Crystallography Open Database

Information card for entry 4114343

Preview

Coordinates	4114343.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H36 Cl2 F2 P2 Pd
Calculated formula	C16 H36 Cl2 F2 P2 Pd
Title of publication	Synthesis of the Elusive (R3P)2MF2 (M = Pd, Pt) Complexes
Authors of publication	Anette Yahav; Israel Goldberg; Arkadi Vigalok
Journal of publication	Journal of the American Chemical Society
Year of publication	2003
Journal volume	125
Pages of publication	13634 - 13635
a	10.955 ± 0.0006 Å
b	14.568 ± 0.0008 Å
c	6.737 ± 0.0002 Å
α	90°
β	99.408 ± 0.003°
γ	90°
Cell volume	1060.71 ± 0.09 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	6
Space group number	8
Hermann-Mauguin space group symbol	C 1 m 1
Hall space group symbol	C -2y
Residual factor for all reflections	0.044
Residual factor for significantly intense reflections	0.0375
Weighted residual factors for significantly intense reflections	0.0744
Weighted residual factors for all reflections included in the refinement	0.0774
Goodness-of-fit parameter for all reflections included in the refinement	1.066
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178914 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/43.	4114343.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4114343.cif
67640	2012-10-01	cif/ Adding structures of 4114343 via cif-deposit CGI script.	4114343.cif