Crystallography Open Database

Information card for entry 4114380

Preview

Coordinates	4114380.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H20 Cl5 Ga P2
Calculated formula	C24 H20 Cl5 Ga P2
Title of publication	Phosphine Coordination Complexes of the Diphenylphosphenium Cation: A Versatile Synthetic Methodology for P-P Bond Formation
Authors of publication	Neil Burford; Paul J. Ragogna; Robert McDonald; Michael J. Ferguson
Journal of publication	Journal of the American Chemical Society
Year of publication	2003
Journal volume	125
Pages of publication	14404 - 14410
a	18.482 ± 0.006 Å
b	27.662 ± 0.008 Å
c	10.744 ± 0.005 Å
α	90°
β	90°
γ	90°
Cell volume	5493 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.2658
Residual factor for significantly intense reflections	0.0512
Weighted residual factors for all reflections	0.2082
Weighted residual factors for significantly intense reflections	0.1329
Goodness-of-fit parameter for all reflections	0.971
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4114380.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4114380.cif
67693	2012-10-02	cif/ Adding structures of 4114380 via cif-deposit CGI script.	4114380.cif