Information card for entry 4114191

Preview

Coordinates	4114191.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	(Dipp*Sn)2K(THF)6.2THF
Formula	C88 H130 K O8 Sn2
Calculated formula	C88 H130 K O8 Sn2
Title of publication	Germanium and Tin Analogues of Alkynes and Their Reduction Products
Authors of publication	Lihung Pu; Andrew D. Phillips; Anne F. Richards; Matthias Stender; Richard S. Simons; Marilyn M. Olmstead; Philip P. Power
Journal of publication	Journal of the American Chemical Society
Year of publication	2003
Journal volume	125
Pages of publication	11626 - 11636
a	17.433 ± 0.002 Å
b	18.014 ± 0.003 Å
c	14.475 ± 0.0018 Å
α	90°
β	96.551 ± 0.004°
γ	90°
Cell volume	4516 ± 1.1 Å³
Cell temperature	143 ± 2 K
Ambient diffraction temperature	143 ± 2 K
Number of distinct elements	5
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0705
Residual factor for significantly intense reflections	0.0546
Weighted residual factors for significantly intense reflections	0.1542
Weighted residual factors for all reflections included in the refinement	0.175
Goodness-of-fit parameter for all reflections included in the refinement	1.154
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178912 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/41.	4114191.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4114191.cif
67474	2012-09-26	cif/ Adding structures of 4114191 via cif-deposit CGI script.	4114191.cif