Crystallography Open Database

Information card for entry 4115383

Preview

Coordinates	4115383.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C45 H69 Sb
Calculated formula	C45 H69 Sb
SMILES	[Sb](c1c(cc(cc1C(C)C)C(C)C)C(C)C)(c1c(cc(cc1C(C)C)C(C)C)C(C)C)c1c(cc(cc1C(C)C)C(C)C)C(C)C
Title of publication	Synthesis, Structure, and Redox Properties of the Extremely Crowded Triarylpnictogens: Tris(2,4,6-triisopropylphenyl)phosphine, Arsine, Stibine, and Bismuthine
Authors of publication	Shigeru Sasaki; Katsuhide Sutoh; Fumiki Murakami; Masaaki Yoshifuji
Journal of publication	Journal of the American Chemical Society
Year of publication	2002
Journal volume	124
Pages of publication	14830 - 14831
a	19.757 ± 0.002 Å
b	18.344 ± 0.002 Å
c	24.842 ± 0.004 Å
α	90°
β	111.049 ± 0.003°
γ	90°
Cell volume	8402.5 ± 1.8 Å³
Cell temperature	115.2 K
Number of distinct elements	3
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for significantly intense reflections	0.0344
Weighted residual factors for all reflections included in the refinement	0.0483
Goodness-of-fit parameter for all reflections included in the refinement	1.339
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4115383.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4115383.cif
68850	2012-11-21	cif/ Adding structures of 4115383 via cif-deposit CGI script.	4115383.cif