Crystallography Open Database

Information card for entry 4114358

Preview

Coordinates	4114358.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	(Rb-crypt)2Rb4(Ge9)(Ge9).7en
Formula	C24 H34 Ge9 N9 O6 Rb3
Calculated formula	C24 H34 Ge9 N9 O6 Rb3
Title of publication	Derivatization of Deltahedral Zintl Ions by Nucleophilic Addition: [Ph-Ge9-SbPh2]2-and [Ph2Sb-Ge9-Ge9-SbPh2]4-
Authors of publication	Angel Ugrinov; Slavi C. Sevov
Journal of publication	Journal of the American Chemical Society
Year of publication	2003
Journal volume	125
Pages of publication	14059 - 14064
a	10.138 ± 0.003 Å
b	13.881 ± 0.002 Å
c	19.311 ± 0.004 Å
α	76.76 ± 0.01°
β	80.9 ± 0.02°
γ	78.6 ± 0.01°
Cell volume	2574.9 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2263
Residual factor for significantly intense reflections	0.0948
Weighted residual factors for significantly intense reflections	0.209
Weighted residual factors for all reflections included in the refinement	0.2541
Goodness-of-fit parameter for all reflections included in the refinement	0.963
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178914 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/43.	4114358.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4114358.cif
67663	2012-10-02	cif/ Adding structures of 4114358 via cif-deposit CGI script.	4114358.cif