Crystallography Open Database

Information card for entry 4114421

Preview

Coordinates	4114421.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C6 H22 B18 Co Cs
Calculated formula	C6 H22 B18 Co Cs
Title of publication	Formation of Bridging Alkene and Conjugated Dialkenes Exclusively Generated from Alkynes on the [3,3'-Co(1,2-C~2~B~9~H~11~)~2~]^-^ Platform. The Unique Hydroboration Role of [3,3'-Co(1,2-C~2~B~9~H~11~)~2~]^-^
Authors of publication	Isabel Rojo; Francesc Teixidor; Raikko Kivekäs; Reijo Sillanpää; Clara Viñas
Journal of publication	Journal of the American Chemical Society
Year of publication	2003
Journal volume	125
Pages of publication	14720 - 14721
a	7.1731 ± 0.0001 Å
b	9.5405 ± 0.0001 Å
c	27.2413 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	1864.26 ± 0.04 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	33
Hermann-Mauguin space group symbol	P c 21 n
Hall space group symbol	P -2n -2ac
Residual factor for all reflections	0.041
Residual factor for significantly intense reflections	0.0297
Weighted residual factors for significantly intense reflections	0.0569
Weighted residual factors for all reflections included in the refinement	0.0603
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178915 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/44.	4114421.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4114421.cif
67742	2012-10-03	cif/ Adding structures of 4114421 via cif-deposit CGI script.	4114421.cif