Crystallography Open Database

Information card for entry 4114353

Preview

Coordinates	4114353.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	(K-crypt)4[Ph2Sb-Ge9-Ge9-SbPh2].2.5en
Formula	C101 H184 Ge18 K4 N13 O24 Sb2
Calculated formula	C101 H184.05 Ge18 K4 N13 O24 Sb2
Title of publication	Derivatization of Deltahedral Zintl Ions by Nucleophilic Addition: [Ph-Ge9-SbPh2]2-and [Ph2Sb-Ge9-Ge9-SbPh2]4-
Authors of publication	Angel Ugrinov; Slavi C. Sevov
Journal of publication	Journal of the American Chemical Society
Year of publication	2003
Journal volume	125
Pages of publication	14059 - 14064
a	14.333 ± 0.005 Å
b	26.108 ± 0.008 Å
c	38.643 ± 0.014 Å
α	80.472 ± 0.007°
β	82.169 ± 0.006°
γ	84.332 ± 0.008°
Cell volume	14085 ± 8 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1734
Residual factor for significantly intense reflections	0.084
Weighted residual factors for significantly intense reflections	0.1928
Weighted residual factors for all reflections included in the refinement	0.2404
Goodness-of-fit parameter for all reflections included in the refinement	1.002
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178914 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/43.	4114353.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4114353.cif
67658	2012-10-02	cif/ Adding structures of 4114353 via cif-deposit CGI script.	4114353.cif